Methods and systems for quantitatively measuring photoprotection
The present disclosure relates, according to some embodiments, to a method of determining a quantitatively measured photoprotection of a photoprotective composition, the method comprising: (a) distributing the photoprotective composition in a position in between a drawdown bar and at least one substrate to produce a distributed photoprotective composition; (b) drawing down the distributed photoprotective composition to a thickness on at least one substrate to produce a drawn down sample film; (c) drying the drawn down sample film to produce a dried sample film; (d) measuring a UV absorption of the dried sample film to produce a UV absorption spectrum; (e) determining the quantitatively measured photoprotection of the photoprotective composition from the UV absorption spectrum.
1. A drawdown system for quantitatively measuring photoprotection of a photoprotective composition, the drawdown system comprising:
(a) at least one substrate;
(b) a platform configured to receive the at least one substrate;
(c) a drawdown bar assembly comprising:
(i) a frame;
(ii) a drawdown bar; and
(iii) at least two spiral micrometers configured to adjust a height of the drawdown bar relative to a sample plate, wherein the height is from about 25 μm to about 200 μm;
(d) a backboard configured to adjust a position of the drawdown bar assembly;
(e) a motor movably connected to the backboard, wherein the motor is configured to adjust the position of the backboard at a velocity; and
(f) a UV absorption spectrophotometer configured to determine a sun protection factor (SPF) of the photoprotection composition.
2. The drawdown system of claim 1 , further comprising a processor configured to control the starting, resetting, velocity, and stopping of the motor.
3. The drawdown system of claim 1 , further comprising a position guide configured to guide a position of the drawdown bar assembly.
4. The drawdown system of claim 1 , wherein the at least one substrate is selected from the group consisting of a glass, a polymer, a skin, a metal, and a textile.
5. The drawdown system of claim 4 , wherein the glass comprises silica, quartz, fused silica, borosilicate glass, soda-lime silicate glass, phosphate glass, or combinations thereof.
6. The drawdown system of claim 4 , wherein the skin comprises a porcine skin, a human skin, a cow skin, a mouse skin, a rat skin, a frog skin, a snake skin, or combinations thereof.
7. The drawdown system of claim 1 , wherein the substrate has a length from about 50 mm to about 100 mm, a width from about 10 mm to about 40 mm, and a height from about 0.5 mm to about 5 mm.
8. The drawdown system of claim 1 , wherein the velocity is from about 0.1 m/s to about 1.0 m/s.
9. The drawdown system of claim 1 , wherein the motor assembly comprises a servomotor.