IP Library Granted Patent US 10,731,242
Granted Patent B2
US 10,731,242 · App. 15/754,068 · Granted Aug 4, 2020

Nitrided steel part and method of production of same

Inventors: Takahide Umehara (Tokyo, JP); Masato Yuya (Tokyo, JP); Yoshihiro Daito (Tokyo, JP)
Assignee: NIPPON STEEL CORPORATION
C23C8/26C21D9/00C21D9/32C22C38/00C22C38/001C22C38/02C22C38/06C22C38/42C22C38/44C22C38/46C22C38/50C22C38/58C22C38/60
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,731,242
App. No.
15/754,068
Granted
Aug 4, 2020
Kind
B2
Abstract

A nitrided steel part excellent in pitting resistance and bending fatigue characteristic enabling reduction of size and decrease of weight of parts or enabling demand for high load capacities to be met, using as a material a steel material containing, by mass %, C: 0.05 to 0.25%, Si: 0.05 to 1.5%, Mn: 0.2 to 2.5%, P: 0.025% or less, S: 0.003 to 0.05%, Cr: over 0.5 to 2.0%, Al: 0.01 to 0.05%, and N: 0.003 to 0.025%, having a balance of Fe and impurities, having formed on the steel surface a compound larger of a thickness 3 μm or less containing iron, nitrogen, and carbon and a hardened layer formed below the compound layer, and having an effective hardened layer depth of 160 to 410 μm.

Claims (47)

1. A nitrided steel part comprising a steel material as a material, the steel material consisting of, by mass %,

C: 0.05 to 0.25%,

Si: 0.05 to 1.5%,

Mn: 0.2 to 2.5%,

P: 0.025% or less,

S: 0.003 to 0.05%,

Cr: over 0.5 to 2.0%,

Al: 0.01 to 0.05%,

N: 0.003 to 0.025%,

optionally one or more of

Mo: 0.01 to less than 0.50%,

V: 0.01 to less than 0.50%,

Cu: 0.01 to less than 0.50%,

Ni: 0.01 to less than 0.50%, and

Ti: 0.005 to less than 0.05%, and

a balance of Fe and impurities,

the nitrided steel part comprising a compound layer of a thickness of 3 μm or less containing iron, nitrogen, and carbon formed on the steel surface and a hardened layer formed under the compound layer,

an effective hardened layer depth of the nitrided steel part being 160 to 410 μm,

wherein the effective hardened layer depth (μm) is defined as the depth in a range where the Vickers hardness in the distribution measured in the depth direction from the surface of the test material using the hardness distribution in the depth direction obtained by the above Vickers hardness test is 300 HV or more.

2. The nitrided part of claim 1 wherein a ratio of voids in an area of 25 μm 2 in a range of 5 μm depth from an outermost surface of said steel material is less than 10%.

3. A method of production of a nitrided steel part comprising a steel material as a material, the steel material consisting of, by mass %,

C: 0.05 to 0.25%,

Si: 0.05 to 1.5%,

Mn: 0.2 to 2.5%,

P: 0.025% or less,

S: 0.003 to 0.05%,

Cr: over 0.5 to 2.0%,

Al: 0.01 to 0.05%,

N: 0.003 to 0.025%,

optionally one or more of

Mo: 0.01 to less than 0.50%,

V: 0.01 to less than 0.50%,

Cu: 0.01 to less than 0.50%,

Ni: 0.01 to less than 0.50%, and

Ti: 0.005 to less than 0.05%, and

a balance of Fe and impurities,

the method comprising providing a step of gas nitriding by heating the steel material in a gas atmosphere containing NH 3 , H 2 , and N 2 to 550 to 620° C., and making the overall treatment time A 1.5 to 10 hours,

the gas nitriding comprising high K N value treatment having a treatment time of X hours and a low K N value treatment after the high K N value treatment having a treatment time of Y hours,

the high K N value treatment having a nitriding potential K NX determined by formula (1) of 0.15 to 1.50 and having an average value K NXave of the nitriding potential K NX determined by formula (2) of 0.30 to 0.80,

the low K N value treatment having a nitriding potential K NY determined by formula (3) of 0.02 to 0.25, having an average value K NYave of the nitriding potential K NY determined by formula (4) of 0.03 to 0.20, and having an average value K Nave of the nitriding potential determined by formula (5) of 0.07 to 0.30:

K NX =(NH 3 partial pressure) X /[(H 2 partial pressure) 3/2 ] X   (1)

K NXave =Σ i=1 n ( X 0 ×K NXi )/ X   (2)

K NY =(NH 3 partial pressure) Y /[(H 2 partial pressure) 3/2 ] Y   (3)

K NYave =Σ i=1 n ( Y 0 ×K NYi )/ Y   (4)

K Nave =( X×K NXave +Y×K NYave )/ A   (5)

wherein, in formula (2) and formula (4), the subscript “i” is a number indicating the number of measurements for each constant time interval, X 0 indicates the measurement interval (hours) of the nitriding potential K NX , Y 0 indicates the measurement interval (hours) of the nitriding potential K NY , K NXi indicates the nitriding potential at the i-th measurement during the high K N value treatment, and K NYi indicates the nitriding potential at the i-th measurement during the low K N value treatment.

4. The method of production of the nitrided steel part of claim 3 wherein the gas atmosphere includes a total of 99.5 vol % of NH 3 , H 2 , and N 2 .

Assignments (2)
CHANGE OF NAME Recorded May 14, 2019
From: NIPPON STEEL & SUMITOMO METAL CORPORATION
To: NIPPON STEEL CORPORATION
Reel/Frame 049257/0828 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 21, 2018
From: UMEHARA, TAKAHIDE; YUYA, MASATO; DAITO, YOSHIHIRO
To: NIPPON STEEL & SUMITOMO METAL CORPORATION
Reel/Frame 044990/0103 →
Priority Claims (1)
JP 2015-176475 · Sep 8, 2015 · national
Continuity (1)
Related Publication 20180245195A1 · Aug 30, 2018