Low thermal mass GC module
A system and method for performing field-portable GC/MS measurements for the rapid sampling and measurement of high temperature boiling semi-volatile organic compounds in environmental samples, wherein other column bundles have cold spots that may prevent high temperature boiling semi-volatile components from eluting the GC column, this new design may eliminate those cold spots on the GC column.
1. A heating system for minimizing cold spots in capillary tubing of a column used for performing field-portable Gas Chromatography/Mass Spectrometer (GC/MS) measurements, said heating system comprised of:
an inner cylindrical ring;
a heating wire wound circumferentially around an entire circumference of the inner cylindrical ring;
a middle cylindrical ring disposed around the heating wire and the inner cylindrical ring, wherein the heating wire is in direct contact with and uniformly heats an inner surface of the middle cylindrical ring, wherein the heating wire is enclosed between the inner cylindrical ring and the middle cylindrical ring;
a capillary tubing used as a GC column and disposed circumferentially and in a single layer around and in contact with an outer surface of the middle cylindrical ring, wherein the capillary tubing is disposed directly opposite the heating wire on the inner surface of the middle cylindrical ring; and
an outer cylindrical ring disposed circumferentially around the capillary tubing and the middle cylindrical ring.
2. The system as defined in claim 1 wherein the system is further comprised of a temperature sensor disposed on the inner cylindrical ring to thereby enable temperature readings of the inner cylindrical ring.
3. The system as defined in claim 2 wherein the outer cylindrical ring is less than 10 cm in diameter to enable the heating system to be used in a field-portable GC/MS measurement system.
4. The system as defined in claim 3 wherein the system is further comprised of an electrical source coupled to the heating wire for providing electricity to enable heating of the heating wire.
5. The system as defined in claim 4 wherein the system is further comprised of a field portable GC/MS unit that is coupled to the capillary tubing.
6. The system as defined in claim 1 wherein the capillary tubing contacts the middle cylindrical ring.
7. The system as defined in claim 1 wherein the outer cylindrical ring comprises tabs that are folded around the inner cylindrical ring.
8. The system as defined in claim 7 wherein the tabs are parallel to the inner cylindrical ring.
9. The system as defined in claim 1 wherein the capillary tubing is disposed circumferentially around the outer surface of the middle cylindrical ring.
10. A system for performing sampling and measurement of high temperature boiling semi-volatile organic compounds in a field-portable GC/MS instrument, said system comprised of:
an inner cylindrical ring;
a heating wire uniformly wound circumferentially around an entire circumference of the inner cylindrical ring;
a middle cylindrical ring disposed around the heating wire and the inner cylindrical ring, wherein the heating wire is in direct contact with and uniformly heats an inner surface of the middle cylindrical ring, wherein the heating wire is enclosed between the inner cylindrical ring and the middle cylindrical ring;
a capillary tubing used as a GC column and disposed circumferentially and in a single layer around and in contact with an outer surface of the middle cylindrical ring, wherein the capillary tubing is disposed directly opposite the heating wire on the inner surface of the middle cylindrical ring;
an outer cylindrical ring disposed circumferentially around the capillary tubing and the middle cylindrical ring; and
a field portable GC/MS instrument that is coupled to the capillary tubing for performing sampling and measurement of high temperature boiling semi-volatile organic compounds.
11. The system as defined in claim 10 wherein the system is further comprised of a temperature sensor disposed on the inner cylindrical ring to thereby enable temperature readings of the inner cylindrical ring.
12. The system as defined in claim 11 wherein the outer cylindrical ring is less than 10 cm in diameter to enable the heating system to be used in the field portable GC/MS instrument.
13. The system as defined in claim 12 wherein the system is further comprised of an electrical source coupled to the heating wire for providing electricity to enable heating of the heating wire.
14. The system as defined in claim 10 wherein the capillary tubing contacts the middle cylindrical ring.
15. The system as defined in claim 10 wherein the outer cylindrical ring comprises tabs that are folded around the inner cylindrical ring.
16. The system as defined in claim 15 wherein the tabs are parallel to the inner cylindrical ring.
17. The system as defined in claim 10 wherein the capillary tubing is disposed circumferentially around the outer surface of the middle cylindrical ring.