IP Library Granted Patent US 10,570,236
Granted Patent B2
US 10,570,236 · App. 15/836,490 · Granted Feb 25, 2020

Combined seals, compositions, and methods of making the same

Inventors: Krishnamachari Gopalan (Troy, MI); Robert J. Lenhart (Fort Wayne, IN); Gending Ji (Waterloo, CA); Roland Herd-Smith (Brignancourt, FR)
Assignee: Cooper-Standard Automotive Inc.
C08F255/02C08J3/24C08J9/0061C08J9/228C08K3/011C08K3/36C08K5/0025C08L23/0815C08L23/12C08L23/14C08L23/142C08L23/16C08F2500/21C08J2351/06C08J2423/08C08J2423/12C08J2423/14C08L2205/025C08L2312/08
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Quick Facts
Patent No.
US 10,570,236
App. No.
15/836,490
Granted
Feb 25, 2020
Kind
B2
Abstract

A combined sealing member is provided that includes a composition comprising two or more polyolefin elastomers selected from the group consisting of a dense, a micro-dense and a dynamic silane-crosslinked polyolefin elastomer having a respective density of less than 0.90 g/cm 3 , less than 0.70 g/cm 3 , and less than 0.60 g/cm 3 . The combined sealing member exhibits a compression set of from about 5.0% to about 35.0%, as measured according to ASTM D 395 (22 hrs @ 70° C.).

Claims (34)

1. A combined sealing member comprising:

a composition comprising two or more polyolefin elastomers selected from the group consisting of a dense, a micro-dense and a dynamic silane-crosslinked polyolefin elastomer having a respective density of less than 0.90 g/cm 3 , less than 0.70 g/cm 3 , and less than 0.60 g/cm 3 ,

wherein the combined sealing member exhibits a compression set of from about 5.0% to about 35.0%, as measured according to ASTM D 395 (22 hrs @ 70° C.).

2. The combined sealing member of claim 1 , wherein the dense silane-crosslinked polyolefin elastomer comprises a first polyolefin having a density less than 0.86 g/cm 3 , a second polyolefin having a percent crystallinity less than 40%, a silane crosslinker, a grafting initiator, and a non-metal condensation catalyst,

wherein the microdense silane-crosslinked polyolefin elastomer comprises a first polyolefin having a density less than 0.86 g/cm 3 , a second polyolefin having a percent crystallinity less than 40%, a silane crosslinker, a grafting initiator, a condensation catalyst and a microencapsulated foaming agent, and

further wherein the dynamic silane-crosslinked polyolefin elastomer comprises a first polyolefin having a density less than 0.86 g/cm 3 , a second polyolefin having a percent crystallinity less than 40%, a silane crosslinker, a grafting initiator, a condensation catalyst and a foaming agent.

3. The combined sealing member of claim 1 , wherein the compression set is from about 15.0% to about 35.0%, as measured according to ASTM D 395 (22 hrs @ 70° C.).

4. The combined sealing member of claim 1 , wherein the density is from about 0.50 g/cm 3 to about 0.89 g/cm 3 .

5. The combined sealing member of claim 1 , wherein the silane-crosslinked polyolefin elastomer exhibits a crystallinity of from about 5% to about 25%.

6. The combined sealing member of claim 1 , wherein the silane-crosslinked polyolefin elastomer exhibits a glass transition temperature of from about −75° C. to about −25° C.

7. The combined sealing member of claim 1 , wherein the composition is a thermoset, but exhibits thermoplastic properties during processing.

8. The combined sealing member of claim 1 , wherein the sealing member exhibits a weathering color difference of from about 0.25 ΔE to about 2.0 ΔE, as measured according to ASTM D2244.

9. The combined sealing member of claim 1 , further comprising:

a coloring agent.

10. A combined sealing member comprising:

a composition comprising a first and a second polyolefin elastomer,

wherein the first elastomer comprises a microdense silane-crosslinked polyolefin elastomer having a density of less than 0.70 g/cm 3 ,

wherein the second elastomer comprises a dense silane-crosslinked polyolefin elastomer having a density of less than 0.90 g/cm 3 or a dynamic silane-crosslinked polyolefin elastomer having a density of less than 0.60 g/cm 3 , and

further wherein the combined sealing member exhibits a compression set of from about 5.0% to about 35.0%, as measured according to ASTM D 395 (22 hrs @ 70° C.).

11. The combined sealing member of claim 10 , wherein the compression set is from about 15.0% to about 35.0%, as measured according to ASTM D 395 (22 hrs @ 70° C.).

12. The combined sealing member of claim 10 , wherein the density is from about 0.50 g/cm 3 to about 0.89 g/cm 3 .

13. The combined sealing member of claim 10 , wherein the silane-crosslinked polyolefin elastomer exhibits a crystallinity of from about 5% to about 25%.

14. The combined sealing member of claim 10 , wherein the silane-crosslinked polyolefin elastomer exhibits a glass transition temperature of from about −75° C. to about −25° C.

15. A combined sealing member comprising:

a composition comprising a first and a second polyolefin elastomer,

wherein the first elastomer comprises a dense silane-crosslinked polyolefin elastomer having a density of less than 0.90 g/cm 3 ,

wherein the second elastomer comprises a dynamic silane-crosslinked polyolefin elastomer having a density of less than 0.60 g/cm 3 , and

further wherein the combined sealing member exhibits a compression set of from about 5.0% to about 35.0%, as measured according to ASTM D 395 (22 hrs @ 70° C.).

16. The combined sealing member of claim 15 , wherein the compression set is from about 15.0% to about 35.0%, as measured according to ASTM D 395 (22 hrs @ 70° C.).

17. The combined sealing member of claim 15 , wherein the density is from about 0.50 g/cm 3 to about 0.89 g/cm 3 .

18. The combined sealing member of claim 15 , wherein the silane-crosslinked polyolefin elastomer exhibits a crystallinity of from about 5% to about 25%.

19. The combined sealing member of claim 15 , wherein the silane-crosslinked polyolefin elastomer exhibits a glass transition temperature of from about −75° C. to about −25° C.

20. The combined sealing member of claim 15 , further comprising:

a coloring agent.

Assignments (11)
PATENT SECURITY AGREEMENT Recorded Mar 5, 2026
From: COOPER-STANDARD AUTOMOTIVE INC.
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION
Reel/Frame 075019/0478 →
RELEASE OF SECURITY INTEREST IN PATENTS PREVIOUSLY RECORDED REEL/FRAME (062544/0357) Recorded Mar 4, 2026
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
Reel/Frame 075022/0543 →
RELEASE OF SECURITY INTEREST IN PATENTS PREVIOUSLY RECORDED AT REEL/FRAME (062545/0715) Recorded Mar 4, 2026
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
Reel/Frame 075022/0267 →
PATENT SECURITY AGREEMENT (1ST LIEN) Recorded Jan 30, 2023
From: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 062544/0357 →
PATENT SECURITY AGREEMENT (3RD LIEN) Recorded Jan 30, 2023
From: COOPER-STANDARD AUTOMOTIVE INC.; COOPER-STANDARD INDUSTRIAL AND SPECIALTY GROUP, LLC
To: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 062545/0715 →
TERMINATION AND RELEASE OF SECURITY INTEREST PREVIOUSLY RECORDED AT REEL/FRAME (052788/0158) Recorded Jan 29, 2023
From: DEUTSCHE BANK AG NEW YORK BRANCH, AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC.
Reel/Frame 062539/0706 →
TERMINATION AND RELEASE OF SECURITY INTEREST PREVIOUSLY RECORDED AT REEL/FRAME (052788/0392) Recorded Jan 27, 2023
From: U.S. BANK TRUST COMPANY, NATIONAL ASSOCIATION (SUCCESSOR IN INTEREST TO U.S. BANK NATIONAL ASSOCIATION), AS COLLATERAL AGENT
To: COOPER-STANDARD AUTOMOTIVE INC
Reel/Frame 062540/0108 →
PATENT SECURITY AGREEMENT Recorded May 31, 2020
From: COOPER-STANDARD AUTOMOTIVE INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 052797/0812 →
PATENT SECURITY AGREEMENT Recorded May 29, 2020
From: COOPER-STANDARD AUTOMOTIVE INC.
To: U.S. BANK NATIONAL ASSOCIATION, AS COLLATERAL AGENT
Reel/Frame 052788/0392 →
SECURITY AGREEMENT Recorded May 29, 2020
From: COOPER-STANDARD AUTOMOTIVE INC.
To: DEUTSCHE BANK AG NEW YORK BRANCH
Reel/Frame 052788/0158 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 8, 2017
From: GOPALAN, KRISHNAMACHARI; LENHART, ROBERT J.; JI, GENDING; HERD-SMITH, ROLAND
To: COOPER-STANDARD AUTOMOTIVE INC.
Reel/Frame 044343/0218 →
Continuity (2)
Provisional Application 62497954 · Dec 10, 2016
Related Publication 20180163032A1 · Jun 14, 2018