IP Library Granted Patent US 10,443,838
Granted Patent B2
US 10,443,838 · App. 15/479,471 · Granted Oct 15, 2019

Method for forming consistently-sized and controllably-timed droplets

Inventor: Larry Baxter (Orem, UT)
Assignee: Hall Labs LLC
F23D11/44B01D53/504B01D53/62B01D53/79F23D3/08F23K5/22B01D2257/302B01D2257/304B01D2257/404B01D2257/504B01D2259/124B05B1/02B05B7/00
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Quick Facts
Patent No.
US 10,443,838
App. No.
15/479,471
Granted
Oct 15, 2019
Kind
B2
Abstract

A method for forming substantially consistently-sized and substantially controllably-timed droplets is disclosed. An opening is provided through which a protrusion passes. The protrusion ends at a tip below the opening. A process liquid is provided to the opening at a controlled flow rate. The process liquid passes through the opening and flows along the protrusion, forming a droplet of the process liquid on the tip that reaches a substantially consistent droplet size and falls. The process liquid continues to pass through the opening at an even time interval based on the flow rate. In this manner, substantially consistently-sized and substantially controllably-timed droplets are formed.

Claims (25)

1. A method for forming substantially consistently-sized and substantially controllably-timed droplets comprising:

providing an opening with a conical protrusion passing through the opening, the conical protrusion ending at a tip below the opening, wherein:

a process liquid is provided to the opening at a controlled flow rate;

the process liquid, passing through the opening and flowing along the conical protrusion, forms droplets of the process liquid on the tip that reaches a substantially consistent droplet size and fall; and,

the process liquid continues to pass through the opening at an even time interval based on the flow rate;

whereby the droplets are substantially consistently-sized and substantially controllably-timed.

2. The method of claim 1 , providing a plate above the opening, wherein the conical protrusion is attached to the plate.

3. The method of claim 1 , further comprising attaching the conical protrusion to an interior side of the opening.

4. The method of claim 1 , forming the droplets in a system comprising spray towers, absorption towers, combustors, prilling towers, or combinations thereof.

5. The method of claim 4 , providing the process liquid to the combustor, the process liquid comprising a fuel.

6. The method of claim 4 , further comprising providing a contact gas or a contact vapor to the system and causing the droplets to interact with the contact gas or the contact vapor by mass exchange, heat exchange, or a combination thereof.

7. The method of claim 6 , providing the contact gas or the contact vapor comprising combustion flue gas, syngas, producer gas, natural gas, steam reforming gas, any hydrocarbon that has a lower freezing point than the temperature of the droplets, light gases, refinery off-gases, or combinations thereof.

8. The method of claim 7 , providing the contact gas or the contact vapor further comprising carbon dioxide, nitrogen oxide, sulfur dioxide, nitrogen dioxide, sulfur trioxide, hydrogen sulfide, hydrogen cyanide, water, hydrocarbons with a higher freezing point than the temperature of the droplets, or combinations thereof.

9. The method of claim 8 , providing the process liquid comprising any compound or mixture of compounds with a freezing point above a temperature at which a component of the contact gas or a component of the contact vapor solidifies.

10. The method of claim 1 , providing the conical protrusion with a surface material inhibiting an adsorption of gases, preventing a deposition of solids, or combinations thereof.

11. The method of claim 1 , providing the tip of the conical protrusion with a diameter smaller than the substantially consistent droplet size.

12. The method of claim 1 , further comprising providing a tube, wherein the opening is axially oriented inside the tube, the tube extending below a bottom portion of the opening and above the tip of the conical protrusion, the tube providing a gas flowing axially downward past the droplets to draw the droplets off the conical protrusion.

13. The method of claim 12 , forming the droplets in a system comprising spray towers, absorption towers, combustors, prilling towers, or combinations thereof.

14. The method of claim 13 , providing the process liquid to the combustor, the process liquid comprising a fuel.

15. The method of claim 13 , further comprising providing a contact gas or a contact vapor to the system and causing the droplets to interact with the contact gas or the contact vapor by mass exchange, heat exchange, or a combination thereof.

16. The method of claim 15 , providing the contact gas or the contact vapor comprising combustion flue gas, syngas, producer gas, natural gas, steam reforming gas, any hydrocarbon that has a lower freezing point than the temperature of the droplets, light gases, refinery off-gases, or combinations thereof.

17. The method of claim 16 , providing the contact gas or the contact vapor further comprising carbon dioxide, nitrogen oxide, sulfur dioxide, nitrogen dioxide, sulfur trioxide, hydrogen sulfide, hydrogen cyanide, water, hydrocarbons with a higher freezing point than the temperature of the droplets, or combinations thereof.

18. The method of claim 17 , providing the process liquid comprising any compound or mixture of compounds with a freezing point above a temperature at which a component of the contact gas or a component of the contact vapor solidifies.

19. The method of claim 12 , providing the conical protrusion with a surface material inhibiting an adsorption of gases, preventing a deposition of solids, or combinations thereof.

20. The method of claim 12 , providing the tip of the conical protrusion with a diameter smaller than the substantially consistent droplet size.

Assignments (5)
PATENT CONFIRMATORY GRANT Recorded Dec 28, 2022
From: SUSTAINABLE ENERGY SOLUTIONS, INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION
Reel/Frame 062231/0950 →
SECURITY INTEREST Recorded Oct 18, 2021
From: SUSTAINABLE ENERGY SOLUTIONS, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 057840/0920 →
CHANGE OF NAME Recorded Dec 21, 2020
From: SUSTAINABLE ENERGY SOLUTIONS, LLC
To: SUSTAINABLE ENERGY SOLUTIONS, INC.
Reel/Frame 054812/0649 →
CONFIRMATORY LICENSE Recorded Apr 10, 2020
From: SUSTAINABLE ENERGY SOLUTIONS, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 052372/0618 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 13, 2018
From: BAXTER, LARRY
To: SUSTAINABLE ENERGY SOLUTIONS, LLC
Reel/Frame 047827/0202 →
Continuity (1)
Related Publication 20180290154A1 · Oct 11, 2018
Cited By (1)
US 12,565,423