IP Library Granted Patent US 10,655,023
Granted Patent B2
US 10,655,023 · App. 15/672,553 · Granted May 19, 2020

Electrodeposition system

Inventors: Victoria J Gelling (Medina, MN); Tapan DebRoy (Victoria, MN); Chun Ren (Wilmington, DE)
Assignee: The Sherwin Williams Company
C09D5/448B01J23/18B01J37/0215B01J37/0225B01J37/348C08G18/22C08G18/227C08G18/282C08G18/3206C08G18/58C08G18/584C08G18/7621C08G18/7664C08G18/80C08G18/8029C08G18/8064C08G59/066C08G59/245C08G59/4028C08G59/68C09D5/4453C09D5/4457C09D7/40C09D7/61C09D163/00C09D175/04C25D13/12C08G2150/90C08K3/11C08K3/24C08K2003/0837C08K2003/2227C25D13/20
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Quick Facts
Patent No.
US 10,655,023
App. No.
15/672,553
Granted
May 19, 2020
Kind
B2
Abstract

An electrocoat system for electrodeposition is described. The system includes an inorganic bismuth-containing compound or a mixture of inorganic and organic bismuth-containing compounds. The system demonstrates a high degree of crosslinking and produces a cured coating with optimal crosslinking and corrosion resistance.

Claims (23)

1. A composition for electrodeposition, comprising:

an electrodeposition resin component; optionally, a crosslinking component;

optionally, an acid component; and

at least an inorganic bismuth salt of a metal oxyanion bismuth-containing compound comprising bismuth aluminate.

2. The composition of claim 1 , wherein the at least one inorganic bismuth-containing compound is a compound substantially insoluble in water at a pH of about 4 to 6 and a temperature of about 37° C.

3. The composition of claim 1 , wherein the composition includes a combination of the at least one inorganic bismuth-containing compound and an organic bismuth-containing compound comprising bismuth citrate.

4. The composition of claim 1 , further comprising:

about 40 to 95 percent by weight of the electrodeposition resin component based on the total weight of resin solids in the composition;

about 10 to 60 percent by weight of the blocked polyisocyanate component based on the total weight of resin solids in the composition;

and

about 0.5 to 10 percent by weight of the at least one inorganic bismuth-containing compound based on the total weight of resin solids in the composition.

5. A method of making a coated article by electrodeposition of a film of the composition of claim 1 .

6. The method of claim 5 , wherein the film has an average thickness of 10 to 25 pm.

7. A cationic electrodeposition bath comprising the composition of claim 1 .

8. The composition of claim 1 , wherein a coating formed from the composition is corrosion resistant.

9. The composition of claim 1 , wherein a coating formed from the composition demonstrates less than 3 mm creep from scribe according to ASTM D1654-08, wherein the coating is applied to a pretreated cold-rolled steel substrate.

10. The composition of claim 1 , wherein a coating formed from the composition demonstrates solvent resistance of at least 30 double rubs according to ASTM D5402-15.

11. A method, comprising:

combining an electrodeposition resin component including at least one crosslinkable functional group with a blocked isocyanate component;

an aliphatic carboxylic acid component; and

at least an inorganic bismuth salt of a metal oxyanion bismuth-containing compound comprising bismuth aluminate.

12. A method for electrodeposition, comprising:

providing an emulsion including a cationizable electrodeposition resin component and a blocked polyisocyanate crosslinker component; providing a pigment paste including a dispersion resin, pigment, and an inorganic bismuth salt of a metal oxyanion bismuth-containing compound comprising bismuth aluminate.

Assignments (8)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 6, 2023
From: THE SHERWIN-WILLIAMS HEADQUARTERS COMPANY
To: SWIMC LLC
Reel/Frame 063275/0494 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 11, 2022
From: THE SHERWIN-WILLIAMS COMPANY
To: THE SHERWIN-WILLIAMS HEADQUARTERS COMPANY
Reel/Frame 060366/0979 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 30, 2021
From: THE VALSPAR CORPORATION
To: THE SHERWIN-WILLIAMS COMPANY
Reel/Frame 057204/0946 →
MERGER Recorded Oct 29, 2020
From: ENGINEERED POLYMER SOLUTIONS, INC.
To: THE VALSPAR CORPORATION
Reel/Frame 054443/0772 →
MERGER Recorded Sep 2, 2020
From: VALSPAR SOURCING, INC.
To: ENGINEERED POLYMER SOLUTIONS, INC.
Reel/Frame 053826/0606 →
NUNC PRO TUNC ASSIGNMENT Recorded Mar 24, 2020
From: THE SHERWIN-WILLIAMS COMPANY
To: VALSPAR SOURCING, INC.
Reel/Frame 052217/0640 →
CORRECTIVE ASSIGNMENT TO CORRECT THE INCORRECT PATENT NO. 8465946 PREVIOUSLY RECORDED AT REEL: 045281 FRAME: 0529. ASSIGNOR(S) HEREBY CONFIRMS THE MERGER. Recorded May 4, 2018
From: VALSPAR SOURCING, INC.
To: THE SHERWIN-WILLIAMS COMPANY
Reel/Frame 046087/0150 →
MERGER Recorded Feb 8, 2018
From: VALSPAR SOURCING. INC
To: THE SHERWIN-WILLIAMS COMPANY
Reel/Frame 045281/0529 →
Continuity (3)
Continuation PCTUS2016017323 · Feb 10, 2016
Provisional Application 62114228 · Feb 10, 2015
Related Publication 20170335120A1 · Nov 23, 2017