IP Library Granted Patent US 9,839,693
Granted Patent B2
US 9,839,693 · App. 15/454,244 · Granted Dec 12, 2017

Anhydrous hydrogel composition and delivery system

Inventors: John Borja (Keyport, NJ); Stephanie Sharon Hayano (Millerton, NY)
Assignee: Acupac Packaging, Inc.
A61K47/38A23L29/20A61K8/0216A61K8/042A61K8/345A61K8/355A61K8/731A61K9/06A61K31/05A61K38/1793A61K47/10A61Q11/00A23V2002/00A61K2800/31A61K2800/81
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Quick Facts
Patent No.
US 9,839,693
App. No.
15/454,244
Granted
Dec 12, 2017
Kind
B2
Abstract

The present disclosure relates to anhydrous hydrogels useful as mucoadhesive (oral compositions) or as topical agents and may be used to deliver an active agent such as active pharmaceutical agents (API's), coagulants, fragrances, flavors, and other actives and excipients.

Claims (38)

1. A composition, comprising:

a. sodium carboxymethyl cellulose (NaCMC) in an amount of from 5% (w/w) to 30% (w/w), said sodium carboxymethyl cellulose including minimal residual water; and

b. anhydrous glycerine in an amount of from 70% (w/w) to 95% (w/w), wherein said composition is a solid or semi-solid gel composition.

2. The composition according to claim 1 , further including an active agent in an amount of from 0.1% (w/w) to 30% (w/w).

3. The composition according to claim 2 , wherein said active agent is cannabidiol (CBD).

4. The composition according to claim 2 , wherein said active agent is selected from cannabidiol (CBD) oil and tetrahydrocannabinol (THC) oil.

5. The composition according to claim 1 , wherein said anhydrous glycerin includes not more than 0.5% water.

6. The composition according to claim 2 , wherein said active agent is moisture sensitive.

7. The composition according to claim 6 , wherein said moisture sensitive active agent comprises pharmaceutical agents including biologicals, enzymes, proteins and fragments thereof, Adderall, alprazolam, gemifloxacin, hydromorphone and zolmitriptan.

8. The composition according to claim 2 wherein said active agent is a pharmaceutical agent selected from analgesics, decongestants, bronchodilators, antiasthmatic agents, cardiovascular agents, diabetic agents, antihistamines, anesthetics, antifungals, anti-nauseants, antiemetics, antibacterial agents, antifungal agents, corticosteroids, neurological agents, anti-inflammatories, vaccines, biological agents, wound healing agents, anticonvulsants and vitamins.

9. The composition according to claim 2 wherein said active agent is a wound healing agent selected from becaplermin, antimicrobial agents, silver, povidone-iodine, polyhexamethylene biguanide, dialkylcarbamoylchloride, lactoferrin, and growth factors.

10. The composition according to claim 2 wherein said active agent is a cosmetic agent.

11. The composition according to claim 10 wherein said active agent is the cosmetic agent ubiquinone.

12. The composition according to claim 2 wherein said active agent is a dental adhesive.

13. The composition according to claim 2 wherein said solid or semi-solid gel composition comprises:

a. sodium carboxymethyl cellulose (NaCMC) in an amount of from 10% (w/w) to 20% (w/w);

b. anhydrous glycerin in an amount of from 80% (w/w) to 90% (w/w); and

c. active agent in an amount of from 0.1% (w/w) to 30% (w/w).

14. The composition according to claim 2 wherein said solid or semi-solid gel composition comprises:

a. sodium carboxymethyl cellulose (NaCMC) in an amount of from 14% (w/w) to 16% (w/w);

b. anhydrous glycerin in an amount of from 84% (w/w) to 86% (w/w); and

c. the active agent in an amount of from 0.1% (w/w) to 30% (w/w).

15. The composition according to claim 2 wherein said solid or semi-solid gel composition is in unit dosage form.

16. A composition, comprising:

a. sodium carboxymethyl cellulose (NaCMC) in an amount of from 5% (w/w) to 30% (w/w), said sodium carboxymethyl cellulose including minimal residual water;

b. anhydrous glycerine in an amount of from 70% (w/w) to 95% (w/w); and

c. cannabidiol (CBD) in an amount of from 0.1% (w/w) to 30% (w/w), wherein said composition is a solid or semi-solid gel composition.

17. A method of preparing a composition comprising:

a. mixing to homogeneity the following:

i. sodium carboxymethyl cellulose (NaCMC) in an amount of from 5% (w/w) to 30% (w/w), said sodium carboxymethyl cellulose including minimal residual water; and

ii. anhydrous glycerine in an amount of from 70% (w/w) to 95% (w/w); and

b. adding sufficient energy to transform the mixture into a solid or semi-solid gel composition.

18. The method according to claim 17 , wherein said mixing step further includes adding an active agent in an amount of from 0.1% (w/w) to 30% (w/w).

19. The method according to claim 17 wherein the energy source is heat.

20. The method according to claim 17 wherein the energy source is radiation.

21. The method according to claim 20 wherein the energy source is heat.

22. The method according to claim 18 , wherein the active agent is cannabidiol (CBD).

23. A kit comprising the composition of claim 1 .

Assignments (5)
SECURITY INTEREST Recorded Aug 15, 2023
From: ACUPAC PACKAGING, INC.
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 064594/0880 →
CORRECTIVE ASSIGNMENT TO CORRECT THE PATENT SCHEDULE BY REMOVING INCORRECTLY LISTED PATENT APPLICATIONS AND PATENTS (ADDEDUM TO SCHEDULE ATTACHED) PREVIOUSLY RECORDED ON REEL 047984 FRAME 0611. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT SECURITY AGREEMENT. Recorded Oct 6, 2021
From: ACUPAC PACKAGING, INC.; AROMAIR FINE FRAGRANCE COMPANY; KDC US HOLDINGS, INC.; KOLMAR LABORATORIES, INC.; KNOWLTON DEVELOPMENT CORPORATION INC.; KNOWLTON PACKAGING INC.; THIBIANT INTERNATIONAL, INC.
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 058115/0820 →
CORRECTIVE ASSIGNMENT TO CORRECT THE SCHEDULE I PREVIOUSLY RECORDED ON REEL 047984 FRAME 0611. ASSIGNOR(S) HEREBY CONFIRMS THE PATENT SECURITY AGREEMENT. Recorded Feb 18, 2021
From: ACUPAC PACKAGING, INC.; AROMAIR FINE FRAGRANCE COMPANY; KDC US HOLDINGS, INC.; KOLMAR LABORATORIES, INC.; THIBIANT INTERNATIONAL, INC.; KNOWLTON DEVELOPMENT CORPORATION INC.; KNOWLTON PACKAGING INC.
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 055342/0163 →
PATENT SECURITY AGREEMENT Recorded Dec 26, 2018
From: ACUPAC PACKAGING, INC.; AROMAIR FINE FRAGRANCE COMPANY; KDC US HOLDINGS, INC.; KOLMAR LABORATORIES, INC.; THIBIANT INTERNATIONAL, INC.; KNOWLTON DEVELOPMENT CORPORATION INC.; KNOWLTON PACKAGING INC.
To: UBS AG, STAMFORD BRANCH, AS COLLATERAL AGENT
Reel/Frame 047984/0611 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 30, 2017
From: BORJA, JOHN; HAYANO, STEPHANIE SHARON
To: ACUPAC PACKAGING, INC.
Reel/Frame 043981/0826 →
Continuity (3)
Continuation 14280220 · May 16, 2014
Provisional Application 61824893 · May 17, 2013
Related Publication 20170239359A1 · Aug 24, 2017