IP Library Granted Patent US 10,457,674
Granted Patent B2
US 10,457,674 · App. 16/073,355 · Granted Oct 29, 2019

Chemical compounds

Inventors: Niall Andrew Anderson (Stevenage, GB); Nicholas Paul Barton (Stevenage, GB); Sebastien Andre Campos (Stevenage, GB); Edward Paul Cannons (Stevenage, GB); Anthony William James Cooper (Stevenage, GB); Kenneth David Down (Stevenage, GB); Kevin James Doyle (Saffron Walden, GB); Julie Nicole Hamblin (Stevenage, GB); Graham George Adam Inglis (Stevenage, GB); Armelle Le Gall (Stevenage, GB); Vipulkumar Kantibhai Patel (Stevenage, GB); Simon Peace (Stevenage, GB); Andrew Sharpe (Saffron Walden, GB); Gemma Victoria White (Stevenage, GB)
Assignee: GlaxoSmithKline Intellectual Property Development Limited
C07D413/14A61P11/06A61P15/08A61P25/24A61P25/28A61P37/08C07D213/76
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,457,674
App. No.
16/073,355
Granted
Oct 29, 2019
Kind
B2
Abstract

The invention is directed to certain novel compounds. Specifically, the invention is directed to compounds of formula (I): and salts thereof. The compounds of the invention are inhibitors of kinase activity, in particular PI3-kinase activity.

Claims (54)

1. A compound of formula (I):

wherein

R 1 is C 1-6 alkoxy or —N(C 1-6 alkyl) 2 ;

R 2 is hydrogen or C 1-6 alkyl optionally substituted by —C(O)OC 1-6 alkyl or —OC(O)C 1-6 alkyl;

R 3 , R 4 , R 5 and R 6 are each independently selected from hydrogen and halogen;

R 7 and R 8 are each independently C 1-6 alkyl, or

R 7 and R 8 , together with the nitrogen atom to which they are attached, are linked to form a 5- or 6-membered heterocyclyl wherein the 5- or 6-membered heterocyclyl optionally contains a further nitrogen atom and is optionally substituted by C 3-6 cycloalkyl, 4- to 6-membered heterocyclyl containing one or two heteroatoms independently selected from oxygen and nitrogen, or C 1-6 alkyl wherein the C 1-6 alkyl is optionally substituted by hydroxy or C 1-6 alkoxy, or

R 7 and R 8 , together with the nitrogen atom to which they are attached, are linked to form a 5- or 6-membered heterocyclyl wherein the 5- or 6-membered heterocyclyl contains an oxygen atom and is optionally substituted by one or two substituents independently selected from C 1-6 alkyl; or a salt thereof.

2. A compound according to claim 1 , or a salt thereof, wherein R 1 is C 1-6 alkoxy.

3. A compound according to claim 1 , or a salt thereof, wherein R 2 is hydrogen.

4. A compound according to claim 1 , or a salt thereof, wherein R 3 , R 4 , R 5 and R 6 are each independently selected from hydrogen and fluoro.

5. A compound according to claim 1 , or a salt thereof, wherein R 7 and R 8 , together with the nitrogen atom to which they are attached, are linked to form a 5- or 6-membered heterocyclyl wherein the 5- or 6-membered heterocyclyl optionally contains a further nitrogen atom and is optionally substituted by C 3-6 cycloalkyl, 4- to 6-membered heterocyclyl containing one or two heteroatoms independently selected from oxygen and nitrogen, or C 1-6 alkyl wherein the C 1-6 alkyl is optionally substituted by hydroxy or C 1-6 alkoxy.

6. A compound which is:

N-(2-(2-fluoro-4((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-(tert-butyl)piperazin-1-yl)methyl)-2-fluorophenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((dimethylamino)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(3-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-(tert-butyl)piperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-cyclobutylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2,6-difluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-(sec-butyl)piperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-(pyrrolidin-1-ylmethyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(3-fluoro-4-(pyrrolidin-1-ylmethyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(3,5-difluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

2-methoxy-5-morpholino-N-(2-(4-((4-(oxetan-3-yl)piperazin-1-yl)methyl)phenyl)pyridin-4-yl)pyridine-3-sulfonamide;

N-(2-(2,3-difluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-((4-(oxetan-3-yl)piperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-cyclobutylpiperazin-1-yl)methyl)-2-fluorophenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2,5-difluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-((4-(2-methoxyethyl)piperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-((3-methylpyrrolidin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4((2-methylpyrrolidin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-(piperidin-1-ylmethyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-((4-(2-hydroxypropan-2-yl)piperidin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-(((cis)-2,6-dimethylmorpholino)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

2-methoxy-5-morpholino-N-(2-(4-(morpholinomethyl)phenyl)pyridin-4-yl)pyridine-3-sulfonamide;

N-(2-(2-fluoro-4-(piperazin-1-ylmethyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

2-(dimethylamino)-N-(2-(2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-(tert-butyl)piperazin-1-yl)methyl)-2-fluorophenyl)pyridin-4-yl)-2-(dimethylamino)-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-((4-(tert-butyl)piperazin-1-yl)methyl)-2-fluorophenyl)pyridin-4-yl)-2-methoxy-N-methyl-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-N-methyl-5-morpholinopyridine-3-sulfonamide;

N-ethyl-N-(2-(2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholino-N-propylpyridine-3-sulfonamide;

N-(2-(2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-N-isopropyl-2-methoxy-5-morpholinopyridine-3-sulfonamide;

ethyl 2-(N-(2-(2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamido)acetate;

(N-(2-(2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamido)methyl pivalate; or

N-(2-(5-chloro-2-fluoro-4-((4-isopropylpiperazin-1-yl)methyl)phenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-(((2S,6R)-2,6-dimethylmorpholino)methyl)-2-fluorophenyl)pyridin-4-yl)-2-methoxy-5-morpholinopyridine-3-sulfonamide;

N-(2-(4-(((2S,6R)-2,6-dimethylmorpholino)methyl)-2-fluorophenyl)pyridin-4-yl)-2-ethoxy-5-morpholinopyridine-3-sulfonamide; or a salt thereof.

7. A compound which is:

or a salt thereof.

8. A compound according to claim 1 in the form of a pharmaceutically acceptable salt thereof.

9. A pharmaceutical composition comprising a compound as defined in claim 1 , or a pharmaceutically acceptable salt thereof, and one or more pharmaceutically acceptable excipients.

Assignments (3)
CHANGE OF ADDRESS Recorded Oct 8, 2025
From: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
To: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
Reel/Frame 073032/0390 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2018
From: ANDERSON, NIALL ANDREW; BARTON, NICHOLAS PAUL; CAMPOS, SEBASTIEN ANDRE; CANNONS, EDWARD PAUL; COOPER, ANTHONY WILLIAM JAMES; DOWN, KENNETH DAVID; HAMBLIN, JULIE NICOLE; INGLIS, GRAHAM GEORGE ADAM; LE GALL, ARMELLE; PATEL, VIPULKUMAR KANTIBHAI; PEACE, SIMON; WHITE, GEMMA VICTORIA
To: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
Reel/Frame 047534/0038 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2018
From: DOYLE, KEVIN JAMES; SHARPE, ANDREW; BIOFOCUS DPI LIMITED
To: GLAXOSMITHKLINE INTELLECTUAL PROPERTY DEVELOPMENT LIMITED
Reel/Frame 047534/0045 →
Priority Claims (1)
GB 1602527.2 · Feb 12, 2016 · national
Continuity (1)
Related Publication 20190040051A1 · Feb 7, 2019