IP Library Granted Patent US 11,554,102
Granted Patent B2
US 11,554,102 · App. 15/930,295 · Granted Jan 17, 2023

Gamma-hydroxybutyrate compositions and their uses for the treatment of disorders

Inventors: Clark P. Allphin (Los Altos, CA); Michael DesJardin (Aptos, CA)
Assignee: JAZZ PHARMACEUTICALS IRELAND LIMITED
A61K31/19A61K9/0053A61K9/08A61K31/554
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Quick Facts
Patent No.
US 11,554,102
App. No.
15/930,295
Granted
Jan 17, 2023
Kind
B2
Abstract

Provided herein are pharmaceutical compositions and formulations comprising mixed salts of gamma-hydroxybutyrate (GHB). Also provided herein are methods of making the pharmaceutical compositions and formulations, and methods of their use for the treatment of sleep disorders such as apnea, sleep time disturbances, narcolepsy, cataplexy, sleep paralysis, hypnagogic hallucination, sleep arousal, insomnia, and nocturnal myoclonus.

Claims (12)

1. A pharmaceutical composition of gamma-hydroxybutyrate (GHB) comprising a mixture of salts of GHB and a pharmaceutically acceptable carrier, wherein the mixture consists of a sodium salt of gamma-hydroxybutyrate (Na.GHB), a potassium salt of gamma-hydroxybutyrate (K.GHB), a magnesium salt of gamma-hydroxybutyrate (Mg.(GHB) 2 ), and a calcium salt of gamma-hydroxybutyrate (Ca.(GHB) 2 ), wherein the Na.GHB salt is present in a % molar equivalents of about 5% to about 40%, the K.GHB salt is present in a % molar equivalents of about 10% to about 40%, the Mg.(GHB) 2 salt is present in a % molar equivalents of about 5% to about 30%, and the Ca.(GHB) 2 salt is present in a % molar equivalents of about 20% to about 80%, wherein the composition is formulated as a liquid formulation, and wherein the liquid formulation has a total concentration of GHB salts of about 350 mg/mL, about 400 mg/mL, about 450 mg/mL, about 500 mg/mL, about 550 mg/mL, or about 600 mg/mL.

2. The pharmaceutical composition of claim 1 , wherein the Na.GHB salt is present in a % molar equivalents of about 5% to about 10%, about 10% to about 15%, about 15% to about 20%, about 20% to about 25%, about 25% to about 30%, about 30% to about 35%, or about 35% to about 40%.

3. The pharmaceutical composition of claim 1 , wherein the K.GHB salt is present in a % molar equivalents of about 10% to about 15%, about 15% to about 20%, about 20% to about 25%, about 25% to about 30%, about 30% to about 35%, or about 35% to about 40%.

4. The pharmaceutical composition of claim 1 , wherein the Mg.(GHB) 2 salt is present in a % molar equivalents of about 5% to about 10%, about 10% to about 15%, about 15% to about 20%, about 20% to about 25%, or about 25% to about 30%.

5. The pharmaceutical composition of claim 1 , wherein the Ca.(GHB) 2 salt is present in a % molar equivalents of about 20% to about 25%, about 25% to about 30%, about 30% to about 35%, about 35% to about 40%, about 40% to about 45%, about 45% to about 50%, about 50% to about 55%, about 55% to about 60%, about 60% to about 65%, about 65% to about 70%, about 70% to about 75%, or about 75% to about 80%.

6. The pharmaceutical composition of claim 1 , wherein the Na.GHB, K.GHB, Mg.(GHB) 2 , and Ca(GHB) 2 salts are present in a % molar equivalents ratio of about 8:23:21:48, respectively.

7. The pharmaceutical composition of claim 1 , wherein the total concentration of GHB salts is about 500 mg/mL.

8. The pharmaceutical composition of claim 1 , wherein the composition has a pH of about 7.5 to about 9.0.

9. The pharmaceutical composition of claim 1 , wherein the composition has a pH of about 8.0 to about 8.5.

10. The pharmaceutical composition of claim 1 , wherein the composition has a pH of about 8.3.

11. The pharmaceutical composition of claim 1 , wherein the composition is chemically stable and resistant to microbial growth, and wherein the composition is free of preservatives.

12. A pharmaceutical composition of gamma-hydroxybutyrate (GHB) comprising a mixture of salts of GHB, wherein the mixture consists of a sodium salt of gamma-hydroxybutyrate (Na.GHB), a potassium salt of gamma-hydroxybutyrate (K.GHB), a magnesium salt of gamma-hydroxybutyrate (Ca.(GHB) 2 ), and a calcium salt of gamma-hydroxybutyrate (Ca.(GHB) 2 ), wherein the Na.GHB, K.GHB, Mg.(GHB) 2 , and Ca.(GHB) 2 salts are present in a % molar equivalents ratio of about 8%:23%:21%:48%, respectively, wherein the composition is in a solid formulation which is a tablet or capsule.

Assignments (3)
SECURITY AGREEMENT Recorded May 5, 2021
From: CAVION, INC.; CELATOR PHARMACEUTICALS, INC.; JAZZ PHARMACEUTICALS IRELAND LIMITED; JAZZ PHARMACEUTICALS, INC.
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 056151/0010 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2020
From: ALLPHIN, CLARK P.; DESJARDIN, MICHAEL
To: JAZZ PHARMACEUTICALS, INC.
Reel/Frame 052805/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 1, 2020
From: JAZZ PHARMACEUTICALS, INC.
To: JAZZ PHARMACEUTICALS IRELAND LIMITED
Reel/Frame 052805/0249 →
Continuity (7)
Continuation 16230460 · Dec 21, 2018
Continuation 15385447 · Dec 20, 2016
Continuation 14821384 · Aug 7, 2015
Continuation 14045673 · Oct 3, 2013
Continuation 13739886 · Jan 11, 2013
Provisional Application 61737695 · Dec 14, 2012
Related Publication 20200338029A1 · Oct 29, 2020