IP Library Granted Patent US 10,995,188
Granted Patent B2
US 10,995,188 · App. 15/794,811 · Granted May 4, 2021

Stabilizer for polyamides

Inventors: Suneel Bandi (West Lafayette, IN); Andreas Pawlik (Recklinghausen, DE)
Assignee: Evonik Operations GmbH
C08J5/043C08G69/265C08L77/06C08J2377/06C08J2465/00
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Quick Facts
Patent No.
US 10,995,188
App. No.
15/794,811
Granted
May 4, 2021
Kind
B2
Abstract

The present invention relates to a thermoplastic composition that provides improved thermal aging stability. The thermoplastic composition includes a polyamide resin, glass fibers, tin(II) oxalate, and a functional additive. It has been found that a combination of a polyamide resin with tin(II) oxalate and a functional additive produces a superior product demonstrating greater thermal stability than the polyamide resin alone.

Claims (21)

1. A thermoplastic composition, comprising, based on a total weight of the composition;

a) 30 to 90 wt % of a polyamide resin;

b) 5 to 65 wt % of reinforcing fibers;

c) 2 to 10 wt % of tin(II) oxalate; and

d) 0.1 to 20 wt % of a functional additive,

wherein the functional additive is polyalkenylene, and

wherein the contents sum up to 100 wt %.

2. The thermoplastic composition of claim 1 , comprising, based on the total weight of the composition:

a) 40 to 70 wt % of the polyamide resin;

b) 20 to 50 wt % of reinforcing fibers;

c) 2 to 5 wt % of tin(II) oxalate; and

d) 1 to 15 wt % of the functional additive which is polyalkenylene,

wherein the contents sum up to 100 wt %.

3. The thermoplastic composition of claim 1 , wherein the polyamide resin is at least one selected from the group consisting of Nylon 6, Nylon 6,6, Nylon 6,12, Nylon 4,6, Nylon 6,10, Nylon 7, Nylon 10, Nylon 10, 10, Nylon 12, Nylon 12, 12, Nylon 9T, Nylon 10 T, Nylon 6T, Nylon 6T/6I, Nylon 6T/DT, and Nylon MXD-6.

4. The thermoplastic composition of claim 1 , wherein the polyamide resin is semicrystalline polyphthalamide.

5. The thermoplastic composition of claim 1 , wherein the reinforcing fibers is glass fibers.

6. The thermoplastic composition of claim 1 , wherein the functional additive is polyalkenylene comprising repeat units of the following formula:

[CH═CH—(CH 2 ) n ],

wherein n=from 3 to 10.

7. The thermoplastic composition of claim 1 , further comprising at least one additive selected from the group consisting of lubricants, glass fillers, mineral fillers, impact modifiers, plasticizers, pigments, dyes, antioxidants, heat stabilizers, hydrolysis stabilizers, nucleating agents, flame retardants, synergists, drip suppressants, and blowing agents.

8. The thermoplastic composition of claim 1 , wherein, after 1000 hours of hot air testing at 230° C., the thermoplastic composition is capable of retaining greater than 60% of its tensile strength compared to a tensile strength before the hot air testing.

Assignments (5)
CHANGE OF NAME Recorded Jan 31, 2020
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 051765/0166 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 26, 2018
From: EVONIK RESOURCE EFFICIENCY GMBH
To: EVONIK DEGUSSA GMBH
Reel/Frame 046981/0271 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 26, 2018
From: EVONIK CORPORATION
To: EVONIK DEGUSSA GMBH
Reel/Frame 046981/0381 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 5, 2018
From: BANDI, SUNEEL
To: EVONIK CORPORATION
Reel/Frame 046785/0651 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 5, 2018
From: PAWLIK, ANDREAS
To: EVONIK RESOURCE EFFICIENCY GMBH
Reel/Frame 046785/0689 →