Method of purifying carbon nanotubes
View Patent ↗Disclosed is a method of purifying carbon nanotubes, including treating carbon nanotubes with an inert gas at a high temperature in a low vacuum in a reactor and obtaining ultrapure carbon nanotubes, wherein the ultrapure carbon nanotubes contain 50 ppm or less of each metal remaining therein.
1. A method of purifying carbon nanotubes, comprising:
(1) treating carbon nanotubes with an inert gas at a treatment temperature of 1800° C. or less in a low vacuum at a reaction pressure of 0.1 Torr or more in a reactor; and
(2) obtaining ultrapure carbon nanotubes,
wherein the ultrapure carbon nanotubes contain 50 ppm or less of each metal remaining therein.
2. The method of claim 1 , wherein Fe is present in an amount of 10 ppm or less, when the metal remaining in the ultrapure carbon nanotubes is Fe.
3. The method of claim 1 , wherein the low vacuum is set at a reaction pressure ranging from 0.1 Torr to 1 Torr.
4. The method of claim 1 , wherein the treatment temperature ranges from 1600° C. to 1800° C.
5. The method of claim 1 , wherein the inert gas is used in an amount of 0.0025 to 0.25 times a volume of the reactor per minute.
6. The method of claim 1 , wherein the treating the carbon nanotubes is performed for 15 min to 120 min.
7. The method of claim 1 , wherein the remaining metal includes Fe, Co, Al 2 O 3 , Mg or a combination thereof.