IP Library Granted Patent US 10,808,197
Granted Patent B2
US 10,808,197 · App. 15/703,388 · Granted Oct 20, 2020

Alkylated alkoxydiarylamine antioxidants

Inventor: Robert G. Rowland (Woodbridge, CT)
Assignee: LANXESS Solutions US Inc.
C10M133/54C07C217/92C10M105/00C10M133/12C10M133/14C10M169/04C10M2203/003C10M2215/062C10M2215/064C10M2215/065C10M2215/26C10N2030/04C10N2030/10C10N2040/04C10N2040/08C10N2040/20C10N2040/25
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Quick Facts
Patent No.
US 10,808,197
App. No.
15/703,388
Granted
Oct 20, 2020
Kind
B2
Abstract

Alkylated diaryl amines further substituted by an alkoxy group on one or more aryl carbon atoms exhibit excellent antioxidant activity in lubricant compositions.

Claims (28)

1. A lubricating oil composition comprising

a) a lubricating oil, and

b) one or more alkylated alkoxydiarylamine of formula III:

wherein x is 0, 1 or 2 and y is 1, 2 or 3;

R′ is C 1-12 alkyl or C 1-12 alkyl substituted by one or more hydroxyl or alkoxy;

each R is independently C 4-24 alkyl, C 7-18 aralkyl, or C 4-24 alkyl substituted by one or more hydroxyl and/or interrupted by one or more oxygen atom;

wherein the total number of carbon atoms of the combined groups R is 12 or higher, and wherein at least one carbon atom adjacent to the amine nitrogen is unsubstituted.

2. The lubricating oil composition according to claim 1 wherein b) is present in an amount of about 0.1 to about 5.0 wt%, based on the weight of the lubricating oil composition.

3. The lubricating oil composition according to claim 1 wherein b) is present in an amount of greater than 5 wt%, up to about 50 wt%, based on the weight of the lubricating oil composition.

4. The lubricating oil composition according to claim 1 further comprising one or more alkylated diarylamine not substituted by an alkoxy group.

5. The lubricating oil composition according to claim 1 wherein in the alkylated alkoxydiarylamine of the formula III x is 0 or 1 and y is 1.

6. The lubricating oil composition according to claim 1 wherein the alkoxy group of the alkoxydiarylamine is at the 3-position relative to the nitrogen according to formula V:

7. The lubricating oil composition according to claim 1 wherein the total number of carbon atoms of the combined groups R is 16 or higher.

8. The lubricating oil composition according to claim 6 wherein in the alkylated alkoxydiarylamine of the formula V x is 0 or 1 and y is 1.

9. The lubricating oil composition according to claim 6 wherein in the alkylated alkoxydiarylamine of the formula V x is 1 and y is 1.

10. The lubricating oil composition according to claim 1 , wherein the alkoxy group R′O is on the phenyl ring at the 2- or 3-position relative to the nitrogen atom.

11. The lubricating oil composition according to claim 1 , wherein x is 1 and y is 1.

12. The lubricating oil composition according to claim 1 , wherein both aryl groups in the formula III are alkylated.

13. The lubricating oil composition according to claim 1 wherein x is 0, y is 1, R′ is methyl or ethyl, and R is selected from dodecyl, octadecyl, and icosane.

14. The lubricating oil composition according to claim 1 wherein x is 1, y is 1, R′ is methyl or ethyl, and R is selected from hexyl, octyl, nonyl, decyl, and dodecyl.

15. The lubricating oil composition according to claim 1 wherein x is 1, y is 1, R′ is methyl or ethyl, and one R is n-butyl, sec-butyl, tert-butyl or hexyl and the other R is t-octyl, nonyl, dodecyl, hexadecyl or octadecyl.

16. The lubricating oil composition according to claim 1 wherein x is 1, y is 1, R′ is butyl or hexyl, and R is selected from n-butyl, sec-butyl, iso-amyl, hexyl, octyl, nonyl, and dodecyl.

17. The lubricating oil composition according to claim 1 , wherein the lubricating oil comprises one or more hydrocarbon base stocks.

18. The lubricating oil composition according to claim 1 wherein x is 0 or 1 and y is 1 or 2.

19. The lubricating oil composition according to claim 1 wherein R′ is C 1-12 alkyl.

20. The lubricating oil composition according to claim 1 wherein each R is independently C 4-24 alkyl.

21. The lubricating oil composition according to claim 20 wherein R′ is C 1-6 .

22. The lubricating oil composition according to claim 21 wherein x is 0 or 1 and y is 1 or 2.

Assignments (3)
MERGER Recorded May 5, 2022
From: LANXESS SOLUTIONS US INC.
To: LANXESS CORPORATION
Reel/Frame 059856/0075 →
MERGER AND CHANGE OF NAME Recorded Sep 7, 2018
From: CHEMTURA CORPORATION; LANXESS SOLUTIONS US INC.
To: LANXESS SOLUTIONS US INC.
Reel/Frame 046809/0667 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Oct 11, 2017
From: ROWLAND, ROBERT G.
To: LANXESS SOLUTIONS US INC.
Reel/Frame 043833/0687 →
Continuity (3)
Provisional Application 62396885 · Sep 20, 2016
Provisional Application 62463834 · Feb 27, 2017
Related Publication 20180079984A1 · Mar 22, 2018