METHODS OF FORMING POLYCRYSTALLINE TABLES AND POLYCRYSTALLINE ELEMENTS
Methods of forming a polycrystalline element comprise disposing a first plurality of particles comprising a superabrasive material, a second plurality of particles comprising the superabrasive material, and a catalyst material in a mold. The first and second pluralities of particles are sintered to form a polycrystalline table comprising a first region having a first permeability and a second region having a second, greater permeability. Catalyst material is at least substantially removed from the polycrystalline table. The polycrystalline table is attached to an end of a substrate, the at least a second region being interposed between the first region and the substrate. Polycrystalline elements comprise a substrate. A polycrystalline table comprising a superabrasive material and having a first region exhibiting a first permeability and at least a second region exhibiting a second, greater permeability is attached to an end of the substrate.
1 . A method of forming a polycrystalline element, comprising:
disposing a first plurality of particles comprising a superabrasive material, a second plurality of particles comprising the superabrasive material, and a catalyst material in a mold;
sintering the first and second pluralities of particles in the presence of the catalyst material to form a polycrystalline table comprising a first region having a first permeability and a second region having a second, greater permeability;
at least substantially removing the catalyst material from the polycrystalline table; and
attaching the polycrystalline table to an end of a substrate comprising a hard material, the at least a second region being interposed between the first region and the substrate.
2 . The method of claim 1 , further comprising:
disposing another substrate comprising a hard material in the mold prior to sintering;
sintering the first plurality of particles, the second plurality of particles, and the another substrate in the presence of the catalyst material to form a polycrystalline table comprising a first region having a first permeability and a second region having a second, greater permeability attached to an end of the another substrate, the second region being interposed between the first region and the another substrate; and
removing the another substrate after sintering.
3 . The method of claim 1 , further comprising:
disposing a third plurality of particles comprising the superabrasive material in the mold; and
sintering the first, second, and third pluralities of particles in the presence of the catalyst material to form a polycrystalline table comprising a first region having a first permeability, a second region comprising a second, greater permeability, and a third region disposed on an end of the first region opposing the at least a second region.
4 . The method of claim 1 , further comprising:
disposing another plurality of particles comprising a non-catalyst material removable by a leaching agent among the second plurality of particles in a region configured to form the second region after sintering.
5 . The method of claim 1 , wherein disposing a first plurality of particles comprising a superabrasive material, a second plurality of particles comprising the superabrasive material, and a catalyst material in a mold comprises disposing the first plurality of particles having a first packing density and the second plurality of particles having a second, lower packing density in the mold.
6 . The method of claim 1 , disposing a first plurality of particles comprising a superabrasive material, a second plurality of particles comprising the superabrasive material, and a catalyst material in a mold comprises disposing the first plurality of particles having a first average particle size and the second plurality of particles having a second, larger average particle size in the mold.
7 . The method of claim 6 , wherein disposing the first plurality of particles having a first average particle size and the second plurality of particles having a second, larger average particle size in the mold comprises disposing the first plurality of particles comprising at least some nanoparticles in the mold.
8 . The method of claim 1 , further comprising:
coating at least some of the first plurality of particles with the catalyst material using chemical solution deposition prior to disposing the first plurality of particles in the mold.
9 . The method of claim 1 , wherein sintering the first and second pluralities of particles in the presence of the catalyst material to form a polycrystalline table comprising a first region having a first permeability and a second region having a second, greater permeability comprises forming a polycrystalline table having a first region having a first volume percentage of superabrasive material and a second region having a second, lesser volume percentage of superabrasive material.
10 . The method of claim 1 , wherein sintering the first and second pluralities of particles in the presence of the catalyst material to form a polycrystalline table comprising a first region having a first permeability and a second region having a second, greater permeability comprises sintering the first and second pluralities of particles in the presence of the catalyst material to form a polycrystalline table having a first region comprising a first volume percentage of catalyst material disposed in interstitial spaces among interbonded grains of superabrasive material and a second region comprising a second, greater volume percentage of catalyst material disposed in interstitial spaces among interbonded grains of superabrasive material.
11 . The method of claim 1 , wherein attaching the polycrystalline table to an end of a substrate, the at least a second region being interposed between the first region and the substrate comprises infiltrating at least the second region of the polycrystalline table with a flowable material from the substrate during a sintering process.
12 . The method of claim 11 , wherein infiltrating at least the second region of the polycrystalline table with a flowable material from the substrate during a sintering process comprises infiltrating at least the second region of the polycrystalline table with another catalyst material different from the catalyst material used to form the polycrystalline table.
13 . A method of attaching a polycrystalline table to a substrate, comprising:
forming a polycrystalline table of superabrasive material and comprising a first region having a first permeability and a second region having a second, greater permeability;
at least substantially removing catalyst material from the polycrystalline table;
contacting the polycrystalline table on an end of a substrate comprising a hard material, the second region being interposed between the first region and the substrate; and
infiltrating at least the second region of the polycrystalline table with a flowable material from the substrate.
14 . The method of claim 13 , wherein forming a polycrystalline table of superabrasive material and comprising a first region having a first permeability and a second region having a second, greater permeability comprises forming the polycrystalline table comprising a third region disposed on an end of the first region opposing the at least a second region.
15 . The method of claim 13 , wherein forming a polycrystalline table of superabrasive material and comprising a first region having a first permeability and a second region having a second, greater permeability comprises forming the polycrystalline table having a first region comprising interstitial spaces among interbonded grains of superabrasive material with a first interconnectivity and a second region comprising interstitial spaces among interbonded grains of superabrasive material with a second, greater interconnectivity.
16 . The method of claim 13 , wherein forming a polycrystalline table of superabrasive material and comprising a first region having a first permeability and a second region having a second, greater permeability comprises forming the polycrystalline table comprising a first region having a first density of superabrasive material and a second region having a second, lesser density of superabrasive material.