Microwave Bonding For Coating Compositions
A method of bonding two or more components of a free flowing powder composition is described herein. At least a first component, such as for example, a metal effect pigment, and at least a second component, such as for example, an organic material is provided, and one or both components are heated by variable frequency microwave radiation to bond or fuse the components together. Coating compositions and coated articles made by the described method are also provided.
1 . A method of bonding a first component of a free flowing powder composition to a second component of the powder composition, comprising:
providing a first component;
providing a second component;
heating the first component or the second component using variable frequency microwave radiation to bond the first component and the second component together,
wherein the Tg of the second component is lower than the Tg of the first component.
2 . The method of claim 1 , wherein the first component is selected from organic material, inorganic material, and mixtures thereof.
3 . The method of claim 1 , wherein the second component is selected from organic material, inorganic material, and mixtures thereof.
4 . The method of claim 1 , wherein the first component is inorganic material.
5 . The method of claim 1 , wherein the first component is flake-type material.
6 . The method of claim 5 , wherein the flake-type material is selected from alumina, mica, MYLAR, glass, and mixtures or combinations thereof.
7 . The method of claim 1 , wherein the first component is metal.
8 . The method of claim 1 , wherein the first component is an inorganic pigment.
9 . The method of claim 1 , wherein the first component is an organic pigment.
10 . The method of claim 1 , wherein the second component comprises an organic binder having Tg between about 40° C. and 110° C.
11 . The method of claim 1 , wherein the second component comprises an organic binder, organic pigments, inorganic pigments, additives, and mixtures thereof.
12 . The method of claim 1 , wherein the second component comprises an organic binder, organic pigments, inorganic pigments, and mixtures thereof.
13 . The method of claim 1 , further comprising:
mixing at least the first component and second components together to obtain a uniform dispersion; and
heating the dispersion with a focused beam of variable frequency microwave radiation to bond the first and second components.
14 . The method of claim 13 , further comprising cooling the bonded powder components to room temperature.
15 . The method of claim 1 , further comprising:
mixing at least the first and second components together to form a uniform mixture; and
using a broad beam of variable frequency microwave radiation to heat the first component to a temperature adequate to raise the temperature of the second component above its Tg.
16 . The method of claim 1 , further comprising:
mixing at least the first and second components together to form a uniform mixture; and
using a broad beam of variable frequency microwave radiation to heat the second component to a temperature to raise the temperature of the second component to around its Tg.
17 . The method of claim 1 , further comprising:
mixing at least the first and second components together to form a uniform mixture; and
using a broad beam of microwave radiation at multiple wavelengths to heat the second component to a temperature adequate to raise the temperature of the second component to above its Tg.
18 . The method of claim 1 , further comprising:
mixing at least the first and second components together to form a uniform mixture;
spraying the mixture into an inert chamber; and
using a focused beam of variable frequency microwave radiation to heat the mixture to a temperature adequate to raise the temperature of the second component to above its Tg.
19 . The method of claim 1 , wherein the first component is present in an amount greater than about 7 to 8 wt % based on the total weight of the powder composition.
20 . The method of claim 1 , wherein the amount of the first and second component that remains unbonded after heating is less than about 1 wt % based on the total weight of the powder composition.