IP Library Granted Patent US 10,934,193
Granted Patent B2
US 10,934,193 · App. 15/571,860 · Granted Mar 2, 2021

Advanced oxidation process methods for degasification of reactor vessel

Inventors: Adam Szczesniak (Berlin, CT); Jonathan H. Wood (Needham, MA); Bruce L. Coulter (Rockford, IL); Christopher Hall (Colorado Springs, TX)
Assignee: Evoqua Water Technologies LLC
C02F1/725C02F1/001C02F1/20C02F1/32C02F1/722C02F1/004C02F2101/34C02F2101/36C02F2101/38C02F2103/06C02F2305/10Y02A20/152
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Quick Facts
Patent No.
US 10,934,193
App. No.
15/571,860
Granted
Mar 2, 2021
Kind
B2
Abstract

According to various aspects and embodiments, a system and method for treating groundwater contaminated with an organic contaminant is provided. According to some embodiments, the contaminated groundwater is treated by introducing a persulfate to produce a first treated aqueous solution, exposing the first treated aqueous solution to ultraviolet light to produce a second treated aqueous solution and one or more gases, and removing the one or more gases generated from exposing the first treated aqueous solution to the ultraviolet light.

Claims (29)

1. A method of removing 1,4-dioxane from a groundwater, comprising:

providing a contaminated groundwater having an initial concentration of 1,4-dioxane of at least 25 ppb;

introducing a persulfate to the contaminated groundwater to produce a first treated aqueous solution;

exposing the first treated aqueous solution to ultraviolet light to produce a second treated aqueous solution and one or more gases from oxidation of the 1,4-dioxane, the second treated aqueous solution having a concentration of the 1,4-dioxane less than about 1 ppb; and

removing the one or more gases generated from exposing the first treated aqueous solution to the ultraviolet light.

2. The method of claim 1 , wherein exposing the first treated aqueous solution comprises introducing the first treated aqueous solution to a reactor vessel.

3. The method of claim 2 , wherein removing the one or more gases comprises removing the one or more gases from the reactor vessel.

4. The method of claim 3 , wherein the one or more gases are removed from the reactor vessel through a degasifier coupled to the reactor vessel.

5. The method of claim 2 , wherein removing the one or more gases comprises removing the one or more gases from a conduit exiting the reactor vessel.

6. The method of claim 2 , wherein the contaminated groundwater is introduced to the reactor vessel at a flow rate of at least 100 gallons per minute.

7. The method of claim 1 , further comprising directing the one or more gases and at least a portion of the second treated aqueous solution to a storage device, the storage device configured to remove at least a portion of the one or more gases.

8. The method of claim 7 , further comprising recirculating at least a portion of the second treated aqueous solution from the storage device to a point upstream from the introduction of the persulfate.

9. The method of claim 1 , further comprising introducing the contaminated groundwater to a media filter prior to introducing the persulfate.

10. The method of claim 1 , further comprising extracting the contaminated groundwater from a remediation site.

11. The method of claim 1 , wherein the contaminated groundwater has an initial 1,4-dioxane concentration of up to about 800 ppb.

12. A system for removing 1,4-dioxane from a groundwater, comprising:

a source of contaminated groundwater having an initial concentration of an 1,4-dioxane of at least 25 ppb;

a source of persulfate fluidly connected to the source of contaminated groundwater and configured to introduce a persulfate to the contaminated groundwater;

an actinic radiation source fluidly connected to the source of contaminated groundwater and configured to irradiate the contaminated groundwater and persulfate to oxidize the 1,4-dioxane in the contaminated groundwater to produce one or more gases;

at least one degasifier configured to remove the one or more gases from the irradiated groundwater.

13. The system of claim 12 , further comprising a reactor fluidly connected to the source of contaminated groundwater and the source of persulfate and configured to house the actinic radiation source.

14. The system of claim 13 , wherein at least one degasifier is coupled to the reactor.

15. The system of claim 14 , wherein the reactor is oriented horizontally.

16. The system of claim 13 , wherein at least one degasifier is coupled to a conduit exiting the reactor.

17. The system of claim 16 , wherein the reactor is oriented vertically.

18. The system of claim 13 , further comprising a storage device positioned downstream from the reactor, wherein at least one degasifier is coupled to the storage device.

19. The system of claim 12 , wherein at least one degasifier is coupled to a conduit in fluid communication with the source of persulfate.

20. The system of claim 12 , further comprising a media filter positioned upstream from the source of persulfate.

21. The system of claim 12 , wherein at least one degasifier is positioned upstream of the actinic radiation source.

Assignments (5)
RELEASE OF SECURITY INTEREST Recorded May 26, 2023
From: JPMORGAN CHASE BANK N.A., AS COLLATERAL AGENT
To: EVOQUA WATER TECHNOLOGIES LLC; NEPTUNE BENSON, INC.
Reel/Frame 063787/0943 →
SECURITY INTEREST Recorded Apr 7, 2021
From: EVOQUA WATER TECHNOLOGIES LLC; NEPTUNE BENSON, INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 055848/0689 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 23, 2018
From: SZCESNIAK, ADAM; WOOD, JONATHAN H.; COULTER, BRUCE L.; HALL, CHRISTOPHER T.
To: EVOQUA WATER TECHNOLOGIES LLC
Reel/Frame 045878/0279 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 10, 2018
From: SZCESNIAK, ADAM; WOOD, JONATHAN H.; COULTER, BRUCE L.; HALL, CHRISTOPHER
To: EVOQUA WATER TECHNOLOGIES LLC
Reel/Frame 045764/0124 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 8, 2018
From: SZCESNIAK, ADAM; WOOD, JONATHAN H.; COULTER, BRUCE L.; HILL, CHRISTOPHER
To: EVOQUA WATER TECHNOLOGIES LLC
Reel/Frame 044871/0950 →
Continuity (2)
Provisional Application 62158014 · May 7, 2015
Related Publication 20180134592A1 · May 17, 2018