Methods of making polycrystalline diamond bodies having annular regions with differing characteristics
View Patent ↗Polycrystalline diamond bodies having an annular region of diamond grains and a core region of diamond grains and methods of making the same are disclosed. In one embodiment, a polycrystalline diamond body includes an annular region of inter-bonded diamond grains having a first characteristic property and a core region of inter-bonded diamond grains bonded to the annular region and having a second characteristic property that differs from the first characteristic property. The annular region decreases in thickness from a perimeter surface of the polycrystalline diamond body towards a centerline axis.
1. A method of making a polycrystalline diamond body, comprising:
positioning a first quantity of diamond grains having a first characteristic property in a low-reactivity cup having a perimeter wall;
distributing the first quantity of diamond grains into an at least partially annular configuration in which the annular region decreases in thickness from the perimeter wall towards a centerline axis of the low-reactivity cup, wherein wherein the first quantity of diamond grains is distributed into the low-reactivity cup by displacing the unbonded diamond grains with a mandrel;
positioning a second quantity of diamond grains having a second characteristic property that differs from the first characteristic property in the low-reactivity cup, the second quantity of diamond grains be positioned to at least partially contact the perimeter wall of the low-reactivity cup and to at least partially contact the first quantity of diamond grains; and
subjecting the low-reactivity cup, the first quantity of diamond grains, and the second quantity of diamond grains to a HPHT process in which adjacent diamond grains are sintered to one another and form diamond-to-diamond bonds.
2. The method of claim 1 , further comprising, during the HPHT process, melting and directing a catalyst material through the first quantity of diamond grains and the second quantity of diamond grains, thereby encouraging diamond-to-diamond bonding of adjacent diamond grains.
3. The method of claim 1 , further comprising positioning a substrate material proximate to the second quantity of diamond grains to enclose the low-reactivity cup.
4. The method of claim 3 , wherein the substrate material comprises hard metal carbides.
5. The method of claim 4 , wherein the substrate material further comprises a catalyst material.
6. The method of claim 1 , further comprising mixing catalyst material into the second quantity of diamond grains.
7. The method of claim 1 , further comprising mixing non-catalyst material into the second quantity of diamond grains.
8. The method of claim 7 , further comprising, during the HPHT process, melting the noncatalyst material and directing the non-catalyst material from the second quantity of diamond grains into the first quantity of diamond grains.
9. The method of claim 1 , wherein the second quantity of diamond grains is in direct contact with the first quantity of diamond grains.
10. The method of claim 2 , wherein the catalyst material comprises a metal from Group VIII in the periodic table.
11. The method of claim 1 , wherein the mandrel is rotated relative to the low-reactivity cup.
12. The method of claim 1 , wherein the mandrel is traversed into the low-reactivity cup.
13. A method of making a polycrystalline diamond body, comprising:
positioning a first quantity of diamond grains having a first characteristic property in a low-reactivity cup having a perimeter wall;
distributing the first quantity of diamond grains into an at least partially annular configuration in which the annular region decreases in thickness from the perimeter wall towards a centerline axis of the low-reactivity cup, wherein the first quantity of diamond grains are distributed into the low-reactivity cup by subjecting the first quantity of diamond grains to centripetal acceleration;
positioning a second quantity of diamond grains having a second characteristic property that differs from the first characteristic property in the low-reactivity cup, the second quantity of diamond grains be positioned to at least partially contact the perimeter wall of the low-reactivity cup and to at least partially contact the first quantity of diamond grains; and
subjecting the low-reactivity cup, the first quantity of diamond grains, and the second quantity of diamond grains to a HPHT process in which adjacent diamond grains are sintered to one another and form diamond-to-diamond bonds.
14. The method of claim 13 , wherein the low-reactivity cup is rotated as the first quantity of diamond grains are distributed into the low-reactivity cup.
15. The method of claim 13 , wherein the second quantity of diamond grains are distributed into the low-reactivity cup without the second quantity of diamond grains being subjected to centripetal acceleration.