IP Library Granted Patent US 10,682,290
Granted Patent B2
US 10,682,290 · App. 15/574,871 · Granted Jun 16, 2020

Kit of parts for conducting a dental impression and retraction process

Inventors: Henning Hoffmann (Windach, DE); Peter U. Osswald (Tuerkheim, DE); Joachim W. Zech (Kaufering, DE); Andreas R. Maurer (Langenneufnach, DE)
Assignee: 3M INNOVATIVE PROPERTIES COMPANY
A61K6/90A61K6/15A61K6/19C08L51/085C08L83/04
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Quick Facts
Patent No.
US 10,682,290
App. No.
15/574,871
Granted
Jun 16, 2020
Kind
B2
Abstract

The present invention relates to a kit of parts comprising Paste (A), Paste (B) and Paste (C), the pastes being characterized as follows: Paste (A) comprising at least one polyorganosiloxane with at least two olefinically unsaturated groups, and at least one organohydrogenpolysiloxane, at least one alkylsiloxane having at least one carbinol, silanol, alkoxy, carboxyl or amino group, optionally filler(s) and optionally additive(s); Paste (B) comprising at least one polyorganosiloxane optionally with olefinically unsaturated groups, at least one addition cure catalyst, optionally at least one alkylsiloxane having at least one carbinol, silanol, alkoxy, carboxyl or amino group, optionally filler(s) and optionally additive(s) Paste (C) comprising a softener, a condensation cure catalyst, optionally filler(s), and optionally additive(s) optionally at least one polyorganosiloxane optionally with olefinically unsaturated groups. The invention is also directed to a system for storing and delivering Paste (A), Paste (B) and Paste (C), the system comprising three compartments for storing the respective pastes, means for delivering the respective pastes to an outlet orifice and an interface for receiving a mixing tip. The kit of parts or the system is in particular useful for conducting a dental retraction and dental impression process.

Claims (74)

1. A kit of parts comprising Paste (A), Paste (B) and Paste (C) for conducting a dental impression and retraction process, comprising:

Paste (A) comprising:

at least one polyorganosiloxane with at least two olefinically unsaturated groups;

at least one organohydrogenpolysiloxane; and

at least one alkylsiloxane having at least one carbinol, silanol, alkoxy, carboxyl or amino group;

Paste (B) comprising:

at least one polyorganosiloxane optionally with olefinically unsaturated groups and

at least one addition cure catalyst;

and

Paste (C) comprising:

a softener; and

a condensation cure catalyst;

wherein the condensation cure catalyst being characterized by at least one of the following features:

being present in an amount from 0.1 to 15.0 wt.-% with respect to the weight of Paste (C);

comprising a Ti, Zr, Zn or Sn containing component.

2. The kit of parts of claim 1 , the addition cure catalyst being characterized by at least one of the following features:

comprising a Pt containing component;

being present in an amount from 0.00005 to 0.05 calculated as elemental platinum with respect to the weight of Paste (B).

3. The kit of parts claim 1 , Paste (A) being characterized by at least one of the following features:

having a consistency according to ISO 4823 in the range from 25 to 50 mm;

having a water contact angle, measured 10 s after placing a drop of water onto the surface of the paste of <90°.

4. The kit of parts of claim 1 , Paste (B) having a consistency of 25 to 50 mm, if determined according to ISO 4823.

5. The kit of parts of claim 1 , Paste (C) having a consistency of 25 to 50 mm, if determined according to ISO 4823.

6. The kit of parts to the of claim 5 , the additive(s) being selected from hydrophilating agent(s), retarder(s), inhibitor(s), colourant(s), stabilizer(s), flavouring(s), hydrogen scavenger(s), rheology modifier(s), astringent(s) and mixtures thereof.

7. A process for taking a dental impression of a dentition including sub-gingival parts of the sulcus, the process comprising:

providing the kit of parts as described in claim 1 ;

mixing Paste (A), Paste (B) and Paste (C) to obtain Composition (ABC);

applying Composition (ABC) into the sulcus of the dentition;

mixing Paste (A) and Paste (B) to obtain Composition (AB);

applying Composition (AB) in contact with Composition (ABC;

optionally applying a further Composition (D) being different from Composition (AB) and Composition (ABC) in contact with Composition (AB); and

removing Composition (ABC) and Composition (AB) and Composition (D), if present, from the dentition.

8. The process of claim 7 , wherein in step b) the mixing ratio of Paste (A), Paste (B) and Paste (C) is (A+B):C from 1:1 to 20:1 by volume, wherein Paste (A) and Paste (B) are mixed in a ratio from 10:1 to 1:5.

9. The process of claim 7 , wherein in step d) the mixing ratio of Paste (A), Paste (B) is from 10:1 to 1:5 by volume.

10. The process of claim 7 , wherein the Composition (ABC) is used in a smaller volume compared to Composition (AB).

11. The process of claim 7 , Composition (ABC) being characterized by at least one or all of the following features:

Consistency according to ISO 4823 of <30 mm;

Shore hardness A determined 10 min after mixing: >20;

Residual gap resistance: larger than 0.50 mm;

Water contact angle, measured 10 s after placing a drop of water onto the surface of the paste, of <90°;

Colour of Composition (ABC) being different from colour of Composition (AB).

12. The process of claim 7 , Composition (AB) being characterized by at least one or all of the following features:

Consistency according to ISO 4823 of >31 mm;

Shore hardness A determined 10 min after mixing: >20;

Residual gap behaviour: less than or equal to 0.2 mm;

Water contact angle, measured 10 s after placing a drop of water onto the surface of the paste, of <90.

13. A system for storing and delivering Paste (A), Paste (B) and Paste (C) as described in claim 1 , the system comprising three compartments for storing the respective pastes, means for delivering the respective pastes to an outlet orifice and an interface for receiving a mixing tip.

14. A process of conducting a dental retraction and dental impression process, the process comprising:

mixing Paste (A), Paste (B) and Paste (C) to obtain Composition (ABC);

applying composition (ABC) into the sulcus of a dentition;

mixing Paste (A) and Paste (B) to obtain Composition (AB);

applying composition (AB) in contact with Composition (ABC);

and removing Composition (ABC) an Composition (AB) from the dentition,

wherein Paste (A) comprises:

at least one polyorganosiloxane with at least two olefinically unsaturated groups, and

at least one organohydrogenpolysiloxane,

at least one alkylsiloxane having at least one carbinol, silanol, alkoxy, carboxyl or amino group;

wherein Paste (B) comprises:

at least one polyorganosiloxane optionally with olefinically unsaturated groups,

at least one addition cure catalyst

wherein Paste (C) comprises:

a softener;

a condensation cure catalyst

wherein the condensation cure catalyst is characterized by at least one of the following features:

being present in an amount from 0.1 to 15.0 wt.-% with respect to the weight of Paste (C);

comprising a Ti, Zr, Zn or Sn containing component.

15. The kit of parts of claim 1 , wherein Paste (A) further comprises filler(s).

16. The kit of parts of claim 1 , wherein Paste (A) further comprises additive(s).

17. The kit of parts of claim 1 , wherein Paste (B) further comprises at least one alkylsiloxane having at least one carbinol, silanol, alkoxy; carboxyl or amino group.

18. The kit of parts of claim 1 , wherein Paste (B) further comprises filler(s).

19. The kit of parts of claim 1 , wherein Paste (B) further comprises additive(s).

20. The kit of parts of claim 1 , wherein Paste (C) further comprises filler(s).

21. The kit of parts of claim 1 , wherein Paste (C) further comprises additive(s).

22. The kit of parts of claim 1 , wherein Paste (C) further comprises at least one polyorganosiloxane optionally with olefinically unsaturated groups.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2024
From: 3M INNOVATIVE PROPERTIES COMPANY
To: SOLVENTUM INTELLECTUAL PROPERTIES COMPANY
Reel/Frame 066430/0193 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 21, 2018
From: HOFFMANN, HENNING; OSSWALD, PETER U.; ZECH, JOACHIM W.; MAURER, ANDREAS R.
To: 3M INNOVATIVE PROPERTIES COMPANY
Reel/Frame 045302/0642 →
Priority Claims (1)
EP 15169805 · May 29, 2015 · regional
Continuity (1)
Related Publication 20180125764A1 · May 10, 2018