IP Library Granted Patent US 10,370,468
Granted Patent B2
US 10,370,468 · App. 15/761,641 · Granted Aug 6, 2019

Saponified ethylene-vinyl ester-based copolymer pellet and producing method therefor

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Quick Facts
Patent No.
US 10,370,468
App. No.
15/761,641
Granted
Aug 6, 2019
Kind
B2
Abstract

Provided is EVOH resin pellet capable of suppressing the occurrence of fish eye even in a resultant monolayer film, and the method for producing the same. The EVOH resin pellet contains a boron compound and the boron amount in a surface portion of the pellet is 1.7 ppm or less. After the EVOH resin pellet is made to contain the boron compound, the EVOH resin pellet is rinsed with a mixture of water and alcohol so that the amount of the boron compound in a surface portion can be reduced.

Claims (9)

1. A pellet, comprising: a saponified ethylene-vinyl ester-based copolymer pellet; and a boron compound; wherein a surface portion of the pellet contains 1.7 ppm or less of boron; wherein a total amount of boron in the pellet is 10 to 1000 ppm.

2. The pellet according to claim 1 , wherein a weight ratio of the boron contained in the surface portion of the pellet to a total amount of boron in the pellet is 1.38×10 −2 or less.

3. The pellet according to claim 1 , further comprising water in an amount of 0.01 to 1 wt % based on a total weight of the pellet.

4. A plurality of pellets, comprising at least one pellet according to claim 1 .

5. A plurality of saponified ethylene-vinyl ester-based copolymer pellets, comprising at least one pellet according to claim 1 .

6. A method for producing the pellet according to claim 1 , comprising:

contacting a pellet comprising a saponified ethylene-vinyl ester-based copolymer and a boron compound with a mixture of water and alcohol having a ratio of water to alcohol of 80/20 to 0/100, until an amount of the boron compound in a surface portion of the pellet is 1.7 ppm or less.

7. The method according to claim 6 , further comprising drying the pellet after contacting it with the mixture of water and alcohol;

wherein the pellet is a porous pellet.

Assignments (2)
MERGER Recorded May 2, 2019
From: THE NIPPON SYNTHETIC CHEMICAL INDUSTRY CO., LTD.
To: MITSUBISHI CHEMICAL CORPORATION
Reel/Frame 049110/0285 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 20, 2018
From: HORI, SHINICHI; YAMAMOTO, NOBUYUKI; NAKAJIMA, TAKUYA
To: THE NIPPON SYNTHETIC CHEMICAL INDUSTRY CO., LTD.
Reel/Frame 045289/0701 →