Process for preparing fat continuous emulsions
A process for preparing a water-in-oil emulsion which emulsion comprises oil and a hardstock fraction next to an aqueous phase. The process involves blending the melted hardstock fraction with a water-continuous dispersion comprising part or all of the oil and part or all of the aqueous phase and with a fat-continuous dispersion comprising the remainder of the oil and the remainder of the aqueous phase. The combined stream is mixed by a high shear mixer with short residence time.
1. A process for preparing a fat-continuous emulsion, which emulsion comprises 15-83% of an aqueous phase and 17-85% of a fat phase, said fat phase comprising 10-100% hardstock fat (weight % on total fat phase), and 0-90% oil (weight % on total fat phase), which process comprises the steps of:
a) providing a water-continuous dispersion at a temperature of between 0° C. and 15° C. comprising part of the aqueous phase as the continuous phase with dispersed therein part of the oil;
b) providing part of hardstock fat in melted form and at a temperature of between 30° C. and 60° C.;
c) providing a fat-continuous dispersion which comprises the remainder of the aqueous phase, the remainder of the oil, and the remainder of the hardstock, which dispersion comprises fat crystals in an amount of from 0.2 to 10% by weight, based on the total dispersion provided by this step c);
d) combining the water-continuous dispersion of step a) with the melted hardstock fat of step b) and the fat-continuous dispersion of step c), wherein the weight ratio of water-continuous dispersion+melted hardstock:fat-continuous dispersion is from 100:1 to 5:1; and
e) subjecting the mixture obtained after step d) to a high shear device to provide a fat-continuous emulsion;
wherein the temperature of the mixture obtained from step d) is below the melting point of the hardstock fat;
wherein the dispersion in step c) comprises a rework stream of the product produced by step e), and wherein the high shear device is a high shear mixing process in a high shear mixer having a rotor and a stator, which mixer has a residence time of less than 3 seconds, and sufficient shear to effect emulsification of water droplets in oil having a droplet size D3.3 of less than 15 micrometers; and
wherein the high shear device results in a temperature increase of the emulsion of less than 5° C., when comparing temperature of the aqueous dispersion at the inlet and the temperature of the emulsion at the outlet of the high shear device.
2. The process according to claim 1 , wherein the water-continuous dispersion of step a) is obtained by mixing continuously in-line an aqueous phase at a temperature of from 0 to 15° C. with oil at a temperature of from 0 to 25° C.
3. The process according to claim 1 , wherein the dispersion of step a) is obtained by providing a stirred tank comprising oil dispersed in the aqueous phase, which stirred tank is held at a temperature of from 0 to 15° C. for at least 30 minutes.
4. The process according to claim 1 , wherein the fat-continuous dispersion in step c) is at a temperature of between 20 and 50° C. prior to combining with the dispersion of step a) and the hardstock of step b) in step d).
5. The process according to claim 1 , wherein the temperature of the water-continuous dispersion in step a) is between 0 and 10° C.
6. The process according to claim 1 , wherein the temperature of the melted hardstock in step b) is between 30 and 45° C.
7. The process according to claim 1 , wherein the water-continuous dispersion of step a) is combined in step d) with the melted hardstock fat of step b) and the fat-continuous dispersion of step c), in a weight ratio of water-continuous dispersion+melted hardstock:fat-continuous dispersion is from 40:1 to 10:1.
8. The process according to claim 1 , wherein step e) is carried out in a continuous process.
9. The process according to claim 1 , wherein subjecting the mixture in step e) to a high shear device is followed by subjecting the mixture to a pin stirrer.
10. The process according to claim 1 , wherein the fat continuous emulsion is a spreadable emulsion.
11. The process according to claim 1 , wherein the emulsion comprises 40-80% fat.
12. The process according to claim 1 , wherein the overall composition of the fat-continuous dispersion of step c) is the same as the overall composition of the fat-continuous emulsion produced by step e).
13. The process according to claim 1 , wherein the dispersion in step c) comprises fat crystals in an amount of from 0.4 to 7% by weight, based on the total dispersion provided by step c).
14. The process according to claim 1 , wherein the dispersion in step c) comprises fat crystals in an amount of from 0.5 to 5% by weight, based on the total dispersion provided by step c).
15. A process for preparing a fat-continuous emulsion, which emulsion comprises 15-83% of an aqueous phase and 17-85% of a fat phase, said fat phase comprising 10-100% hardstock fat (weight % on total fat phase), and 0-90% oil (weight % on total fat phase), which process comprises the steps of:
a) providing a water-continuous dispersion at a temperature of between 0° C. and 15° C. comprising part of the aqueous phase as the continuous phase with dispersed therein part of the oil;
b) providing part of hardstock fat in melted form and at a temperature of between 30° C. and 60° C.;
c) providing a fat-continuous dispersion which comprises the remainder of the aqueous phase, the remainder of the oil, and the remainder of the hardstock, which dispersion comprises fat crystals in an amount of from 0.2 to 10% by weight, based on the total dispersion provided by this step c);
d) combining the water-continuous dispersion of step a) with the melted hardstock fat of step b) and the fat-continuous dispersion of step c), wherein the weight ratio of water-continuous dispersion+melted hardstock:fat-continuous dispersion is from 100:1 to 5:1; and
e) subjecting the mixture obtained after step d) to a high shear device to provide a fat-continuous emulsion;
wherein the temperature of the mixture obtained from step d) is below the melting point of the hardstock fat;
wherein the dispersion in step c) comprises a rework stream of the product produced by step e), and wherein the high shear device is a high shear mixing process in a high shear mixer having a rotor and a stator, which mixer has a residence time of less than 3 seconds, and sufficient shear to effect emulsification of water droplets in oil having a droplet size D3.3 of less than 15 micrometers; and
wherein the fat-continuous dispersion of step c) comprises at least a portion of the fat-continuous spread produced in step e).