Distillation Column with Connected Reboiler
A method and device are disclosed for a distillation column. The distillation column comprises a first liquid portion below a first gas portion. The first liquid portion comprises an opening through a side wall comprising a gas backflow preventer. A horizontal reboiler is attached to the opening, the reboiler comprising a second gas portion above a second liquid portion. The recycle gas outlet and the recycle gas inlet are connected by a recycle gas pipe. A descending process liquid stream passes through a recycle gas stream in the first gas portion, forming a bottoms liquid stream, which pools and passes through the opening into the reboiler, and is separated in the reboiler into a product liquid stream, which passes out a liquid outlet, and the recycle gas stream, which is prevented from passing back through the opening by the gas backflow preventer, passing instead through a recycle gas outlet.
1 . A device comprising:
a distillation column comprising a first liquid portion below a first gas portion;
the first gas portion comprising a recycle gas inlet;
the first liquid portion comprising an opening through a side wall comprising a gas backflow preventer;
a horizontal reboiler comprising a second gas portion above a second liquid portion, the horizontal reboiler attached to the opening;
the second gas portion comprising a recycle gas outlet and the second liquid portion comprising a liquid outlet;
the recycle gas outlet and the recycle gas inlet being connected by a recycle gas pipe;
the distillation column, wherein:
a descending process liquid stream passes through a recycle gas stream in the first gas portion, forming a bottoms liquid stream;
the bottoms liquid stream pools in the first liquid portion, passes through the opening into the reboiler, and is separated in the reboiler into a product liquid stream, which passes out the liquid outlet, and the recycle gas stream, which is prevented from passing back through the opening by the gas backflow preventer, passing instead through the recycle gas outlet.
2 . The device of claim 1 , the reboiler comprising a heating element, a liquid outlet, and a gas outlet, the gas outlet extending from a top portion of the reboiler to a side of the distillation column, the liquid outlet being on a bottom portion of the reboiler.
3 . The device of claim 2 , wherein the liquid outlet is situated opposite the opening.
4 . The device of claim 1 , wherein a diameter of a connection between the distillation column and the reboiler are substantially the same as an inner diameter of the reboiler.
5 . The device of claim 1 , further comprising level detection by a differential pressure transmitter, level transmitter, or combinations thereof
6 . The device of claim 1 , wherein the distillation column comprises a plurality of trays above the first gas portion.
7 . The device of claim 6 , wherein the first liquid portion is below all other portions of the distillation column.
8 . The device of claim 1 , wherein the opening comprises a flanged connection, a welded connection, or a threaded connection.
9 . The device of claim 1 , wherein the process liquid stream comprises water, hydrocarbons, organic solvents, ammonia, or combinations thereof.
10 . The device of claim 1 , wherein the distillation column and the horizontal reboiler comprise stainless steel, carbon steel, aluminum, ceramics, plastics, or combinations thereof
11 . A method for operating a distillation column comprising:
providing a distillation column comprising a first liquid portion below a first gas portion, the first gas portion comprising a recycle gas inlet and the first liquid portion comprising an opening through a side wall comprising a gas backflow preventer;
providing a horizontal reboiler comprising a second gas portion above a second liquid portion attached to the opening, the second gas portion comprising a recycle gas outlet, the second liquid portion comprising a liquid outlet, and the recycle gas outlet and the recycle gas inlet being connected by a recycle gas pipe;
passing a descending process liquid stream through a recycle gas stream in the first gas portion, forming a bottoms liquid stream;
pooling the bottoms liquid stream in the first liquid portion;
passing the bottoms liquid stream through the opening into the reboiler;
separating the bottoms liquid stream into a product liquid stream, which passes out the liquid outlet, and the recycle gas stream, which is prevented from passing back through the opening by the gas backflow preventer, passing instead through the recycle gas outlet.
12 . The method of claim 11 , the reboiler comprising a heating element, a liquid outlet, and a gas outlet, the gas outlet extending from a top portion of the reboiler to a side of the distillation column, the liquid outlet being on a bottom portion of the reboiler.
13 . The method of claim 12 , wherein the liquid outlet is situated opposite the opening.
14 . The method of claim 11 , wherein a diameter of a connection between the distillation column and the reboiler are substantially the same as an inner diameter of the reboiler.
15 . The method of claim 11 , further comprising detecting level by a differential pressure transmitter, level transmitter, or combinations thereof
16 . The method of claim 11 , providing the distillation column comprising a plurality of trays above the first gas portion.
17 . The method of claim 16 , wherein the first liquid portion is below all other portions of the distillation column.
18 . The method of claim 11 , wherein the opening comprises a flanged connection, a welded connection, or a threaded connection.
19 . The method of claim 11 , providing the process liquid stream comprising water, hydrocarbons, organic solvents, ammonia, or combinations thereof
20 . The method of claim 11 , wherein the distillation column and the horizontal reboiler comprise stainless steel, carbon steel, aluminum, ceramics, plastics, or combinations thereof.