IP Library Granted Patent US 10,358,532
Granted Patent B2
US 10,358,532 · App. 15/544,449 · Granted Jul 23, 2019

Method for producing a non-porous composite material that is water-absorbent and lipid-absorbent for active liquid compositions

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Quick Facts
Patent No.
US 10,358,532
App. No.
15/544,449
Granted
Jul 23, 2019
Kind
B2
Abstract

The subject matter of the present invention is a method for producing a biodegradable, non-porous composite material made water-absorbent and/or lipid-absorbent, used for obtaining diversely shaped solid objects to be subsequently loaded with active liquid hydrophilic and/or lipophilic compositions comprising at least one active ingredient intended to be delivered into an environment in a controlled and continuous manner.

Claims (29)

1. A method of making a non-porous biodegradable composite material that is made water-absorbent and/or lipid-absorbent for obtaining diversely shaped solid objects and to be subsequently loaded with a hydrophilic liquid composition or a lipophilic liquid composition comprising an active ingredient intended to be delivered into an environment in a controlled and continuous manner, comprising:

(a) selecting a base solid material or a mixture of a plurality of base solid materials, wherein the base solid material comprises lignocellulosic, glucidic, or protidic biopolymers of natural or synthetic origin;

(b) mixing the base solid material or the mixture of a plurality of base solid materials with a solid cohesion co-formulant or a solid coabsorbant;

(c) pulverizing a mixture of solid materials obtained in step (b);

(d) wetting the mixture obtained in step (c) at a moisture level between 9% and 13.5%;

(e) adding a liquid cohesion co-formulant or a liquid coabsorbant to the wetted mixture obtained in step (d) to get a fine powder or a meal;

(f) stocking the fine powder or the meal obtained in step (e) for maturation thereof;

(g) shaping the fine powder or meal obtained in step (f) into water-absorbent and/or lipid-absorbent non-porous solid objects;

(h) stocking the non-porous water-absorbent and/or lipid-absorbent solid objects obtained in step (g) in moisture-proof sealed containers;

subsequently incorporating the lipophilic liquid composition or the hydrophilic liquid composition in the non-porous solid objects obtained in step (h) resulting in a solid object;

(j) optionally, coating the solid object obtained in step (i); and

(k) stocking the solid object obtained in (i) or if applicable in (j) in a sealed container;

wherein the active ingredient is a fertilizer, a biostimulant, a plant protection substance, a herbicide, a biocide, an insecticide, an insect repellent, an attractant, a repellent, a pheromone, an antiparasitic, an anti-pest, a rodenticide, a fragrance, an essential oil, a plant extract, or a mixture thereof.

2. The method of claim 1 , wherein the lignocellulosic, glucidic, or protidic biopolymers are free or are in association in natural or synthetic structures.

3. The method of claim 1 , wherein the base solid material is an agro-industrial by-product chosen from sunflower, soy oil cake, grape seed oil cake, corncob, coffee grounds, wheat bran, pulp beet, wheat flour, corn flour, processed animal proteins or a mixture thereof.

4. The method of claim 1 , wherein the base solid material is a vegetal fiber from miscanthus , hemp, flax or a mixture thereof.

5. The method of claim 1 , wherein the solid cohesion co-formulant is a vegetal resin, a paraffin, a natural gum, a cellulose derivative, a soy isolate, a casein, a gelatin or a mixture thereof.

6. The method of claim 1 , wherein the solid coabsorbant is a biodegradable polymer, of a natural origin or not, having an affinity with the hydrophilic liquid composition or the lipophilic liquid composition to absorb.

7. The method of claim 1 , wherein the solid coabsorbant is a polysaccharide, a natural gum or a mixture thereof.

8. The method of claim 1 , wherein the coabsorbant is a liquid amphiphilic substance selected from glycerol, a long-carbon chain alcohol compatible with the hydrophilic liquid composition or the lipophilic liquid composition to absorb or a mixture thereof.

9. The method of claim 1 , wherein the coabsorbant is a liquid lipophilic substance selected from an oil of a vegetal or animal origin, a mineral oil or a mixture thereof.

10. The method of claim 1 , wherein the coabsorbant is added into the powder or meal at a level between 1% and 50% by weight relative to the total weight of the non-porous biodegradable composite material.

11. The method of claim 1 , wherein the coabsorbant is intended to form a network of hydrophilic and/or lipophilic absorbing wicks in the mass of the non-porous biodegradable composite material.

12. The method of claim 1 , wherein the hydrophilic and/or lipophilic wicks serve as penetration channels for the hydrophilic liquid composition or the lipophilic liquid composition into the non-porous biodegradable composite material.

13. An object for delivering an active ingredient into an environment, made of a water-absorbent and/or lipid-absorbent non-porous biodegradable composite material obtained from the method of claim 1 , wherein the object is shaped as granules of sizes varying between 2 millimeters and 1 centimeter in diameter and 2 millimeters and 4 centimeters in length.

14. The object of claim 13 , wherein the object is shaped as plates with edges from 10 centimeters to 1 meter of side, or polyhedral.

15. The object of claim 13 , wherein the object is loaded with an hydrophilic liquid composition or a lipophilic liquid composition comprising an active ingredient chosen from a fertilizer, a biostimulant, a plant protection substance, a herbicide, a biocide, an insecticide, an insect repellent, an attractant, a repellent, a pheromone, an antiparasitic, an anti-pest, a rodenticide, a fragrance, an essential oil, a plant extract, or a mixture thereof.

16. The object of claim 13 , wherein the hydrophilic liquid composition or lipophilic liquid composition absorbed is at a level of between 5% and 50% by weight relative to the weight of the object.

17. A method of delivering at least one active ingredient into an environment in a controlled and continuous manner comprising using the object of claim 13 in agriculture, human or animal feeding, breeding, veterinary medicine, hygiene, perfumery, ambient air treatment, or maintenance of green spaces.

Assignments (2)
MERGER Recorded Mar 24, 2023
From: AB7 INNOVATION SASU
To: AB7 SANTE
Reel/Frame 063088/0287 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 23, 2019
From: CHELLE, RENÉ; NGUYEN, DAVID; VILBERT, ARNAUD
To: AB7 INNOVATION S.A.S.U.
Reel/Frame 049269/0269 →