IP Library Granted Patent US 10,879,012
Granted Patent B2
US 10,879,012 · App. 15/997,403 · Granted Dec 29, 2020

Oxide layers and methods of making the same

Inventors: Philip Schulz (Massy, FR); Joseph Jonathan Berry (Boulder, CO); Arrelaine Allen Dameron (Boulder, CO); Paul Francois Ndione (Lakewood, CO)
Assignee: Alliance for Sustainable Energy, LLC
H01G9/2018H01G9/0036H01G9/2009H01L51/0001H01L51/0077H01L51/4226H01L51/4253H01L51/0009H01L2251/303
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Quick Facts
Patent No.
US 10,879,012
App. No.
15/997,403
Granted
Dec 29, 2020
Kind
B2
Abstract

The present application discloses devices that include a perovskite layer, a first layer that includes an oxide, and an interface layer, where the interface layer is positioned between the first layer and the perovskite layer, the interface layer is in physical contact with both the first layer and the perovskite layer, and the interface layer consists essentially of the oxide.

Claims (21)

1. A device comprising, in order:

a first oxide layer comprising TiO 2 ;

a perovskite layer comprising a halogen;

a second oxide layer comprising TiO 2 and having a first surface and a second surface defining a thickness between the first surface and the second surface; and

a hole transport layer, wherein:

the thickness is between 1 nm and 16 nm,

the first oxide layer is n-type,

the first surface is in physical contact with the perovskite layer, resulting in an interface between the perovskite layer and the first surface,

the interface is substantially free of an oxygen species comprising the halogen,

the second surface is in physical contact with the hole transport layer,

the second oxide layer is n type at the interface, and

the second oxide layer is less n-type at the second surface than at the interface.

2. The device of claim 1 , wherein the second oxide layer is free of an oxy-halogen species.

3. The device of claim 1 , further comprising a substrate, wherein the first oxide layer is positioned between the perovskite layer and the substrate.

4. The device of claim 1 , wherein the perovskite layer comprises at least one methyl ammonium lead iodide or formamidinium lead iodide.

5. The device of claim 1 , wherein the first oxide layer comprises a transparent conducting oxide.

6. The device of claim 5 , wherein the transparent conducting oxide comprises fluorine-doped tin oxide.

7. The device of claim 1 , wherein the hole transport layer comprises spiro-OMeTAD.

8. The device of claim 2 , wherein the oxy-halogen species comprises an oxy-iodo species.

9. The device of claim 1 , wherein the interface is free of any oxy-halogen species.

10. The device of claim 1 , wherein the second oxide layer is deposited by atomic layer deposition in the absence of oxygen.

Assignments (3)
CHANGE OF NAME Recorded Dec 16, 2025
From: ALLIANCE FOR SUSTAINABLE ENERGY, LLC
To: ALLIANCE FOR ENERGY INNOVATION, LLC
Reel/Frame 073993/0276 →
CONFIRMATORY LICENSE Recorded Apr 3, 2019
From: NATIONAL RENEWABLE ENERGY LABORATORY
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 048788/0437 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 4, 2018
From: SCHULZ, PHILIP; BERRY, JOSEPH JONATHAN; DAMERON, ARRELAINE ALLEN; NDIONE, PAUL FRANCOIS
To: ALLIANCE FOR SUSTAINABLE ENERGY, LLC
Reel/Frame 045982/0811 →