IP Library Granted Patent US 10,472,350
Granted Patent B2
US 10,472,350 · App. 15/911,797 · Granted Nov 12, 2019

Soluble guanylate cyclase activators and their use

Inventors: Nerina Dodic (Les Ulis, FR); Anne Marie Jeanne Bouillot (Les Ulis, FR)
Assignee: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
C07D405/14C07D401/14
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Quick Facts
Patent No.
US 10,472,350
App. No.
15/911,797
Granted
Nov 12, 2019
Kind
B2
Abstract

The invention relates to activators of soluble guanylate cyclase and their use in pharmaceutical compositions, primarily topically administered ophthalmic compositions. The pharmaceutical compositions are useful for reducing intraocular pressure in animals of the mammalian species.

Claims (46)

1. A pharmaceutical composition comprising a compound, or a pharmaceutically acceptable salt thereof, which is 1-(6-(3,5-difluoro-2-((4-methyl-6-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)pyridin-3-yl)methoxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(tetrahydrofuran-3-carbonyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, or 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, and one or more pharmaceutically acceptable excipients.

2. A method for reducing elevated intraocular pressure in a human comprising administering to the human an effective amount of a compound according to Formula (I), or a pharmaceutically acceptable salt thereof:

wherein:

R 1 is selected from H and —C 1-3 alkyl;

R 2 and R 3 are each independently selected from H and halogen;

R 4 is selected from H, —C 1-3 alkyl, —O—C 1-3 alkyl, —O—C 3-4 cycloalkyl, —O—(CH 2 ) p -oxetanyl, and —O—(CH 2 ) p -tetrahydrofuranyl;

X and Y are each CH; or if X is N, then Y is CH; or if Y is N then X is CH;

A is absent or O;

R 5 is selected from —C 1-4 alkyl, —C 3-4 cycloalkyl, —(CH 2 ) n CN, —(CH 2 ) n CF 3 , —(CH 2 ) m -tetrahydrofuranyl, —(CH 2 ) m -oxetanyl, —C 2-5 alkyl-OH, —C 2-5 alkyl-OCH 3 and —CO—R 6 ;

R 6 is selected from —C 1-6 alkyl and —C 3-6 cycloalkyl, optionally substituted by —OH, —OCH 3 , —CN, COOH or —F, or R 6 is —(CH 2 ) m -tetrahydrofuranyl or —(CH 2 ) m -oxetanyl, or R 6 is a (CH 2 ) m -4 to 5-membered heterocycle;

n is 1 or 2;

m is 0 or 1; and

p is 0 or 1.

3. A method of treating glaucoma in a human comprising administering to the human an effective amount of a compound of Formula (I), or a pharmaceutically acceptable salt thereof:

wherein:

R 1 is selected from H and —C 1-3 alkyl;

R 2 and R 3 are each independently selected from H and halogen;

R 4 is selected from H, —C 1-3 alkyl, —O—C 1-3 alkyl, —O—C 3-4 cycloalkyl, —O—(CH 2 ) p -oxetanyl, and —O—(CH 2 ) p -tetrahydrofuranyl;

X and Y are each CH; or if X is N, then Y is CH; or if Y is N then X is CH;

A is absent or O;

R 5 is selected from —C 1-4 alkyl, —C 3-4 cycloalkyl, —(CH 2 ) n CN, —(CH 2 ) n CF 3 , —(CH 2 ) m -tetrahydrofuranyl, —(CH 2 ) m -oxetanyl, —C 2-5 alkyl-OH, —C 2-5 alkyl-OCH 3 and —CO—R 6 ;

R 6 is selected from —C 1-6 alkyl and —C 3-6 cycloalkyl, optionally substituted by —OH, —OCH 3 , —CN, COOH or —F, or R 6 is —(CH 2 ) m -tetrahydrofuranyl or —(CH 2 ) m -oxetanyl, or R 6 is a (CH 2 ) m -4 to 5-membered heterocycle;

n is 1 or 2;

m is 0 or 1; and

p is 0 or 1.

4. A method of treating ocular hypertension in a human comprising administering to the human an effective amount of a compound of Formula (I), or a pharmaceutically acceptable salt thereof:

wherein:

R 1 is selected from H and —C 1-3 alkyl;

R 2 and R 3 are each independently selected from H and halogen;

R 4 is selected from H, —C 1-3 alkyl, —O—C 1-3 alkyl, —O—C 3-4 cycloalkyl, —O—(CH 2 ) p -oxetanyl, and —O—(CH 2 ) p -tetrahydrofuranyl;

X and Y are each CH; or if X is N, then Y is CH; or if Y is N then X is CH;

A is absent or O;

R 5 is selected from —C 1-4 alkyl, —C 3-4 cycloalkyl, —(CH 2 ) n CN, —(CH 2 ) n CF 3 , —(CH 2 ) m -tetrahydrofuranyl, —(CH 2 ) m -oxetanyl, —C 2-5 alkyl-OH, —C 2-5 alkyl-OCH 3 and —CO—R 6 ;

R 6 is selected from —C 1-6 alkyl and —C 3-6 cycloalkyl, optionally substituted by —OH, —OCH 3 , —CN, COOH or —F, or R 6 is —(CH 2 ) m -tetrahydrofuranyl or —(CH 2 ) m -oxetanyl, or R 6 is a (CH 2 ) m -4 to 5-membered heterocycle;

n is 1 or 2;

m is 0 or 1; and

p is 0 or 1.

5. The method according to claim 2 , wherein the compound, or a pharmaceutically acceptable salt thereof, is selected from 1-(6-(3,5-difluoro-2-((4-methyl-6-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)pyridin-3-yl)methoxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(tetrahydrofuran-3-carbonyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, or 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid.

6. The method according to claim 3 , wherein the compound, or a pharmaceutically acceptable salt thereof, is selected from 1-(6-(3,5-difluoro-2-((4-methyl-6-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)pyridin-3-yl)methoxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(tetrahydrofuran-3-carbonyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, or 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid.

7. The method according to claim 4 , wherein the compound, or a pharmaceutically acceptable salt thereof, is selected from 1-(6-(3,5-difluoro-2-((4-methyl-6-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)pyridin-3-yl)methoxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(tetrahydrofuran-3-carbonyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid, or 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid.

8. A method for reducing elevated intraocular pressure in a human comprising administering to the human an effective amount of a compound which is 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid:

or a pharmaceutically acceptable salt thereof.

9. A method of treating glaucoma in a human comprising administering to the human an effective amount of a compound which is 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid:

or a pharmaceutically acceptable salt thereof.

10. A method of treating ocular hypertension in a human comprising administering to the human an effective amount of a compound which is 1-(6-(3,5-difluoro-2-((2-methyl-4-(1-(2,2,2-trifluoroethyl)piperidin-4-yl)benzyl)oxy)phenyl)pyridin-2-yl)piperidine-4-carboxylic acid:

or a pharmaceutically acceptable salt thereof.

Assignments (2)
CHANGE OF ADDRESS Recorded Oct 8, 2025
From: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
To: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
Reel/Frame 073032/0390 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 11, 2019
From: BOUILLOT, ANNE MARIE JEANNE; DODIC, NERINA
To: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
Reel/Frame 049725/0736 →
Continuity (3)
Division 15509895
Provisional Application 62052537 · Sep 19, 2014
Related Publication 20180194756A1 · Jul 12, 2018