IP Library Granted Patent US 11,162,021
Granted Patent B2
US 11,162,021 · App. 16/012,452 · Granted Nov 2, 2021

Wellbore composition

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Quick Facts
Patent No.
US 11,162,021
App. No.
16/012,452
Granted
Nov 2, 2021
Kind
B2
Abstract

The embodiments described herein generally relate to methods and chemical compositions for use with wellbore treatment processes. In one embodiment, a composition is provided comprising a mineral acid and a retardation agent selected from the group of an amine containing compound, an amide containing compound, lignosulfonate, and combinations thereof.

Claims (54)

1. A composition, comprising:

from 5.0 to 28 wt % of a mineral acid; and

a retardation agent comprising:

an amine-containing resin; and

lignosulfonate; and

a viscosity modifier, wherein the amine-containing resin, comprises from 0.01 to 5.0 wt % of the composition.

2. The composition of claim 1 , wherein the composition further comprises water.

3. The composition of claim 1 , wherein the mineral acid is selected from the group consisting of hydrochloric acid, nitric acid, phosphoric acid, sulfuric acid, hydrofluoric acid, hydrobromic acid, perchloric acid, hydroiodic acid, and combinations thereof.

4. The composition of claim 1 , wherein the amine-containing resins are selected from the group consisting of urea-formaldehyde, urea-formaldehyde derivative, and combinations thereof.

5. The composition of claim 1 , wherein the composition further comprises an additive selected from the group consisting of a corrosion inhibitor, an anti-sludge agent, a chelating agent, an hydrogen sulfide scavenger, and combinations thereof.

6. The composition of claim 1 , wherein the lignosulfonate exerts a degree of sulfonation ranging from about 0.2 to about 5.0.

7. The composition of claim 1 , wherein the lignosulfonate comprises one or more cations selected from the group consisting of ammonium cations, lithium cations, sodium cations, potassium cations, silver cations, calcium cations, magnesium cations, zinc cations, iron cations, copper cations, cobalt cations, manganese cations, nickel cations, titanium cations, aluminum cations, and combinations thereof.

8. The composition of claim 4 , wherein the amine-containing resins are selected from the group consisting of urea-formaldehyde resin, melamine-formaldehyde resins, melamine-urea-formaldehyde resins, derivations thereof, and combinations thereof.

9. The composition of claim 1 , wherein the

mineral acid and

retardation agent

comprise a wt % ratio of mineral acid to retardation agent from 1:1 to 5:1.

10. The composition of claim 1 , wherein the composition comprises:

from 5.0 to 28 wt % hydrochloric acid;

from 0.01 to 5.0 wt % sulfuric acid;

from 0.01 to 5.0 wt % urea-formaldehyde, urea-formaldehyde derivative, or both;

from 0.01 to 20 wt % lignosulfonate; and

from 42 to 94.97 wt % water, wherein the amount of the components totals 100 wt. %.

11. The composition of claim 5 , wherein the composition comprises:

from about 0.01 to about 5.0 wt % of the additive selected from the group consisting of a corrosion inhibitor, an anti-sludge agent, a chelating agent, a hydrogen sulfide scavenger, and combinations thereof.

12. The composition of claim 5 , wherein the composition comprises:

from about 5.0 to about 28 wt % hydrochloric acid;

from about 0.01 to about 5.0 wt % sulfuric acid;

from about 0.01 to about 5.0 wt % urea-formaldehyde, urea-formaldehyde derivative, or both;

from about 0.01 to about 20 wt % lignosulfonate;

from about 0.01 to about 5.0 wt % viscosity modifier, a corrosion inhibitor, an anti-sludge agent, a chelating agent, a hydrogen sulfide scavenger, and combinations thereof; and

from about 37 to about 94.96 wt % water, wherein the amount of the components totals 100 wt. %.

13. The composition of claim 5 , wherein the composition comprises:

from 5.0 to 28 wt % hydrochloric acid;

from 0.01 to 5.0 wt % urea-formaldehyde, urea-formaldehyde derivative, or both;

from 0.01 to 20 wt % lignosulfonate;

from 0.01 to 5.0 wt % viscosity modifier; and

from 42 to 94.97 wt % water, wherein the amount of the components totals 100 wt. %.

14. The composition of claim 5 , wherein a composition comprises:

from 5.0 to 28 wt % hydrochloric acid;

from 0.01 to 5.0 wt % sulfuric acid;

from 0.01 to 20 wt % lignosulfonate;

from 0.01 to 5.0 wt % viscosity modifier; and

from 42 to 94.97 wt % water, wherein the amount of the components totals 100 wt. %.

15. The composition of claim 1 , wherein the retardation agent and the mineral acid comprise a molar ratio from about 0.1 to about 2.0.

16. A process for using a composition, comprising:

providing the composition of claim 1 ; and

depositing the composition downhole of a wellbore.

17. The process of claim 16 , wherein the composition comprises solid powders.

18. The process of claim 16 , wherein the composition comprises aqueous slurries.

19. The process of claim 16 , wherein the composition is pre-blended with concentrated mineral acid in an acid tank, a transportation vessel, a downhole flowline, or a combination thereof.

20. A process for using a composition, comprising:

providing the composition of claim 1 ; and

blending into an acidizing treatment fluid for the purpose of metal pickling.

Assignments (11)
RELEASE OF SECURITY INTEREST IN PATENTS (TERM LOAN) RECORDED AT REEL/FRAME 049741/0425 Recorded Mar 18, 2022
From: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
To: HEXION INC.
Reel/Frame 059435/0473 →
RELEASE OF SECURITY INTEREST IN PATENTS (ABL) RECORDED AT REEL/FRAME 049740/0770 Recorded Mar 18, 2022
From: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
To: HEXION INC.
Reel/Frame 059435/0490 →
SECURITY INTEREST Recorded Mar 18, 2022
From: HEXION INC.; HEXION INVESTMENTS INC.
To: GOLDMAN SACHS BANK USA, AS ADMINISTRATIVE AGENT
Reel/Frame 059436/0748 →
SECURITY INTEREST Recorded Mar 18, 2022
From: HEXION INC.; HEXION INVESTMENTS INC.
To: GOLDMAN SACHS BANK USA, AS ADMINISTRATIVE AGENT
Reel/Frame 059436/0823 →
SECURITY INTEREST Recorded Mar 18, 2022
From: HEXION INC.; HEXION INVESTMENTS INC.
To: ROYAL BANK OF CANADA, AS ADMINISTRATIVE AGENT
Reel/Frame 059436/0842 →
PATENT SECURITY INTEREST (ABL) Recorded Jul 12, 2019
From: HEXION INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 049740/0770 →
PATENT SECURITY INTEREST (TERM LOAN) Recorded Jul 12, 2019
From: HEXION INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 049741/0425 →
SECURITY INTEREST Recorded Feb 1, 2019
From: HEXION INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 048216/0628 →
SECURITY INTEREST Recorded Feb 1, 2019
From: HEXION INC.
To: WILMINGTON TRUST, NATIONAL ASSOCIATION
Reel/Frame 048216/0683 →
SECURITY INTEREST Recorded Jul 18, 2018
From: HEXION INC.
To: WILMINGTON TRUST COMPANY, AS COLLATERAL AGENT
Reel/Frame 046380/0855 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 13, 2018
From: JIANG, LI; BEETGE, JAN
To: HEXION INC.
Reel/Frame 046341/0405 →