IP Library Granted Patent US 11,395,982
Granted Patent B1
US 11,395,982 · App. 16/011,496 · Granted Jul 26, 2022

Ultra low power acoustic separation

Inventors: James E. Coons (Los Alamos, NM); Felix Trampler (Hinterbruehl, AT); Benjamin H. J. Yap (Emeryville, CA)
Assignees: Triad National Security, LLC; SonoSep Technologies Inc.
B01D21/283B01J19/10C02F1/36
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Quick Facts
Patent No.
US 11,395,982
App. No.
16/011,496
Granted
Jul 26, 2022
Kind
B1
Abstract

Energy-efficient separation of particulates from fluids is based on determining particulate mass removal as a function of applied energy. Energy-efficient ultrasonic field powers and exposure durations are applied to a particulate containing fluid, and particles removed. In some cases, ultrasonic exposures are selected that provide the maximum particulate removal per applied energy.

Claims (33)

1. An ultrasonic separation method, comprising:

measuring at least a reference portion containing particulates in a fluid to determine an energy-efficient ultrasonic exposure for use in separation of particulates from the fluid, wherein the measuring a reference portion containing particulates in the fluid to determine the energy-efficient ultrasonic exposure comprises exposing the reference sample to an ultrasonic field at a selected ultrasonic power; measuring particulate separations at a plurality of times during the exposing, and determining the energy-efficient ultrasonic exposure based on the measured particulate separations and the plurality of times; and

processing at least a sample portion containing particulates in a fluid according to the energy-efficient ultrasonic exposure so as to separate a portion of particulates from the sample portion.

2. The ultrasonic separation method of claim 1 , further comprising:

selecting an ultrasonic exposure duration;

based on the selected ultrasonic exposure duration and the energy-efficient exposure, selecting an ultrasonic power, wherein the processing sample portion containing particulates in the fluid according to the energy-efficient ultrasonic exposure corresponds to applying the selected ultrasonic power for the selected ultrasonic exposure duration.

3. The ultrasonic separation method of claim 2 , wherein selecting the ultrasonic power corresponds to selecting an electrical drive power to an ultrasonic transducer.

4. The ultrasonic separation method of claim 2 , wherein selecting the ultrasonic power corresponds to selecting an electrical drive voltage and the selected ultrasonic power is applied based on driving an acoustic transducer with the selected electrical drive voltage.

5. The ultrasonic separation method of claim 1 , wherein the energy-efficient exposure is determined based on a change in a rate of particulate mass removal as a function of exposure.

6. The ultrasonic separation method of claim 1 , wherein the energy-efficient exposure is determined based on a decrease in a rate of change of particulate mass removal as a function of exposure.

7. The ultrasonic separation method of claim 6 , wherein the energy-efficient exposure is a determined based on a decrease of a rate of change of particulate mass removal as a function of exposure of at least of at least 20% with respect to a maximum rate of change.

8. The ultrasonic separation method of claim 1 , wherein the energy-efficient exposure is selected from an energy-efficient range associated with an estimated minimum energy per unit mass for particulate removal.

9. The ultrasonic separation method of claim 8 , wherein the energy-efficient range is defined by exposures within ±10% of a minimum energy exposure.

10. The ultrasonic separation method of claim 1 , wherein the energy-efficient exposure corresponds to an estimated minimum energy per unit mass for particulate removal.

11. The ultrasonic separation method of claim 1 , further comprising obtaining the reference portion and the sample portion from a common sample.

12. The ultrasonic separation method of claim 1 , further comprising extracting the separated particles.

13. An ultrasonic separator, comprising:

a sample container;

an ultrasonic generator situated to couple an ultrasonic field having a selected power to the sample container for a selected duration; and

an ultrasonic generator controller coupled to the ultrasonic generator configured to establish the selected power and the selected duration and provide an energy-efficient exposure to a particulate containing fluid situated in the sample container to extract particulates from the fluid in the sample container.

14. The ultrasonic separator of claim 13 , further comprising a memory device coupled to the ultrasonic generator controller, the memory device storing at least one energy-efficient exposure range or energy-efficient exposure associated with particulate extraction from the fluid.

15. The ultrasonic separator of claim 13 , wherein the ultrasonic generator and the sample container are configured to define an ultrasonic resonator so as to increase an ultrasonic field amplitude in the sample container.

16. The ultrasonic separator of claim 13 , further comprising a turbidity sensor coupled to the sample container and the ultrasonic generator controller, the turbidity sensor situated to determine a particulate concentration in a sample in the sample container, wherein the ultrasonic generator controller is coupled to adjust at least one of an RF drive power, a flow rate, or an exposure time based on at least one indicator of particulate concentration.

17. The ultrasonic separator of claim 16 , wherein the ultrasonic generator controller is coupled to adjust at least one of an RF drive power, a flow rate, or an exposure time based on a rate of change of particulate concentration.

18. The ultrasonic separator of claim 17 , wherein the ultrasonic generator controller is coupled to halt exposure based on a change in rate of change of a particulate concentration.

19. The ultrasonic separator of claim 17 , wherein the particulate concentration is in mass per volume.

20. An ultrasonic separation method, comprising:

exposing a first portion of a sample containing particulates in a fluid to an ultrasonic field to determine an energy-efficient ultrasonic exposure for use in separation of particulates from the fluid; and

exposing a second portion of the sample to an ultrasonic field according to the energy-efficient ultrasonic exposure so as to separate a portion of the particulates from the second portion of the sample.

21. An ultrasonic separation method, comprising:

obtaining a reference portion and a sample portion from a common sample containing particulates in a fluid;

measuring the reference portion containing particulates in the fluid to determine an energy-efficient ultrasonic exposure for use in separation of particulates from the fluid, wherein the measuring a reference portion containing particulates in the fluid to determine the energy-efficient ultrasonic exposure comprises exposing the reference sample to an ultrasonic field at a selected ultrasonic power, measuring particulate separations at a plurality of times during the exposing, and determining the energy-efficient ultrasonic exposure based on the measured particulate separations and the plurality of times; and

processing at least the sample portion containing particulates in the fluid according to the energy-efficient ultrasonic exposure so as to separate a portion of particulates from the sample portion.

Assignments (6)
CONFIRMATORY LICENSE Recorded Jan 24, 2023
From: TRIAD NATIONAL SECURITY, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 062490/0815 →
CONFIRMATORY LICENSE Recorded Mar 14, 2022
From: TRIAD NATIONAL SECURITY, LLC
To: UNITED STATES DEPARTMENT OF ENERGY
Reel/Frame 059807/0991 →
CONFIRMATORY LICENSE Recorded May 18, 2020
From: TRIAD NATIONAL SECURITY, LLC
To: U.S. DEPARTMENT OF ENERGY
Reel/Frame 052683/0997 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2018
From: LOS ALAMOS NATIONAL SECURITY, LLC
To: TRIAD NATIONAL SECURITY, LLC
Reel/Frame 048007/0803 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2018
From: COONS, JAMES E.; YAP, BENJAMIN H.J.
To: LOS ALAMOS NATIONAL SECURITY, LLC
Reel/Frame 046134/0236 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 19, 2018
From: TRAMPLER, FELIX
To: SONOSEP TECHNOLOGIES INC.
Reel/Frame 046134/0251 →
Continuity (1)
Provisional Application 62521149 · Jun 16, 2017