Method for producing a conversion element
A method for producing a conversion element is disclosed. In an embodiment, the method includes providing an acidic medium having a pH value of less than 2, adding a conversion material into the acidic medium thereby forming a mixture and adding a silicate solution having a viscosity between 2 to 10 000 poize inclusive to the mixture such that the pH value during the addition of the silicate solution is smaller than 2. The method further includes obtaining a precipitate which contains the conversion material and silicon dioxide as a matrix material, separating the precipitate, washing the precipitate with a washing medium, wherein the washing medium has a pH value of less than 2; and hardening the precipitate thereby forming the conversion element.
1. A method for producing a conversion element for an optoelectronic component, the method comprising:
providing an acidic medium having a pH value of less than 2;
adding a conversion material into the acidic medium thereby forming a mixture;
adding a silicate solution having a viscosity between 2 and 10 000 poise inclusive to the mixture such that the pH value during the addition of the silicate solution is smaller than 2;
obtaining a precipitate which contains the conversion material and silicon dioxide as a matrix material;
separating the precipitate;
washing the precipitate with a washing medium, wherein the washing medium has a pH value of less than 2; and
hardening the precipitate thereby forming the conversion element.
2. The method according to claim 1 , further comprising:
converting the precipitate into a mold before hardening the precipitate; and
curing during hardening by a gas flow under pressure.
3. The method according to claim 2 , wherein the mold comprises a screen.
4. The method according to claim 1 , wherein the conversion material is selected from the group consisting of (Y,Lu,Gd,Tb) 3 (Al 1-x Ga x ) 5 O 12 , (Ba,Sr,Ca)Si 2 O 2 N 2 , (Ba,Sr,Ca) 2 SiO 4 , (Ba,Sr,Ca) 2 Si 5 N 8 , (Sr,Ca)AlSiN 3 Si 2 N 2 O, (Sr,Ca)AlSiN 3 and Ca 8 Mg(SiO 4 ) 4 Cl 2 .
5. The method according to claim 1 , wherein adding the conversion material comprises homogeneously dispersing the conversion material.
6. The method according to claim 1 , wherein the conversion material has a proportion of 50% by weight to 60% by weight, inclusive, in the matrix material.
7. The method according to claim 1 , further comprising applying the conversion element to an optoelectronic semiconductor chip after forming the conversion element.
8. The method according to claim 1 , further comprising applying the washed precipitate to an optoelectronic semiconductor chip by spray coating after washing the precipitate and before hardening the precipitate.
9. The method according to claim 1 , wherein adding the conversion material further comprises dispersing scattering particles.
10. The method according to claim 1 , wherein the acidic medium is selected from a group consisting of hydrochloric acid, phosphoric acid, nitric acid, sulphuric acid, chlorosulfonic acid, sulphuryl chloride, perchloric acid and combinations thereof.
11. The method according to claim 1 , wherein the acidic medium is present in concentrated or dilute form.
12. The method according to claim 1 , further comprising adding an indicator of a peroxide, which indicates a completeness of the precipitation of the precipitate by color change.
13. The method according to claim 1 , further comprising grinding the conversion element after hardening the conversion element.
14. The method according to claim 1 , wherein adding a silicate solution comprises a solution of a sodium water glass, potassium water glass or lithium water glass.