Method for producing multilayer member
A method for producing a multilayer member having a first member containing a crystallizable thermoplastic resin, an adhesion layer, and a second member includes performing a dry treatment on a surface of the first member containing a crystallizable thermoplastic resin so as to satisfy conditions A and B, applying an adhesive to the surface of the first member to form an adhesive layer on the surface, and adhering the second member to the adhesive layer. (A) The ultimate temperature of the first member is lower than the peak temperature of endothermic peak obtained by DSC of the crystallizable thermoplastic resin. (B) The high temperature holding time of the first member is less than 3.0 seconds, which is when the first member is continuously held at a temperature not lower than a temperature at the starting point of the endothermic peak obtained by DSC of the crystallizable thermoplastic resin.
1. A method for producing a multilayer member having a first member containing a crystallizable thermoplastic resin, an adhesion layer, and a second member in this order, the method comprising:
a surface treatment step of performing a dry treatment on a surface of the first member containing a crystallizable thermoplastic resin to satisfy conditions A and B;
an adhesive application step of applying an adhesive to the surface of the first member subjected to the dry treatment without a primer composition, to form an adhesive layer on the surface; and
an adhering step of adhering a surface of the second member directly to the adhesive layer;
Condition A: an ultimate temperature of the first member is lower than a peak temperature of endothermic peak obtained by differential scanning calorimetry of the crystallizable thermoplastic resin contained in the first member; and
Condition B: a high temperature holding time of the first member is less than 0.5 seconds, wherein a high temperature holding time of the first member is a time when the first member is continuously held at a temperature not lower than a temperature at a starting point of the endothermic peak obtained by differential scanning calorimetry of the crystallizable thermoplastic resin contained in the first member.
2. The method for producing a multilayer member according to claim 1 , wherein the second member is a coated member.
3. The method for producing a multilayer member according to claim 1 , wherein the dry treatment is at least one selected from the group consisting of a corona treatment, a plasma treatment, a flame treatment, ITRO treatment, an UV treatment, and an excimer treatment.
4. The method for producing a multilayer member according to claim 1 , wherein the first member is a composite material containing a polyolefin resin as the crystallizable thermoplastic resin and an inorganic substance.
5. The method for producing a multilayer member according to claim 1 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
6. The method for producing a multilayer member according to claim 1 , wherein in the dry treatment, the temperature of the first member is measured by using a contact thermocouple, an ink to be discolored by heat, a seal to be discolored by heat, a thermography, or a radiation thermometer.
7. The method for producing a multilayer member according to claim 1 , further comprising a surface treatment step of performing a dry treatment on a surface of the second member before the adhering step to satisfy conditions A2 and B2,
wherein the second member contains a crystallizable thermoplastic resin, and in the bonding step, the surface of the second member in which the surface treatment is performed is bonded to the adhesive layer;
Condition A2: an ultimate temperature of the second member is lower than the peak temperature of endothermic peak obtained by differential scanning calorimetry of the crystallizable thermoplastic resin contained in the second member; and
Condition B2: a high temperature holding time of the second member is less than 3.0 seconds, where a high temperature holding time of the second member is a time when the second member is continuously held at a temperature not lower than a temperature at a starting point of the endothermic peak obtained by differential scanning calorimetry of the crystallizable thermoplastic resin contained in the second member.
8. The method for producing a multilayer member according to claim 2 , wherein the dry treatment is at least one selected from the group consisting of a corona treatment, a plasma treatment, a flame treatment, ITRO treatment, an UV treatment, and an excimer treatment.
9. The method for producing a multilayer member according to claim 2 , wherein the first member is a composite material containing a polyolefin resin as the crystallizable thermoplastic resin and an inorganic substance.
10. The method for producing a multilayer member according to claim 3 , wherein the first member is a composite material containing a polyolefin resin as the crystallizable thermoplastic resin and an inorganic substance.
11. The method for producing a multilayer member according to claim 8 , wherein the first member is a composite material containing a polyolefin resin as the crystallizable thermoplastic resin and an inorganic substance.
12. The method for producing a multilayer member according to claim 2 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
13. The method for producing a multilayer member according to claim 3 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
14. The method for producing a multilayer member according to claim 4 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
15. The method for producing a multilayer member according to claim 8 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
16. The method for producing a multilayer member according to claim 9 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
17. The method for producing a multilayer member according to claim 10 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
18. The method for producing a multilayer member according to claim 11 , wherein the adhesive is at least one selected from the group consisting of a urethane-based adhesive, an epoxy-based adhesive, a modified silicone-based adhesive, and an acrylic adhesive.
19. The method for producing a multilayer member according to claim 2 , wherein in the dry treatment, the temperature of the first member is measured by using a contact thermocouple, an ink to be discolored by heat, a seal to be discolored by heat, a thermography, or a radiation thermometer.
20. The method for producing a multilayer member according to claim 3 , wherein in the dry treatment, the temperature of the first member is measured by using a contact thermocouple, an ink to be discolored by heat, a seal to be discolored by heat, a thermography, or a radiation thermometer.