IP Library Granted Patent US 10,239,783
Granted Patent B2
US 10,239,783 · App. 15/730,448 · Granted Mar 26, 2019

Method of producing glass substrate and glass substrate

Inventors: Hiroshi Hanekawa (Tokyo, JP); Nobutaka Aomine (Tokyo, JP); Yuki Aoshima (Tokyo, JP); Hirotomo Kawahara (Tokyo, JP); Kazunobu Maeshige (Tokyo, JP)
Assignee: AGC INC.
C03C17/245C03C17/3411C03C17/36C03C17/366C23C16/40G02B1/11G02B5/08G02B5/208C03C2217/73C03C2218/152C03C2218/153
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,239,783
App. No.
15/730,448
Granted
Mar 26, 2019
Kind
B2
Abstract

A method of producing a glass substrate having a first layer formed on a surface of the substrate by low-temperature CVD includes preparing the glass substrate and forming the first layer on the glass substrate by the low-temperature CVD. In the glass substrate after forming the first layer, an integrated value after a baseline correction in a wavenumber range of 2600 cm −1 to 3800 cm −1 in a peak due to OH groups obtained by an FTIR measurement on the first layer is 9.0 or less, and the C content of the first layer is 1.64 at % or less.

Claims (16)

1. A method of producing a glass substrate having a first layer formed on a surface of the substrate by low-temperature CVD, the method comprising:

preparing the glass substrate; and

forming the first layer on the glass substrate by the low-temperature CVD,

wherein the first layer is formed on a surface of the glass substrate at a plasma power of 20 kW/m or higher, and

wherein, in the glass substrate after said forming the first layer, an integrated value after a baseline correction in a wavenumber range of 2600 cm −1 to 3800 cm −1 in a peak due to OH groups obtained by an FTIR measurement on the first layer is 9.0 or less, and a C content of the first layer is 1.64 at % or less.

2. The method as claimed in claim 1 , wherein said forming the first layer includes supplying the glass substrate with an organic metal precursor.

3. The method as claimed in claim 2 , wherein the organic metal precursor includes at least one component selected from the group consisting of Si, Ti, Zn, Sn and Al.

4. The method as claimed in claim 2 , wherein the organic metal precursor includes at least one component selected from the group consisting of a —CH 3 group, a —OH group and a —H group.

5. The method as claimed in claim 1 , wherein the first layer is at least one of oxide, nitride, and oxynitride.

6. The method as claimed in claim 1 , wherein said forming the first layer is performed at a deposition rate in a range of 50 nm·m/min to 400 nm·m/min.

7. The method as claimed in claim 1 , wherein the low-temperature CVD is PECVD.

8. The method as claimed in claim 1 , further comprising: forming a second layer over the glass substrate by a method other than the low-temperature CVD.

9. The method as claimed in claim 8 , wherein said forming the second layer is performed before or after said forming the first layer.

10. The method as claimed in claim 8 , further comprising: forming a third layer over the glass substrate by the low-temperature CVD after said forming the first layer.

11. The method as claimed in claim 10 , wherein, in the glass substrate after said forming the third layer, an integrated value after the baseline correction in the wavenumber range of 2600 cm −1 to 3800 cm −1 in a peak due to OH groups obtained by an FTIR measurement on the first through third layers is 9.0 or less.

12. The method as claimed in claim 8 , wherein the method other than the low-temperature CVD is sputtering or thermal CVD.

Assignments (1)
CHANGE OF NAME Recorded Aug 7, 2018
From: ASAHI GLASS COMPANY, LIMITED
To: AGC INC.
Reel/Frame 046730/0786 →
Priority Claims (1)
JP 2012-118997 · May 24, 2012 · national
Continuity (3)
Division 14552053 · Nov 24, 2014
Continuation PCTJP2013064087 · May 21, 2013
Related Publication 20180044229A1 · Feb 15, 2018