IP Library Granted Patent US 10,400,314
Granted Patent B2
US 10,400,314 · App. 15/801,707 · Granted Sep 3, 2019

Niobium-based alloy that is resistant to aqueous corrosion

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Quick Facts
Patent No.
US 10,400,314
App. No.
15/801,707
Granted
Sep 3, 2019
Kind
B2
Abstract

In various embodiments, a metal alloy resistant to aqueous corrosion consists essentially of or consists of niobium with additions of tungsten, molybdenum, and one or both of ruthenium and palladium.

Claims (43)

1. A heat exchanger for use with acidic process fluid, the heat exchanger comprising:

a shell defining therewithin an interior volume for containing a heat-exchange fluid;

disposed within the interior volume, a plurality of tubes for containing the process fluid during heat exchange between the process fluid and the heat-exchange fluid;

fluidly connected to the plurality of tubes, a process inlet for supplying the process fluid to the plurality of tubes;

fluidly connected to the plurality of tubes, a process outlet for receiving the process fluid from the plurality of tubes;

fluidly connected to the interior volume, an exchange inlet for supplying the heat-exchange fluid to the interior volume; and

fluidly connected to the interior volume, an exchange outlet for receiving the heat-exchange fluid from the interior volume,

wherein an interior of each of the tubes is composed of a metallic alloy consisting essentially of (i) 2 weight percent-10 weight percent tungsten, (ii) 0.5 weight percent-10 weight percent molybdenum, (iii) at least one of ruthenium or palladium collectively present at 0.2 weight percent-5 weight percent, and (iv) the balance niobium.

2. The heat exchanger of claim 1 , wherein a grain size of the metallic alloy is greater than 6 microns.

3. The heat exchanger of claim 1 , wherein each of the tubes comprises steel and a layer of the metallic alloy disposed on an interior surface thereof.

4. The heat exchanger of claim 1 , wherein the shell of the heat exchanger comprises steel.

5. The heat exchanger of claim 1 , wherein an entirety of each of the tubes is composed of the metallic alloy.

6. The heat exchanger of claim 1 , wherein the alloy comprises both ruthenium and palladium.

7. The heat exchanger of claim 6 , wherein a ratio of ruthenium content to palladium content in the alloy ranges from 1000:1 to 1:1000.

8. The heat exchanger of claim 6 , wherein a ratio of ruthenium content to palladium content in the alloy ranges from 500:1 to 1:500.

9. The heat exchanger of claim 6 , wherein a ratio of ruthenium content to palladium content in the alloy ranges from 100:1 to 1:100.

10. The heat exchanger of claim 1 , wherein the alloy contains 2 weight percent-10 weight percent molybdenum.

11. The heat exchanger of claim 1 , wherein the alloy contains at least one of ruthenium or palladium collectively present at 2 weight percent-5 weight percent.

12. A heat exchanger for use with acidic process fluid, the heat exchanger comprising:

a shell defining therewithin an interior volume for containing a heat-exchange fluid;

disposed within the interior volume, a plurality of tubes for containing the process fluid during heat exchange between the process fluid and the heat-exchange fluid;

fluidly connected to the plurality of tubes, a process inlet for supplying the process fluid to the plurality of tubes;

fluidly connected to the plurality of tubes, a process outlet for receiving the process fluid from the plurality of tubes;

fluidly connected to the interior volume, an exchange inlet for supplying the heat-exchange fluid to the interior volume; and

fluidly connected to the interior volume, an exchange outlet for receiving the heat-exchange fluid from the interior volume,

wherein an interior of each of the tubes is composed of a metallic alloy consisting essentially of (i) 1 weight percent-10 weight percent tungsten, (ii) 2 weight percent-10 weight percent molybdenum, (iii) at least one of ruthenium or palladium collectively present at 0.2 weight percent-5 weight percent, and (iv) the balance niobium.

13. The heat exchanger of claim 12 , wherein each of the tubes comprises steel and a layer of the metallic alloy disposed on an interior surface thereof.

14. The heat exchanger of claim 12 , wherein the shell of the heat exchanger comprises steel.

15. The heat exchanger of claim 12 , wherein an entirety of each of the tubes is composed of the metallic alloy.

16. The heat exchanger of claim 12 , wherein the alloy comprises both ruthenium and palladium.

17. The heat exchanger of claim 12 , wherein the alloy contains at least one of ruthenium or palladium collectively present at 2 weight percent-5 weight percent.

18. A heat exchanger for use with acidic process fluid, the heat exchanger comprising:

a shell defining therewithin an interior volume for containing a heat-exchange fluid;

disposed within the interior volume, a plurality of tubes for containing the process fluid during heat exchange between the process fluid and the heat-exchange fluid;

fluidly connected to the plurality of tubes, a process inlet for supplying the process fluid to the plurality of tubes;

fluidly connected to the plurality of tubes, a process outlet for receiving the process fluid from the plurality of tubes;

fluidly connected to the interior volume, an exchange inlet for supplying the heat-exchange fluid to the interior volume; and

fluidly connected to the interior volume, an exchange outlet for receiving the heat-exchange fluid from the interior volume,

wherein an interior of each of the tubes is composed of a metallic alloy consisting essentially of (i) 1 weight percent-10 weight percent tungsten, (ii) 0.5 weight percent-10 weight percent molybdenum, (iii) at least one of ruthenium or palladium collectively present at 2 weight percent-5 weight percent, and (iv) the balance niobium.

19. The heat exchanger of claim 18 , wherein each of the tubes comprises steel and a layer of the metallic alloy disposed on an interior surface thereof.

20. The heat exchanger of claim 18 , wherein the shell of the heat exchanger comprises steel.

21. The heat exchanger of claim 18 , wherein an entirety of each of the tubes is composed of the metallic alloy.

22. The heat exchanger of claim 18 , wherein the alloy comprises both ruthenium and palladium.

Assignments (3)
CHANGE OF NAME Recorded Apr 5, 2022
From: H.C. STARCK INC.
To: MATERION NEWTON INC.
Reel/Frame 059596/0925 →
SECURITY INTEREST Recorded Nov 1, 2021
From: H.C. STARCK INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 057978/0970 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 3, 2017
From: AIMONE, PAUL; YANG, MEI
To: H.C. STARCK INC.
Reel/Frame 044029/0625 →