AEI zeolite synthesis
A novel method for synthesizing AEI zeolites is provided which results in high overall relative yields on silica and the structure directing agent.
1. A washcoat comprising AEI zeolite crystals having a mean aspect ratio (L/D) of less than or equal to about 3 and a mean crystallite size of about 1 to about 1.5 microns, wherein the AEI zeolite comprises phosphorous in an amount less than 0.1 weight percent based on the total weight of the zeolite.
2. The washcoat of claim 1 , wherein the alumniosilicate AEI zeolite crystals have a mean aspect ratio (L/D) of less than or equal to 2.0.
3. The washcoat of claim 1 , wherein the aluminosilicate AEI zeolite crystals have a silica-to-alumina ratio of about 10 to about 35.
4. The washcoat of claim 1 , wherein the aluminosilicate AEI zeolite crystals have a silica-to-alumina ratio of about 15 to about 25.
5. The washcoat of claim 1 , wherein the aluminosilicate AEI zeolite crystals contain post-synthesis exchanged ions of one or more transition metals.
6. The washcoat of claim 5 , wherein the transition metals comprise at least one metal selected from the group consisting of manganese, iron, cobalt, nickel, and mixtures thereof.
7. The washcoat of claim 5 , wherein the post-synthesis exchanged ions of one or more transition metals are present in an amount of about 0.1 to about 10 weight percent.
8. The washcoat of claim 1 , wherein the aluminosilicate zeolite contains about 0.5 to 5 weight percent post-synthesis exchanged copper ions, based on the total weight of the zeolite.