IP Library Granted Patent US 10,961,355
Granted Patent B2
US 10,961,355 · App. 16/072,673 · Granted Mar 30, 2021

Aqueous solution of cellulose ether acetate

Inventors: Oliver Petermann (Hamburg, DE); Jin Zhao (Midland, MI)
Assignee: Nutrition & Biosciences USA 1, LLC
C08J3/07A61K9/4816A61K9/5042A61K47/38C08L1/12A61K9/2866C08J2301/12C08L2201/54
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Quick Facts
Patent No.
US 10,961,355
App. No.
16/072,673
Granted
Mar 30, 2021
Kind
B2
Abstract

An aqueous composition comprising a cellulose ether acetate being at least partially dissolved in an aqueous liquid is produced in a process, wherein an aqueous liquid is mixed with a cellulose ether acetate having a degree of substitution of acetyl groups, DSAc, of from 0.05 to 0.75 and the temperature of the mixture of the cellulose ether acetate and the aqueous liquid is set to less than 10 C to at least partially dissolve the cellulose ether acetate in the aqueous liquid.

Claims (19)

1. A process for producing an aqueous composition comprising a cellulose ether acetate being at least partially dissolved in an aqueous liquid, wherein the cellulose ether acetate comprises acetyl groups as the only ester groups and the process comprises the step of

mixing an aqueous liquid with a cellulose ether acetate having a degree of substitution of acetyl groups, DSAc, of from 0.05 to 0.75 and

setting the temperature of the mixture of the cellulose ether acetate and the aqueous liquid to less than 10° C. to at least partially dissolve the cellulose ether acetate in the aqueous liquid.

2. The process of claim 1 wherein the cellulose ether acetate has a degree of substitution of methyl groups, DSM, of from 1.60 to 2.05.

3. The process of claim 1 wherein the temperature of the mixture of the cellulose ether acetate and the aqueous liquid is set to less than 5° C.

4. The process of claim 1 wherein the cellulose ether acetate has a degree of substitution of acetyl groups, DSAc, of from 0.25 to 0.70.

5. The process of claim 1 wherein after at least partial dissolution of the cellulose ether acetate in the aqueous liquid at a temperature of less than 10° C. the temperature of the aqueous composition is increased to not more than 25° C.

6. The process of claim 1 wherein the cellulose ether acetate is a hydroxypropyl methylcellulose acetate.

7. The process of claim 1 wherein the produced aqueous composition comprises at least 2.0 weight percent hydroxypropyl methylcellulose acetate dissolved in the aqueous liquid.

8. A process for manufacturing capsule shells comprising the steps of

producing, according to the process of claim 1 , an aqueous composition comprising a cellulose ether acetate at least partially dissolved in an aqueous liquid, and

contacting dipping pins having a higher temperature than the aqueous composition with the aqueous composition or with the portion of the aqueous composition wherein cellulose ether acetate is dissolved.

9. A process for coating dosage forms comprising the steps of

producing, according to the process of claim 1 , an aqueous composition comprising a cellulose ether acetate at least partially dissolved in an aqueous liquid, and

contacting dosage forms with the aqueous composition or with the portion of the aqueous composition wherein cellulose ether acetate is dissolved.

10. A process for preparing a solid dispersion of an active ingredient in a cellulose ether acetate comprising the steps of

producing, according to the process of claim 1 , an aqueous composition comprising a cellulose ether acetate at least partially dissolved in an aqueous liquid,

dissolving an active ingredient in the aqueous composition or in the portion of the aqueous composition wherein cellulose ether acetate is dissolved, and

drying the aqueous composition or the portion of the aqueous composition wherein cellulose ether acetate and active ingredient are dissolved to produce the solid dispersion of an active ingredient in a cellulose ether acetate.

Assignments (4)
CHANGE OF LEGAL ENTITY Recorded Nov 28, 2020
From: DDP SPECIALTY ELECTRONIC MATERIALS US, INC.
To: DDP SPECIALTY ELECTRONIC MATERIALS US, LLC.
Reel/Frame 054530/0384 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2020
From: DOW GLOBAL TECHNOLOGIES LLC
To: THE DOW CHEMICAL COMPANY
Reel/Frame 054531/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2020
From: THE DOW CHEMICAL COMPANY
To: DDP SPECIALTY ELECTRONIC MATERIALS US, INC.
Reel/Frame 054533/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 28, 2020
From: DDP SPECIALTY ELECTRONIC MATERIALS US, LLC.
To: NUTRITION & BIOSCIENCES USA 1, LLC
Reel/Frame 054533/0575 →