IP Library Granted Patent US 9,956,188
Granted Patent B2
US 9,956,188 · App. 15/459,093 · Granted May 1, 2018

Eutectic formulations of cyclobenzaprine hydrochloride and amitriptyline hydrochloride

Inventors: Marino Nebuloni (Rho, IT); Patrizia Colombo (Trezzano sul Naviglio, IT)
Assignee: TONIX PHARMA HOLDINGS LIMITED
A61K31/135A61K47/26
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Quick Facts
Patent No.
US 9,956,188
App. No.
15/459,093
Granted
May 1, 2018
Kind
B2
Abstract

The present invention relates to pharmaceutical compositions and methods of manufacturing the same, comprising a eutectic of Cyclobenzaprine HCl and mannitol or Amitriptyline HCl and mannitol.

Claims (9)

1. A eutectic of mannitol and cyclobenzaprine HCl, comprising 75%±2% cyclobenzaprine HCl and 25%±2% mannitol by weight.

2. The eutectic of claim 1 , wherein the cyclobenzaprine HCl is micronized cyclobenzaprine HCl.

3. A method of manufacturing the eutectic of claim 1 , said method comprising mixing cyclobenzaprine HCl and mannitol or milling cyclobenzaprine HCl and mannitol, wherein the eutectic comprises 75%±2% cyclobenzaprine HCl and 25%±2% mannitol by weight.

4. The method of claim 3 , comprising milling cyclobenzaprine HCl and mannitol.

5. The method of claim 4 , wherein, the cyclobenzaprine HCl and mannitol are milled in a high shear granulator.

6. The method of claim 3 , comprising mixing cyclobenzaprine HCl and mannitol.

7. The method of claim 6 , wherein the cyclobenzaprine HCl and mannitol are mixed via compression.

8. The method of claim 7 , wherein the cyclobenzaprine HCl and mannitol are compressed via roller compaction.

9. The method of claim 3 , wherein the cyclobenzaprine HCl is micronized cyclobenzaprine HCl.

Assignments (5)
NOVATION AGREEMENT Recorded Jul 8, 2024
From: TONIX PHARMA HOLDINGS LIMITED
To: TONIX PHARMA LIMITED
Reel/Frame 068217/0592 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 25, 2020
From: TONIX PHARMACEUTICALS, INC.
To: TONIX PHARMA HOLDINGS LIMITED
Reel/Frame 052010/0959 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2017
From: NEBULONI, MARINO; COLOMBO, PATRIZIA
To: REDOX SRL
Reel/Frame 042576/0185 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2017
From: REDOX SRL
To: TONIX PHARMACEUTICALS, INC.
Reel/Frame 042576/0200 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 2, 2017
From: TONIX PHARMACEUTICALS, INC.
To: TONIX PHARMA HOLDINGS LIMITED
Reel/Frame 042576/0213 →
Continuity (3)
Continuation 14214433 · Mar 14, 2014
Provisional Application 61792757 · Mar 15, 2013
Related Publication 20170239195A1 · Aug 24, 2017