IP Library Granted Patent US 10,538,688
Granted Patent B2
US 10,538,688 · App. 15/886,512 · Granted Jan 21, 2020

Extrudable pressure sensitive adhesive composition and methods for preparing the same

Inventors: Jiansheng Tang (Westfield, IN); John Fieldhouse (Nashville, TN)
Assignee: Firestone Building Products Co., LLC
C09J115/02C08F36/08C08G18/542C08J3/005C08J3/24C08L23/22C08L75/04C09J175/04C08G2170/40C08J2315/02C08J2475/04
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,538,688
App. No.
15/886,512
Granted
Jan 21, 2020
Kind
B2
Abstract

A phase-separated polymeric composition is provided that comprises a first phase including polyurethane domains and a second phase including a butyl rubber matrix. A method is also provided for producing a polymer composition. The method includes providing a masterbatch composition that is prepared by combining a halogenated butyl rubber with at least one phenolic resin, introducing the masterbatch composition to a reactor, introducing to the reactor an isocyanate and a polyurethane catalyst to form a blend, and subjecting the blend to conditions sufficient to form a polyurethane.

Claims (11)

1. A method for producing a polymer blend that includes butyl rubber and polyurethane, the method comprising:

i. providing a masterbatch composition that is prepared by combining a halogenated butyl rubber with at least one unfunctionalized phenolic resin, to form a partially crosslinked butyl rubber;

ii. introducing the masterbatch composition and, optionally, additional unfunctionalized phenolic resin to a reactor;

iii, introducing an isocyanate and a polyurethane catalyst to the reactor containing the masterbatch composition; and

iv. subjecting the reactor to conditions sufficient to form a polyurethane in the presence of the partially crosslinked butyl rubber, thereby forming a polymer blend of butyl rubber and polyurethane.

2. The method of claim 1 , where the isocyanate is a diisocyanate.

3. The method of claim 1 , where the polyurethane is in the form of discreet domains within a matrix formed by the butyl rubber up to temperatures of at least 100° C.

4. The method of claim 1 , where the polyurethane is in the form of discrete domains within a matrix formed by the butyl rubber up to temperatures of at least 120° C.

5. The method of claim 1 , further comprising the step of introducing an oil to the reactor.

6. The method of claim 1 , further comprising the step of introducing a tackifier resin to the reactor.

7. The method of claim 1 , where the polyurethane is cocontinuous with the butyl rubber at temperatures above 120° C.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 28, 2025
From: HOLCIM TECHNOLOGY LTD
To: AMRIZE TECHNOLOGY SWITZERLAND LLC
Reel/Frame 073030/0406 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 6, 2022
From: FIRESTONE BUILDING PRODUCTS COMPANY, LLC
To: HOLCIM TECHNOLOGY LTD
Reel/Frame 061034/0752 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 1, 2018
From: FIELDHOUSE, JOHN; TANG, JIANSHENG
To: FIRESTONE BUILDING PRODUCTS CO., LLC
Reel/Frame 044803/0114 →