Process for manufacturing cold-rolled steel sheet
View Patent ↗A hot-rolled steel sheet having a composition comprising, in mass %, C: 0.06 to 0.3%, Si: 0.4 to 2.5%, Mn: 0.6 to 3.5%, P: at most 0.1%, S: at most 0.05%, Ti: 0 to 0.08%, Nb: 0 to 0.04%, a total content of Ti and Nb: 0 to 0.10%, sol.Al: 0 to 2.0%, Cr: 0 to 1%, Mo: 0 to 0.3%, V: 0 to 0.3%, B: 0 to 0.005%, Ca: 0 to 0.003%, REM: 0 to 0.003%, the remainder Fe and impurities, is cold rolled, then heated at an average heating rate of at least 15° C./sec so that a proportion of an unrecrystallization of a region not transformed to austenite at a time of reaching (Ac 1 point+10° C.) is at least 30 area %, and then held for 30 seconds at temperature of at least (0.9×Ac 1 point+0.1×Ac 3 point) and at most (Ac 3 point+100° C.).
1. A process for manufacturing a cold-rolled steel sheet comprising:
(A) a cold rolling step in which a hot-rolled steel sheet having a chemical composition comprising, in mass %, C: 0.06 to 0.3%, Si: 0.4 to 2.5%, Mn: 0.6 to 3.5%, P: at most 0.1%, S: at most 0.05%, Ti: 0 to 0.08%, Nb: 0 to 0.04%, a total content of Ti and Nb: 0 to 0.10%, sol.Al: 0 to 2.0%, Cr: 0 to 1%, Mo: 0 to 0.3%, V: 0 to 0.3%, B: 0 to 0.005%, Ca: 0 to 0.003%, REM: 0 to 0.003% and the remainder of Fe and impurities, is cold-rolled to obtain a cold-rolled steel sheet, wherein the hot-rolled steel sheet is a steel sheet in which average grain diameter of a BCC phase defined by high angle grain boundaries having a tilt angle of at least 15° is at most 6 μm, the steel sheet being obtained by a hot rolling step of cooling at a cooling rate (Crate) satisfying following Equation (5) for a temperature range from a temperature at the completion of rolling to a temperature at the completion of rolling—100° C. after completion of hot rolling in which hot rolling is completed at at least an Ar 3 point:
IC
(
T
)
=
0.1
-
3
×
10
-
3
·
T
+
4
×
10
-
5
·
T
2
-
5
×
10
-
7
·
T
3
+
5
×
10
-
9
·
T
4
-
7
×
10
-
11
·
T
5
∫
0
-
100
-
d
T
Crate
(
T
)
·
IC
(
T
)
<
4
(
5
)
where Crate (T) is a cooling rate (° C./s) (positive value),
T is a relative temperature (° C., negative value) with the temperature at the completion of rolling as zero, and
if there is a temperature at which Crate is zero, a value obtained by dividing a detention period (Δt) at the temperature by IC (T) is added as an integral for the section; and
(B) an annealing step in which the cold-rolled steel sheet obtained in the step (A) is annealed under conditions that the cold-rolled steel sheet is heated at an average heating rate of at least 15° C./sec so that a proportion of an unrecrystallization of a region not transformed to austenite at a time of reaching (Ac 1 point+10° C.) is at least 30 area %, and is then held in a temperature range of at least (0.9×Ac 1 point+0.1×Ac 3 point) and at most (Ac 3 point+100° C.) for at least 30 seconds.
2. The process for manufacturing cold-rolled steel sheet as set forth in claim 1 , wherein the hot-rolled steel sheet, after completion of hot rolling, is coiled at a temperature of at most 300° C. and subsequent heat treatment in a temperature range of 500° C. to 700° C.
3. The process for manufacturing cold-rolled steel sheet as set forth in claim 1 , wherein the cooling for the temperature range includes starting cooling at a cooling rate of at least 400° C./sec and cooling at the cooling rate for a temperature range of at least 30° C.
4. The process for manufacturing cold-rolled steel sheet as set forth in claim 1 , wherein the cooling for the temperature range includes starting water cooling at a cooling rate of at least 400° C./sec and cooling at the cooling rate for a temperature range of at least 30° C. and at most 80° C., and then stopping a water cooling stop time of 0.2 to 1.5 seconds to measure a shape of the sheet during the time, and subsequently cooling at a rate of at least 50° C./sec.
5. The process for manufacturing cold-rolled steel sheet as set forth in claim 1 , further comprising the step of plating the cold-rolled steel sheet after the (B) step.