IP Library Granted Patent US 10,960,656
Granted Patent B2
US 10,960,656 · App. 16/043,496 · Granted Mar 30, 2021

Negatively-working lithographic printing plate precursor and method

Inventors: Koji Hayashi (Tatebayashi, JP); James Russell Matz (Fairport, NY); Satoshi Ishii (Oura-gun, JP); Yoshiaki Sekiguchi (Kumagaya, JP); Masamichi Kamiya (Oura-gun, JP)
Assignee: EASTMAN KODAK COMPANY
B41C1/1016B41C1/1008G03F7/0045G03F7/027B41C2210/04B41C2210/22B41C2210/24
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Quick Facts
Patent No.
US 10,960,656
App. No.
16/043,496
Granted
Mar 30, 2021
Kind
B2
Abstract

A negative-working infrared radiation-sensitive lithographic printing plate precursor can be imaged and developed on-press to provide a lithographic printing plate. Such precursor has an initiator composition that contains compound A of Structure (I) and one or more compounds collectively as compound B of Structure (II) or Structure (III): wherein R 1 , R 2 , R 3 , R 4 , R 5 and R 6 are independently alkyl groups each having 3 to 6 carbon atoms; at least one of R 3 and R 4 is different from R 1 or R 2 ; the difference of total number of carbon atoms in R 1 and R 2 and the total number of carbon atoms in R 3 and R 4 is 0, 1, or 2; the difference of total number of carbon atoms in R 1 and R 2 and the total number of carbon atoms in R 5 and R 6 is 0, 1, or 2; and X 1 , X 2 and X 3 are the same or different anions.

Claims (40)

1. A negative-working, infrared radiation-sensitive lithographic printing plate precursor comprising:

a substrate having a hydrophilic surface, and

an infrared radiation-sensitive imageable layer that is disposed on the hydrophilic surface of the substrate, and comprises:

one or more free radically polymerizable compounds;

one or more infrared radiation absorbers;

an initiator composition that provides free radicals upon exposure of the infrared radiation-sensitive imageable layer to infrared radiation, the initiator composition comprising compound A and, one or more compounds collectively as compound B; and

optionally, a primary polymeric binder,

the molar ratio of compound A to compound B is from 20:80 to and including 80:20;

the sum of the weight of both compound A and compound B is at least 7 weight % and up to and including 15 weight %, based on the total dry weight of the infrared radiation-sensitive imageable layer; and

at least one infrared radiation absorber is a cyanine dye,

wherein Compound A includes one of the following cations, and each cation is present with a tetraphenyl borate anion:

and Compound B includes one of the following cations or a mixture thereof, and each cation is present with a tetraphenyl borate anion:

or a mixture of

2. The negative-working, infrared radiation-sensitive lithographic printing plate precursor of claim 1 , wherein at least one infrared radiation absorber is a cyanine dye comprising a tetraarylborate anion.

3. The negative-working, infrared radiation-sensitive lithographic printing plate precursor of claim 1 , wherein the primary polymeric binder is present in particulate form.

4. The negative-working, infrared radiation-sensitive lithographic printing plate precursor of claim 1 , wherein the primary polymeric binder is present and comprises recurring units comprising polyalkylene oxide segments and recurring units comprising pendant cyano groups.

5. A negative-working, infrared radiation-sensitive lithographic printing plate precursor that is on-press developable, comprising:

a substrate having a hydrophilic surface, and

an infrared radiation-sensitive imageable layer that is disposed on the hydrophilic surface of the substrate, and comprises:

one or more free radically polymerizable compounds;

one or more infrared radiation absorbers;

an initiator composition that provides free radicals upon exposure of the infrared radiation-sensitive imageable layer to infrared radiation, the initiator composition comprising compound A and one or more compounds collectively as compound B; and

optionally, a primary polymeric binder that is present in particulate form,

wherein:

Compound A includes one of the following cations, and each cation is present with a tetraphenyl borate anion:

and Compound B includes one of the following cations or mixture thereof, and each cation is present with a tetraphenyl borate anion:

or a mixture of

the molar ratio of compound A to compound B is from 20:80 to and including 80:20;

the sum of the weight of both compound A and compound B is at least 7 weight % and up to and including 15 weight %, based on the total dry weight of the infrared radiation-sensitive imageable layer; and

at least one infrared radiation absorber is a cyanine dye.

6. The negative-working, infrared radiation-sensitive lithographic printing plate precursor of claim 5 , wherein the primary polymeric binder is present in particulate form and comprises recurring units comprising polyalkylene oxide segments and recurring units comprising pendant cyano groups.

7. A method for providing a lithographic printing plate, the method comprising in sequence:

imagewise exposing the negative-working, infrared radiation-sensitive lithographic printing plate precursor of claim 1 to infrared radiation to provide an exposed precursor comprising exposed regions and non-exposed regions in the infrared radiation-sensitive imageable layer,

mounting the exposed precursor onto a lithographic printing press, and

removing the infrared radiation-sensitive imageable layer in the non-exposed regions using a lithographic ink, fountain solution, or both a lithographic ink and a fountain solution to provide a lithographic printing plate.

8. The method of claim 7 , wherein the negatively-working infrared radiation-sensitive lithographic printing plate precursor is defined by:

Compound A includes one of the following cations, and each cation is present with a tetraphenyl borate anion:

and Compound B includes one of the following cations or mixture thereof, and each cation is present with a tetraphenyl borate anion:

or a mixture of

9. The method of claim 7 , wherein the primary polymeric binder is present in particulate form in the infrared radiation-sensitive imageable layer, and the primary polymeric binder comprises recurring units comprising polyalkylene oxide segments and recurring units comprising pendant cyano groups.

Assignments (9)
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: ALTER DOMUS (US) LLC
Reel/Frame 056733/0681 →
NOTICE OF SECURITY INTERESTS Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: BANK OF AMERICA, N.A., AS AGENT
Reel/Frame 056984/0001 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: ALTER DOMUS (US) LLC
Reel/Frame 056734/0233 →
INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Mar 4, 2021
From: EASTMAN KODAK COMPANY
To: ALTER DOMUS (US) LLC
Reel/Frame 056734/0001 →
RELEASE OF SECURITY INTEREST Recorded Jul 30, 2019
From: JP MORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; PFC, INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; KODAK IMAGING NETWORK, INC.; KODAK PORTUGUESA LIMITED; KODAK REALTY, INC.; LASER PACIFIC MEDIA CORPORATION; PAKON, INC.; QUALEX, INC.; KODAK PHILIPPINES, LTD.; NPEC, INC.; CREO MANUFACTURING AMERICA LLC; KODAK AVIATION LEASING LLC
Reel/Frame 049901/0001 →
RELEASE OF SECURITY INTEREST Recorded Jul 22, 2019
From: JP MORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: QUALEX, INC.; EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; FPC, INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; KODAK IMAGING NETWORK, INC.; KODAK PORTUGUESA LIMITED; KODAK REALTY, INC.; LASER PACIFIC MEDIA CORPORATION; PAKON, INC.; KODAK PHILIPPINES, LTD.; NPEC, INC.; CREO MANUFACTURING AMERICA LLC; KODAK AVIATION LEASING LLC
Reel/Frame 050239/0001 →
SECURITY INTEREST Recorded Sep 13, 2018
From: EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; FPC INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; LASER-PACIFIC MEDIA CORPORATION; QUALEX INC.; KODAK PHILIPPINES, LTD.; NPEC INC.
To: JP MORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 046860/0842 →
SECURITY INTEREST Recorded Sep 13, 2018
From: EASTMAN KODAK COMPANY; FAR EAST DEVELOPMENT LTD.; FPC INC.; KODAK (NEAR EAST), INC.; KODAK AMERICAS, LTD.; LASER-PACIFIC MEDIA CORPORATION; QUALEX INC.; KODAK PHILIPPINES, LTD.; NPEC INC.
To: BANK OF AMERICA N.A., AS AGENT
Reel/Frame 046860/0721 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 24, 2018
From: HAYASHI, KOJI; MATZ, JAMES RUSSELL; ISHII, SATOSHI; SEKIGUCHI, YOSHIAKI; KAMIYA, MASAMICHI
To: EASTMAN KODAK COMPANY
Reel/Frame 046441/0695 →