IP Library Granted Patent US 10,167,536
Granted Patent B2
US 10,167,536 · App. 15/784,416 · Granted Jan 1, 2019

Tungsten alloy, tungsten alloy part, discharge lamp, transmitting tube, and magnetron

Inventors: Shinichi Yamamoto (Fujisawa, JP); Kayo Nakano (Yokohama, JP); Hiromichi Horie (Yokosuka, JP); Takashi Sano (Fujisawa, JP); Yoshiko Minami (Machida, JP); Satoshi Yamaguchi (Hachioji, JP)
Assignees: Kabushiki Kaisha Toshiba; Toshiba Materials Co., Ltd.
C22C27/04B22F3/1007C22C1/045C22C43/00C22F1/18H01J23/05
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Quick Facts
Patent No.
US 10,167,536
App. No.
15/784,416
Granted
Jan 1, 2019
Kind
B2
Abstract

According to one embodiment, a tungsten alloy includes a W component and a Hf component including HfC. A content of the Hf component in terms of HfC is 0.1 wt % or more and 3 wt % or less.

Claims (13)

1. A method for producing a tungsten alloy for a discharge lamp, a transmitting tube or a magnetron, the method comprising:

mixing a HfC powder comprising primary particles having an average particle diameter of 15 μm or less and a tungsten powder having an average particle diameter of 0.5 to 10 μm to obtain a raw powder;

molding the raw powder to obtain a molded body;

sintering the molded body to obtain a sintered body; and

performing at least one process selected from the group consisting of forging, rolling, wiredrawing, cutting, and polishing, after the sintering step;

wherein a processing ratio [(A−B)/A]×100 of the at least one process is within a range of 30 to 90%, wherein A is a sectional area of the sintered body before the at least one process and B is a sectional area of the sintered body after the at least one process.

2. The method according to claim 1 , wherein a content of the HfC powder in the raw powder is 0.1 to 3 wt %.

3. The method according to claim 1 , wherein the raw powder comprises 0.01 wt % or less of a dope material which is at least one element selected from the group consisting of K, Si, and Al.

4. The method according to claim 1 , wherein an average particle diameter of the HfC powder is equal to or smaller than the average particle diameter of the tungsten powder.

5. The method according to claim 1 , wherein the sintering is performed at a temperature of 1400 to 3000° C. for 1 to 20 hours.

6. The method according to claim 1 , wherein the sintering comprises presintering of the molded body at a temperature of 1250 to 1500° C. to obtain a presintered body and electric sintering of the presintered body at a temperature of 2100 to 2500° C.

7. The method according to claim 1 , further comprising performing a stress relief heat treatment at a temperature of 1300 to 2500° C. after the at least one process.

8. The method according to claim 1 , wherein the average particle diameter of the HfC powder is less than the average particle diameter of the tungsten powder.

Assignments (3)
NUNC PRO TUNC ASSIGNMENT Recorded Feb 19, 2026
From: KABUSHIKI KAISHA TOSHIBA
To: TOSHIBA MATERIALS CO. LTD.
Reel/Frame 074940/0511 →
CHANGE OF NAME Recorded Feb 19, 2026
From: TOSHIBA MATERIALS CO. LTD.
To: NITERRA MATERIALS CO., LTD.
Reel/Frame 074941/0803 →
CHANGE OF ADDRESS Recorded Feb 19, 2026
From: KABUSHIKI KAISHA TOSHIBA
To: KABUSHIKI KAISHA TOSHIBA
Reel/Frame 074941/0846 →
Priority Claims (2)
JP 2011-278944 · Dec 20, 2011 · national
JP 2012-150017 · Jul 3, 2012 · national
Continuity (3)
Continuation 14309025 · Jun 19, 2014
Continuation PCTJP2012083106 · Dec 20, 2012
Related Publication 20180073107A1 · Mar 15, 2018