IP Library Granted Patent US 10,752,969
Granted Patent B2
US 10,752,969 · App. 15/537,578 · Granted Aug 25, 2020

Steel for suspension spring and method of manufacturing same

Inventors: Manabu Kubota (Nishinomiya, JP); Koichi Banno (Hokkaido, JP); Keisuke Chiba (Toyota, JP); Ryuuichi Seki (Hokkaido, JP)
Assignee: NIPPON STEEL CORPORATION
C21D8/06C21D9/52C22C38/00C22C38/02C22C38/04C22C38/06C22C38/18C22C38/20C22C38/22C22C38/24C22C38/26C22C38/28C22C38/40C22C38/42C22C38/44C22C38/46C22C38/48C22C38/50C22C38/54C22C38/58F16F1/02
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Quick Facts
Patent No.
US 10,752,969
App. No.
15/537,578
Granted
Aug 25, 2020
Kind
B2
Abstract

Steel for a suspension spring including, as a chemical composition, by % by mass: C: more than 0.40% and 0.65% or less; Si: 1.00% to 3.50%; Mn: more than 2.00% and 3.00% or less; Cr: 0.01% to 2.00%; V: 0.02% to 0.50%; P: 0.020% or less; S: 0.020% or less: N: 0.0100% or less; and a remainder of Fe and impurities, in which Kf is 280 or more, in which a structure contains a tempered martensite of which an area ratio is 90% or more, in which a Fe-based carbide precipitated in the tempered martensite is a cementite, and in which an average of an area ratios of prior austenite grains which stretch in a longitudinal direction of the steel and of which an aspect ratio exceeds 3.0, is 80% or more in a case of depths of 0.1 mm, 0.2 mm, and 0.3 mm in a sheet thickness direction from a surface of the steel.

Claims (51)

1. Steel for a suspension spring comprising, as a chemical composition, by % by mass:

C: more than 0.40% and 0.65% or less;

Si: 1.00% to 3.50%;

Mn: 2.10% to 3.00%;

Cr: 0.01% to 2.00%;

V: 0.02% to 0.50%;

Al: 0% to 0.060%;

Mo: 0% or more and less than 0.50%;

Cu: 0% to 1.00%;

Ni: 0% to 1.50%;

Nb: 0% to 0.015%;

Ti: 0% to 0.200%;

B: 0% to 0.0050%;

P: limited to 0.020% or less;

S: limited to 0.020% or less:

N: limited to 0.0100% or less; and

a remainder of Fe and impurities,

wherein Kf defined by the following Equation (1) is 280 or more,

wherein a structure contains a tempered martensite of which an area ratio is 90% or more,

wherein a Fe-based carbide precipitated in the tempered martensite is a cementite,

wherein an average of an area ratios of prior austenite grains which stretch in a longitudinal direction of the steel and of which an aspect ratio exceeds 3.0, is 80% or more in a case of depths of 0.1 mm, 0.2 mm, and 0.3 mm in a sheet thickness direction from a surface of the steel, and

wherein a tensile strength is 1900 MPa or more,

Kf= 10 (3.288×C (%)−0.168×Si (%)+1.068×Mn (%)+0.3×Ni (%)+1.266×Cr (%)+0.626×Cu (%)+2.086×Mo (%)−1.931)   (1)

here, C (%), Si (%), Mn (%), Ni (%), Cr (%), Cu (%), and Mo (%) in the equation (1) indicate the amounts of C, Si, Mn, Ni, Cr, Cu, and Mo by % by mass, and in a case where the elements are not contained, the value is 0.

2. The steel for a suspension spring according to claim 1 , comprising, as a chemical composition, by % by mass:

one of or two or more of Mo: 0.02% or more and less than 0.50%;

Cu: 0.02% to 1.0%;

Ni: 0.02% to 1.5%; and

Nb: 0.002% to 0.015%.

3. The steel for a suspension spring according to claim 1 or 2 , comprising, as a chemical composition, by % by mass:

one of or both of Ti: 0.010% to 0.200%; and

B: 0.0005% to 0.0050%,

in case the steel comprises Ti and B, the amount of Ti and the amount of N satisfy Ti≥3.5×N.

4. A method of manufacturing the steel for a suspension spring according to claim 1 , the method comprising:

heating a steel piece containing the chemical composition within a temperature range of 950° C. or more and less than 1150° C.;

a wire rod rolling including a finish rolling in which a reduction of an area is 30% or more and a finish rolling temperature is 750° C. to 850° C., with respect to the heated steel piece to obtain a wire rod;

winding with respect to the wire rod to make the wire rod into a coil;

cooling the coil so as to start cooling in 5 to 30 seconds after the performing of the winding and to set an average cooling rate when the temperature is 800 to 300° C. to be 5 to 50° C./s to cool the coil until reaching 300° C. or less; and

tempering of retention for 10 to 1800 seconds at 410° C. to 550° C. after the cooling.

5. A method of manufacturing the steel for a suspension spring according to claim 2 , the method comprising:

heating a steel piece containing the chemical composition within a temperature range of 950° C. or more and less than 1150° C.;

a wire rod rolling including a finish rolling in which a reduction of an area is 30% or more and a finish rolling temperature is 750° C. to 850° C., with respect to the heated steel piece to obtain a wire rod;

winding with respect to the wire rod to make the wire rod into a coil;

cooling the coil so as to start cooling in 5 to 30 seconds after the performing of the winding and to set an average cooling rate when the temperature is 800 to 300° C. to be 5 to 50° C./s to cool the coil until reaching 300° C. or less; and

tempering of retention for 10 to 1800 seconds at 410° C. to 550° C. after the cooling.

6. A method of manufacturing the steel for a suspension spring according to claim 3 , the method comprising:

heating a steel piece containing the chemical composition within a temperature range of 950° C. or more and less than 1150° C.;

a wire rod rolling including a finish rolling in which a reduction of an area is 30% or more and a finish rolling temperature is 750° C. to 850° C., with respect to the heated steel piece to obtain a wire rod;

winding with respect to the wire rod to make the wire rod into a coil;

cooling the coil so as to start cooling in 5 to 30 seconds after the performing of the winding and to set an average cooling rate when the temperature is 800 to 300° C. to be 5 to 50° C./s to cool the coil until reaching 300° C. or less; and

tempering of retention for 10 to 1800 seconds at 410° C. to 550° C. after the cooling.

Assignments (2)
CHANGE OF NAME Recorded May 14, 2019
From: NIPPON STEEL & SUMITOMO METAL CORPORATION
To: NIPPON STEEL CORPORATION
Reel/Frame 049257/0828 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 20, 2017
From: KUBOTA, MANABU; BANNO, KOICHI; CHIBA, KEISUKE; SEKI, RYUUICHI
To: NIPPON STEEL & SUMITOMO METAL CORPORATION
Reel/Frame 042753/0037 →
Priority Claims (1)
JP 2015-046915 · Mar 10, 2015 · national
Continuity (1)
Related Publication 20180265940A1 · Sep 20, 2018