IP Library Granted Patent US 10,301,213
Granted Patent B2
US 10,301,213 · App. 15/635,963 · Granted May 28, 2019

Inorganic fiber with improved shrinkage and strength

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Quick Facts
Patent No.
US 10,301,213
App. No.
15/635,963
Granted
May 28, 2019
Kind
B2
Abstract

An inorganic fiber containing silica and magnesia as the major fiber components and which further includes intended addition of lithium oxide to improve the thermal stability of the fiber. The inorganic fiber exhibits good thermal performance at 1260° C. and greater, low linear shrinkage, retains mechanical integrity after exposure to the use temperature, and exhibits low biopersistence in physiological fluids. Also provided are thermal insulation product forms prepared from a plurality of the inorganic fibers, methods of preparing the inorganic fiber and of thermally insulating articles using thermal insulation prepared from a plurality of the inorganic fibers.

Claims (13)

1. An inorganic fiber consisting essentially of the fiberization product of about 65 to about 86 weight percent silica, about 14 to about 35 weight percent magnesia, greater than 0 to about 2% alumina and greater than 0 to about 0.45 weight percent lithium oxide, wherein said inorganic fiber has compression recovery of at least about 10% after exposure to a temperature of 1400° C. for 24 hours, exhibits a shrinkage of 5% or less at 1260° C. for 24 hours and a shrinkage of 10% or less at 1400° C. for 24 hours.

2. The inorganic fiber of claim 1 , consisting essentially of the fiberization product of about 65 to about 86 weight percent silica, about 14 to about 35 weight percent magnesia, and greater than 0 to about 0.35 weight percent lithium oxide.

3. The inorganic fiber of claim 1 , consisting essentially of the fiberization product of about 70 to about 80 weight percent silica, about 20 to about 30 weight percent magnesia, and greater than 0 to about 0.45 weight percent lithium oxide.

4. The inorganic fiber of claim 3 , consisting essentially of the fiberization product of about 70 to about 80 weight percent silica, about 20 to about 30 weight percent magnesia, and greater than 0 to about 0.35 weight percent lithium oxide.

5. The inorganic fiber of claim 1 , consisting essentially of the fiberization product of about 75 to about 80 weight percent silica, about 20 to about 25 weight percent magnesia, and greater than 0 to about 0.45 weight percent lithium oxide.

6. The inorganic fiber of claim 5 , consisting essentially of the fiberization product of about 75 to about 80 weight percent silica, about 20 to about 25 weight percent magnesia, and greater than 0 to about 0.35 weight percent lithium oxide.

7. The inorganic fiber of claim 1 , consisting essentially of the fiberization product of about 76 to about 80 weight percent silica, about 20 to about 24 weight percent magnesia, greater than 0 to about 0.45 weight percent lithium oxide.

8. The inorganic fiber of claim 7 , consisting essentially of the fiberization product of about 76 to about 80 weight percent silica, about 20 to about 24 weight percent magnesia, greater than 0 to about 0.35 weight percent lithium oxide.

9. The inorganic fiber of claim 1 , consisting essentially of the fiberization product of about 77 to about 80 weight percent silica, about 20 to about 23 weight percent magnesia, greater than 0 to about 0.45 weight percent lithium oxide.

10. The inorganic fiber of claim 9 , consisting essentially of the fiberization product of about 77 to about 80 weight percent silica, about 20 to about 23 weight percent magnesia, greater than 0 to about 0.35 weight percent lithium oxide.

11. The inorganic fiber of claim 1 , consisting essentially of the fiberization product of about 78 to about 80 weight percent silica, about 20 to about 22 weight percent magnesia, greater than 0 to about 0.45 weight percent lithium oxide.

12. The inorganic fiber of claim 11 , consisting essentially of the fiberization product of about 78 to about 80 weight percent silica, about 20 to about 22 weight percent magnesia, greater than 0 to about 0.35 weight percent lithium oxide.

13. An inorganic fiber containing article comprising at least one of bulk fiber, blankets, blocks, boards, caulking compositions, cement compositions, coatings, felts, mats, moldable compositions, modules, papers, pumpable compositions, putty compositions, sheets, tamping mixtures, vacuum cast shapes, vacuum cast forms, or woven textiles, braids, cloths, fabrics, ropes, tapes, sleeving, wicking, said fiber containing article comprising the fiberization product of claim 1 .

Assignments (11)
RELEASE OF FIRST LIEN SECURITY INTEREST IN PATENT COLLATERAL AT REEL/FRAME NO. 47909/0937 Recorded Oct 2, 2024
From: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
To: UNIFRAX I LLC
Reel/Frame 069103/0582 →
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Oct 2, 2024
From: LYDALL PERFORMANCE MATERIALS (US), INC.; LYDALL INC.; REFRACTORY SPECIALTIES, INCORPORATED; SOUTHERN FELT COMPANY, INC.; UNIFRAX I LLC; STELLAR MATERIALS
To: WILMINGTON SAVINGS FUND SOCIETY, FSB, AS COLLATERAL AGENT
Reel/Frame 069091/0735 →
SECOND LIEN TRADEMARK SECURITY AGREEMENT Recorded Oct 2, 2024
From: LYDALL PERFORMANCE MATERIALS (US), INC.; LYDALL INC.; REFRACTORY SPECIALTIES, INCORPORATED; SOUTHERN FELT COMPANY, INC.; UNIFRAX I LLC; STELLAR MATERIALS
To: WILMINGTON TRUST, NATIONAL ASSOCIATION, AS SECOND LIEN NOTES COLLATERAL AGENT
Reel/Frame 069091/0923 →
RELEASE OF SECURITY INTEREST IN PATENT COLLATERAL AT REEL/FRAME NO. 49014/0755 Recorded Oct 4, 2021
From: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
To: UNIFRAX I LLC
Reel/Frame 057710/0669 →
RELEASE OF SECOND LIEN SECURITY INTEREST RECORDED AT REEL 044392, FRAME 0366 Recorded Dec 17, 2018
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: UNIFRAX I LLC
Reel/Frame 047940/0601 →
RELEASE OF SECOND LIEN SECURITY INTEREST RECORDED AT REEL 044393, FRAME 0273 Recorded Dec 17, 2018
From: GOLDMAN SACHS LENDING PARTNERS LLC
To: UNIFRAX I LLC
Reel/Frame 047940/0758 →
FIRST LIEN PATENT SECURITY AGREEMENT Recorded Dec 14, 2018
From: UNIFRAX I LLC
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 047909/0937 →
SECOND LIEN PATENT SECURITY AGREEMENT Recorded Dec 14, 2018
From: UNIFRAX I LLC
To: MORGAN STANLEY SENIOR FUNDING, INC., AS COLLATERAL AGENT
Reel/Frame 049014/0755 →
SECURITY INTEREST Recorded Nov 7, 2017
From: UNIFRAX I LLC
To: GOLDMAN SACHS LENDING PARTNERS LLC, AS COLLATERAL AGENT
Reel/Frame 044393/0273 →
SUPPLEMENTAL PATENT SECURITY AGREEMENT Recorded Nov 7, 2017
From: UNIFRAX I LLC
To: GOLDMAN SACHS LENDING PARTNERS LLC, AS COLLATERAL AGENT
Reel/Frame 044392/0366 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 28, 2017
From: ZHAO, DONGHUI; ZOITOS, BRUCE K.; ANDREJCAK, MICHAEL J.; HAMILTON, JASON M.
To: UNIFRAX I LLC
Reel/Frame 042851/0945 →