IP Library Granted Patent US 11,267,916
Granted Patent B2
US 11,267,916 · App. 15/929,578 · Granted Mar 8, 2022

Adhesive composition comprising amorphous propylene-ethylene copolymer and polyolefins

Inventors: Terri Roxanne Carvagno (Church Hill, TN); Susana Marques (Rotterdam, NL); Ming Allison Yuan (Shanghai, CN); Da Yu Vincent Zhang (Shanghai, CN); Boon Hui Janice Ang (Singapore, SG); Marc Stacey Somers (Kilgore, TX); Raymond Prescott Cottle (Longview, TX); Bennett H. Novak (Longview, TX); Puthenkovilakom Rajesh Raja (Baytown, TX)
Assignee: Eastman Chemical Company
C08F210/06C08F4/6465C08F4/6543C08F10/06C08K5/01C08K5/134C08K11/00C08L23/10C08L53/02C08L53/025C09J11/06C09J123/08C09J123/10C09J123/14C08L2205/025
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 11,267,916
App. No.
15/929,578
Granted
Mar 8, 2022
Kind
B2
Abstract

Amorphous propylene-ethylene copolymers are described herein that can include high amounts of ethylene and exhibit desirable softening points and needle penetrations. The desirable combinations of softening points and needle penetrations in these propylene-ethylene copolymers allow them to have a broad operating window. Due their broad operating window, the propylene-ethylene copolymers can be utilized in a wide array of applications and products, including hot melt adhesives.

Claims (54)

1. An adhesive comprising at least one propylene-ethylene copolymer and at least one polyolefin, wherein said at least one propylene-ethylene copolymer comprises:

a) at least 10 weight percent of ethylene, and

b) a softening point in the range of 90° C. to 121° C., and

c) a glass transition temperature (Tg) in the range of about −60 to about 20° C., and

d) needle penetration in the range of 10 to 30 dmm,

wherein said adhesive comprises:

(a) 5 to 95 weight percent of said at least one propylene-ethylene copolymer;

(b) 5 to 90 weight percent of said at least one polyolefin;

(c) not more than 70 weight percent of at least one tackifier;

(d) not more than 20 weight percent of at least one processing oil; and

(e) not more than 20 weight percent of at least one wax.

2. The adhesive of claim 1 , wherein said at least one polyolefin is selected from the group consisting of metallocene-catalyzed polyolefin polymers and elastomers, and chain shuttling catalyzed olefin block copolymers.

3. The adhesive of claim 1 , wherein said at least one polyolefin is selected from the group consisting of amorphous poly alpha olefins (APAO), wherein said amorphous poly alpha polyolefin comprises at least one monomer selected from the group consisting of ethylene, propylene, linear C 4 -C 10 alpha-olefin monomers, and branched C 4 -C 10 alpha-olefin monomers.

4. The adhesive of claim 2 , wherein said adhesive comprises:

(a) 5 to 95 weight percent of said at least one propylene-ethylene copolymer;

(b) 5 to 90 weight percent of said at least one polyolefin;

(c) not more than 70 weight percent of at least one tackifier;

(d) not more than 20 weight percent of at least one processing oil; and

(e) not more than 30 weight percent of at least one wax.

5. The adhesive of claim 2 , wherein said adhesive comprises:

(a) 10 to 70 weight percent of said at least one propylene-ethylene copolymer;

(b) 5 to 55 weight percent of said at least one polyolefin;

(c) not more than 70 weight percent of at least one tackifier;

(d) not more than 20 weight percent of at least one processing oil; and

(e) not more than 20 weight percent of at least one wax.

6. The adhesive of claim 2 , wherein said adhesive comprises:

(a) 20 to 80 weight percent of said at least one propylene-ethylene copolymer;

(b) 1 to 45 weight percent of said at least one polyolefin;

(c) not more than 70 weight percent of at least one tackifier;

(d) not more than 20 weight percent of at least one processing oil; and

(e) not more than 20 weight percent of at least one wax.

7. The adhesive of claim 3 , wherein said adhesive comprises:

(a) 5 to 95 weight percent of said at least one propylene-ethylene copolymer;

(b) 5 to 90 weight percent of said at least one polyolefin;

(c) not more than 70 weight percent of at least one tackifier;

(d) not more than 20 weight percent of at least one processing oil; and

(e) not more than 30 weight percent of at least one wax.

8. The adhesive of claim 3 , wherein said adhesive comprises:

(a) 10 to 70 weight percent of said at least one propylene-ethylene copolymer;

(b) 5 to 55 weight percent of said at least one polyolefin;

(c) not more than 70 weight percent of at least one tackifier;

(d) not more than 20 weight percent of at least one processing oil; and

(e) not more than 20 weight percent of at least one wax.

9. The adhesive of claim 3 , wherein said adhesive comprises:

(a) 20 to 80 weight percent of said at least one propylene-ethylene copolymer;

(b) 1 to 45 weight percent of said at least one polyolefin;

(c) not more than 70 weight percent of at least one tackifier;

(d) not more than 20 weight percent of at least one processing oil; and

(e) not more than 20 weight percent of at least one wax.

10. An article comprising the adhesive of claim 1 wherein said article is selected from the group consisting of adhesives, sealants, caulks, roofing membranes, waterproof membranes and underlayments, carpet, laminates, laminated articles, tapes labels, mastics, polymer blends, wire coatings, molded articles, heat seal coatings, disposable hygiene articles, insulating glass (IG) units, bridge decking, water proofing membranes, waterproofing compounds, underlayments, cable flooding/filling compounds, sheet molded compounds, dough molded compounds, overmolded compounds, rubber compounds, polyester composites, glass composites, fiberglass reinforced plastics, wood-plastic composites, polyacrylic blended compounds, lost-wax precision castings, investment casting wax compositions, candles, windows, films, gaskets, seals, o-rings, motor vehicle molded parts, motor vehicle extruded parts, clothing articles, rubber additive/processing aids, and fibers.

11. An article comprising the adhesive of claim 2 wherein said article is selected from the group consisting of adhesives, sealants, caulks, roofing membranes, waterproof membranes and underlayments, carpet, laminates, laminated articles, tapes labels, mastics, polymer blends, wire coatings, molded articles, heat seal coatings, disposable hygiene articles, insulating glass (IG) units, bridge decking, water proofing membranes, waterproofing compounds, underlayments, cable flooding/filling compounds, sheet molded compounds, dough molded compounds, overmolded compounds, rubber compounds, polyester composites, glass composites, fiberglass reinforced plastics, wood-plastic composites, polyacrylic blended compounds, lost-wax precision castings, investment casting wax compositions, candles, windows, films, gaskets, seals, o-rings, motor vehicle molded parts, motor vehicle extruded parts, clothing articles, rubber additive/processing aids, and fibers.

12. An article comprising the adhesive of claim 3 wherein said article is selected from the group consisting of adhesives, sealants, caulks, roofing membranes, waterproof membranes and underlayments, carpet, laminates, laminated articles, tapes labels, mastics, polymer blends, wire coatings, molded articles, heat seal coatings, disposable hygiene articles, insulating glass (IG) units, bridge decking, water proofing membranes, waterproofing compounds, underlayments, cable flooding/filling compounds, sheet molded compounds, dough molded compounds, overmolded compounds, rubber compounds, polyester composites, glass composites, fiberglass reinforced plastics, wood-plastic composites, polyacrylic blended compounds, lost-wax precision castings, investment casting wax compositions, candles, windows, films, gaskets, seals, o-rings, motor vehicle molded parts, motor vehicle extruded parts, clothing articles, rubber additive/processing aids, and fibers.

13. An article comprising the adhesive of claim 4 wherein said article is selected from the group consisting of adhesives, sealants, caulks, roofing membranes, waterproof membranes and underlayments, carpet, laminates, laminated articles, tapes labels, mastics, polymer blends, wire coatings, molded articles, heat seal coatings, disposable hygiene articles, insulating glass (IG) units, bridge decking, water proofing membranes, waterproofing compounds, underlayments, cable flooding/filling compounds, sheet molded compounds, dough molded compounds, overmolded compounds, rubber compounds, polyester composites, glass composites, fiberglass reinforced plastics, wood-plastic composites, polyacrylic blended compounds, lost-wax precision castings, investment casting wax compositions, candles, windows, films, gaskets, seals, o-rings, motor vehicle molded parts, motor vehicle extruded parts, clothing articles, rubber additive/processing aids, and fibers.

14. An article comprising the adhesive of claim 7 wherein said article is selected from the group consisting of adhesives, sealants, caulks, roofing membranes, waterproof membranes and underlayments, carpet, laminates, laminated articles, tapes labels, mastics, polymer blends, wire coatings, molded articles, heat seal coatings, disposable hygiene articles, insulating glass (IG) units, bridge decking, water proofing membranes, waterproofing compounds, underlayments, cable flooding/filling compounds, sheet molded compounds, dough molded compounds, overmolded compounds, rubber compounds, polyester composites, glass composites, fiberglass reinforced plastics, wood-plastic composites, polyacrylic blended compounds, lost-wax precision castings, investment casting wax compositions, candles, windows, films, gaskets, seals, o-rings, motor vehicle molded parts, motor vehicle extruded parts, clothing articles, rubber additive/processing aids, and fibers.

Assignments (9)
SECURITY INTEREST Recorded May 1, 2026
From: SYNTHOMER ADHESIVE TECHNOLOGIES LLC
To: GLAS TRUST CORPORATION LIMITED, AS SECURITY AGENT
Reel/Frame 075312/0405 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 25, 2022
From: EASTMAN CHEMICAL COMPANY
To: SYNTHOMER ADHESIVE TECHNOLOGIES LLC
Reel/Frame 059701/0508 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 31, 2020
From: EASTMAN CHEMICAL MIDDELBURG B.V.
To: EASTMAN CHEMICAL COMPANY
Reel/Frame 052795/0717 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 31, 2020
From: EASTMAN CHEMICAL (CHINA) CO., LTD.
To: EASTMAN CHEMICAL COMPANY
Reel/Frame 052795/0720 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 31, 2020
From: EASTMAN CHEMICAL, ASIA PACIFIC PTE.
To: EASTMAN CHEMICAL COMPANY
Reel/Frame 052795/0723 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2020
From: ANG, BOON HUI JANICE
To: EASTMAN CHEMICAL, ASIA PACIFIC PTE LIMITED
Reel/Frame 052687/0596 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2020
From: YUAN, MING ALLISON; ZHANG, DAYU VINCENT
To: EASTMAN CHEMICAL (CHINA) CO., LTD.
Reel/Frame 052687/0168 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2020
From: MARQUES, SUSANA DUARTE
To: EASTMAN CHEMICAL MIDDELBURG B. V.
Reel/Frame 052687/0604 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 18, 2020
From: CARVAGNO, TERRI ROXANNE; SOMERS, MARC STACEY; COTTLE, RAYMOND PRESCOTT; NOVAK, BENNETT H.; RAJA, PUTHENKOVILAKOM RAJESH
To: EASTMAN CHEMICAL COMPANY
Reel/Frame 052687/0621 →