IP Library Patent Application 15610342
Patent Application
App. No. 15/610,342

WILD-CARD-MODIFICATION SEARCH TECHNIQUE FOR PEPTIDE IDENTIFICATION

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Quick Facts
Patent No.
US None
App. No.
15/610,342
Abstract

Embodiments of a computer system, a method, and a computer-program product (e.g., software) for analyzing tandem-mass-spectrometry data are described. Using this analysis technique, unanticipated chemical modifications to peptides associated with proteins can be identified. In particular, a modification called a wild-card modification is used to identify the most likely chemical modifications in the peptides. A wild-card modification allows the addition of any mass, typically any integer atomic mass within a range, to any one amino acid residue within a candidate peptide.

Claims (42)

1 . A method for identifying potential modifications to peptides associated with a precursor peptide, the method comprising:

receiving tandem-mass-spectrometry data associated with the precursor peptide, wherein the data includes a measured mass value for the precursor peptide and a number of peak locations;

generating one or more theoretical spectra for a candidate peptide using known spectral information associated with the candidate peptide, which comprises:

determining at least one variable mass modification to at least one amino acid within the candidate peptide; and

varying the variable mass modification within a predetermined range; and

identifying the potential modifications to the candidate peptide by comparing peak locations of the received tandem-mass-spectrometry data with peak locations of the generated theoretical spectra.

2 . The method of claim 1 , wherein the identified potential modifications include a post-translational modification.

3 . The method of claim 1 , wherein the identified potential modifications include a substitution of an amino acid.

4 . The method of claim 3 , further comprising:

obtaining the known spectral information associated with the candidate peptide from a predetermined peptide database;

modifying the candidate peptide based on the substitution of the amino acid; and

adding the modified candidate peptide to the predetermined database.

5 . The method of claim 1 , wherein generating the theoretical spectra further comprises applying one of more known mass modifications to the candidate peptide.

6 . The method of claim 5 , wherein the known modifications include: methylation, dimethylation, oxidation, deamidation, carbamylation, phosphorylation or acetylation.

7 . The method of claim 5 , wherein the known modifications include a known amino acid substitution.

8 . The method of claim 1 , wherein generating a respective theoretical spectrum further comprising shifting peak locations of fragments containing the at least one amino acid based on the variable mass modification.

9 . The method of claim 8 , wherein identifying the potential modifications to the candidate peptide involves an iterative process, in which a variable mass modification identified in a given iteration is treated as a known modification in a subsequent iteration.

10 . The method of claim 8 , wherein identifying the potential modifications to the candidate peptide involves an iterative process, in which a variable mass modification identified in a given iteration is treated as a known amino acid substitution in a subsequent iteration.

11 . A non-transitory computer-readable storage medium storing instructions that when executed by a computer system cause the computer to perform a method for identifying potential modifications to peptides associated with a precursor peptide, the method comprising:

receiving tandem-mass-spectrometry data associated with the precursor peptide, wherein the data includes a measured mass value for the precursor peptide and a number of peak locations;

generating one or more theoretical spectra for a candidate peptide using known spectral information associated with the candidate peptide, which comprises:

determining at least one variable mass modification to at least one amino acid within the candidate peptide; and

varying the variable mass modification within a predetermined range; and

identifying the potential modifications to the candidate peptide by comparing peak locations of the received tandem-mass-spectrometry data with peak locations of the generated theoretical spectra.

12 . The storage medium of claim 11 , wherein the identified potential modifications include a post-translational modification.

13 . The storage medium of claim 11 , wherein the identified potential modifications include a substitution of an amino acid.

14 . The storage medium of claim 11 , wherein generating the theoretical spectra further comprises applying one of more known mass modifications to the candidate peptide.

15 . The storage medium of claim 14 , wherein the known modifications include: methylation, dimethylation, oxidation, deamidation, carbamylation, phosphorylation or acetylation.

16 . The storage medium of claim 14 , wherein the known modifications include a known amino acid substitution.

17 . The storage medium of claim 11 , wherein generating a respective theoretical spectrum further comprising shifting peak locations of fragments containing the at least one amino acid based on the variable mass modification.

18 . The storage medium of claim 17 , wherein identifying the potential modifications to the candidate peptide involves an iterative process, in which a variable mass modification identified in a given iteration is treated as a known modification in a subsequent iteration.

19 . The method of claim 17 , wherein identifying the potential modifications to the candidate peptide involves an iterative process, in which a variable mass modification identified in a given iteration is treated as a known amino acid substitution in a subsequent iteration.

20 . A computer system, comprising:

a processor;

a storage device storing instructions that when executed by the processor cause the processor to perform a method for identifying potential modifications to peptides associated with a precursor peptide, the method comprising:

receiving tandem-mass-spectrometry data associated with the precursor peptide, wherein the data includes a measured mass value for the precursor peptide and a number of peak locations;

generating one or more modified theoretical spectra for a candidate peptide using known spectral information associated with the candidate peptide, which comprises:

identifying one or more known mass modifications for the candidate peptide;

determining at least one variable mass modification to at least one amino acid within the candidate peptide;

varying the variable mass modification within a predetermined range to produce a set of varied mass modifications; and

for each varied mass modification, generating a modified theoretical spectrum for the candidate peptide by combining the known mass modifications and the variable mass modification; and

identifying the potential modifications to the candidate peptide by comparing peak locations of the received tandem-mass-spectrometry data with peak locations of each modified theoretical spectrum.

Assignments (3)
RELEASE OF SECURITY INTEREST Recorded Jul 2, 2024
From: BARINGS FINANCE LLC, AS COLLATERAL AGENT
To: PROTEIN METRICS, INC.
Reel/Frame 067895/0115 →
TERMINATION OF PATENT SECURITY AGREEMENT AT REEL 58457/FRAME 0205 Recorded Jul 1, 2024
From: BARINGS FINANCE LLC, AS ADMINISTRATIVE AGENT AND COLLATERAL AGENT
To: PROTEIN METRICS, INC. (N/K/A PROTEIN METRICS, LLC)
Reel/Frame 068102/0310 →
SECURITY INTEREST Recorded Dec 22, 2021
From: PROTEIN METRICS INC.
To: BARINGS FINANCE LLC, AS COLLATERAL AGENT
Reel/Frame 058457/0205 →