IP Library Granted Patent US 10,324,069
Granted Patent B2
US 10,324,069 · App. 15/441,372 · Granted Jun 18, 2019

Chromatographic system temperature control system

Inventors: Stanley D. Stearns (Houston, TX); Huamin Cai (Houston, TX); Chris Bishop (Houston, TX); Robert Simpson (Houston, TX); Chris S. Cowles (Houston, TX); Dale Ashworth (Houston, TX); Douglas Dailey (Houston, TX)
Assignee: Valco Instruments Company, L.P.
G01N30/30G01N2030/3069G01N2030/3084
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Quick Facts
Patent No.
US 10,324,069
App. No.
15/441,372
Granted
Jun 18, 2019
Kind
B2
Abstract

A temperature controller for simultaneously controlling the temperatures of a plurality of heating elements for use in chromatographic analysis including columns, detectors, valves, transport lines and other components.

Claims (30)

1. A chromatographic system, comprising:

a first chromatographic component selected from the group consisting of a transport line, a valve, a sample loop, a column, and a detector;

a second chromatographic component selected from the group comprising a transport line, a valve, a sample loop, a column, and a detector;

a first electrically-controlled heating element associated with the first chromatographic component;

a second electrically-controlled heating element associated with the second chromatographic component;

a first temperature sensor associated with the first chromatographic component, the first temperature sensor generating a first temperature sensor signal;

a second temperature sensor associated with the second chromatographic component, the second temperature sensor generating a second temperature sensor signal;

a power supply;

a temperature controller, the temperature controller having a processor, a first electrically-controlled heating element output, a second electrically-controlled heating element output, a first temperature sensor input, and a second temperature sensor input;

the processor adapted to receive the first temperature sensor signal at the first temperature sensor input and to construct a first actual time-temperature profile;

the processor adapted to receive the second temperature sensor signal at the second temperature sensor input and to construct a second actual time-temperature profile;

the processor adapted to receive a first time-temperature profile for the first chromatographic component;

the processor adapted to receive a second time-temperature profile for the second chromatographic component selected from the group of the first time-temperature profile and the first actual time-temperature profile of the first chromatographic component;

the processor having a first power supply control for controlling a first output from the power supply to the first electrically-controlled heating element output;

the processor having a second power supply control for controlling a second output from the power supply to the first electrically-controlled heating element output;

the processor adapted to alter the first output from the power supply so the first actual time-temperature profile approaches the first time-temperature profile;

the processor adapted to alter the second output from the power supply so the second actual time-temperature profile approaches the second time-temperature profile.

2. The chromatographic system of claim 1 wherein one of the first electrically-controlled heating element and the second electrically-controlled heating element is a wire composed of nickel.

3. The chromatographic system of claim 1 wherein one of the first electrically-controlled heating element and the second electrically-controlled heating element is a wire composed of a nickel alloy.

4. The chromatographic system of claim 1 further comprising a fan to induce air flow about one of the first component and the second component, wherein the processor has a third power supply control for controlling a third output from the power supply to the fan.

5. A temperature controller, comprising

a processor, a first electrically-controlled heating element output, a second electrically-controlled heating element output, a first temperature sensor input, and a second temperature sensor input;

the processor adapted to receive the first temperature sensor signal at the first temperature sensor input and to construct a first actual time-temperature profile;

the processor adapted to receive the second temperature sensor signal at the second temperature sensor input and to construct a second actual time-temperature profile;

the processor adapted to receive a first time-temperature profile for the first chromatographic component;

the processor adapted to receive a second time-temperature profile for the second chromatographic component selected from the group of the first time-temperature profile and the first actual time-temperature profile of the first chromatographic component;

the processor having a first power supply control for controlling a first output from the power supply to the first electrically-controlled heating element output;

the processor having a second power supply control for controlling a second output from the power supply to the first electrically-controlled heating element output;

the processor adapted to alter the first output from the power supply so the first actual time-temperature profile approaches the first time-temperature profile;

the processor adapted to alter the second output from the power supply so the second actual time-temperature profile approaches the second time-temperature profile.

Assignments (2)
CONVERSION OF CORPORATE ENTITY Recorded Feb 18, 2022
From: VALCO INSTRUMENTS COMPANY, L.P.
To: VALCO INSTRUMENTS COMPANY, INC.
Reel/Frame 059232/0008 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 13, 2017
From: STEARNS, STANLEY D.; CAI, HUAMIN; HOCKMAN, MATIAS; BISHOP, CHRIS; SIMPSON, ROBERT; COWLES, CHRIS S.; ASHWORTH, DALE; DAILEY, DOUGLAS
To: VALCO INSTRUMENTS COMPANY,L.P.
Reel/Frame 042004/0761 →
Continuity (1)
Related Publication 20180246074A1 · Aug 30, 2018