IP Library Granted Patent US 10,336,767
Granted Patent B2
US 10,336,767 · App. 15/694,252 · Granted Jul 2, 2019

Crystalline forms of therapeutic compounds and uses thereof

Inventors: Minh Ngoc Nguyen (Dorchester, MA); Winston Zapanta Ong (Stoneham, MA)
Assignee: Kala Pharmaceuticals, Inc.
C07D491/107C07B2200/13
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Quick Facts
Patent No.
US 10,336,767
App. No.
15/694,252
Granted
Jul 2, 2019
Kind
B2
Abstract

Described herein are crystalline forms of Compound 1 useful for the prevention and treatment of angiogenic ocular conditions; methods of treating a disease comprising; processes for preparing; and kits comprising, the same.

Claims (11)

1. A crystalline form of Compound 1:

wherein the crystalline form has an X-ray powder diffraction (XRPD) pattern comprising peaks at about 8-9 degrees 2θ, about 10.5-11.5 degrees 2θ, and about 18-19 degrees 2θ.

2. The compound of claim 1 wherein the crystalline form is an anhydrate.

3. A process for preparing a crystalline form of claim 1 , comprising:

mixing amorphous Compound 1 and ethyl acetate; and

recovering crystalline form C.

4. A pharmaceutical composition comprising the crystalline form of claim 1 and a pharmaceutically acceptable carrier.

5. The pharmaceutical composition of claim 4 , wherein the pharmaceutical composition is suitable for topical administration.

6. The pharmaceutical composition of claim 4 , wherein the pharmaceutical composition is suitable for injection.

7. The pharmaceutical composition of claim 4 , wherein the pharmaceutical composition is suitable for delivery to the eye.

8. A kit comprising the pharmaceutical composition of claim 4 .

Assignments (6)
CHANGE OF NAME Recorded Sep 21, 2023
From: KALA PHARMACEUTICALS, INC.
To: KALA BIO, INC.
Reel/Frame 065017/0488 →
FIRST AMENDMENT TO IP SECURITY AGREEMENT Recorded Dec 22, 2022
From: KALA PHARMACEUTICALS, INC.
To: OXFORD FINANCE LLC
Reel/Frame 062205/0883 →
SECURITY INTEREST Recorded May 6, 2021
From: KALA PHARMACEUTICALS, INC.
To: OXFORD FINANCE LLC
Reel/Frame 056168/0602 →
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS AT REEL AND FRAME: 047602 / 0480 & 047172 / 0481 Recorded May 5, 2021
From: ATHYRIUM OPPORTUNITIES III ACQUISITION LP
To: KALA PHARMACEUTICALS, INC
Reel/Frame 056151/0092 →
SECURITY INTEREST Recorded Oct 1, 2018
From: KALA PHARMACEUTICALS, INC.
To: ATHYRIUM OPPORTUNITIES III ACQUISITION LP
Reel/Frame 047172/0481 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 1, 2017
From: NGUYEN, MINH NGOC; ONG, WINSTON ZAPANTA
To: KALA PHARMACEUTICALS, INC.
Reel/Frame 043473/0537 →
Continuity (2)
Provisional Application 62385148 · Sep 8, 2016
Related Publication 20180065977A1 · Mar 8, 2018