IP Library Granted Patent US 10,918,972
Granted Patent B2
US 10,918,972 · App. 16/073,394 · Granted Feb 16, 2021

Methods for the separation of at least one emulsion by applying an electrical field and device for carrying out said method

Inventors: Andreas Leitner (Freistadt, AT); Michael Schadenböck (Enns, AT); Udo Muster (Salzburg, AT)
Assignee: Borealis AG
B01D17/06B03C11/00C10G33/02B03C2201/02
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Quick Facts
Patent No.
US 10,918,972
App. No.
16/073,394
Granted
Feb 16, 2021
Kind
B2
Abstract

Disclosed is a method for the break-up of at least one emulsion and separation of the light and heavy phase with at least an de-emulsification rate of more than 9% in only one apparatus within less than 5 min by applying at least one time dependent electrical field. The electrical field is a high frequency singular alternating current field with an electrical field strength between 2,000 and 100,000 V/m and a frequency between 12,000 Hz and 200,000 Hz. The present invention relates furthermore to a method for the treatment of at least one emulsion by applying at least one direct current field and at least one high frequency alternating current field.

Claims (10)

1. A method for the separation of at least one liquid/liquid (L/L) emulsion with a water content of up to 70 mass % comprising applying at least one time dependent electrical field,

wherein

the at least one electrical field is a singular alternating current (AC) field with an electrical field strength between 2,000 and 100,000 V/m and a frequency (HF) between >10,000 Hz and 200,000 Hz, and

wherein separation of the at least one L/L emulsion performed with a de-emulsification rate of at least 95% is achieved in less than 5 minutes.

2. The method according to claim 1 , wherein the at least one AC-field is applied with an electrical field strength between 4,000 and 70,000 V/m.

3. The method according to claim 1 , wherein the at least one AC-field is applied with a frequency between 12,000 and 150,000 Hz.

4. The method according to claim 1 , wherein the emulsion to be separated is a phenolic water emulsion of the Hock-synthesis with an equimolar Phenol/Acetone-ratio and water contents up to 70 wt. %.

5. The method according to claim 1 , wherein the at least one AC-field is applied with an electrical field strength between 30,000 and 50,000 V/m and a frequency between 16,000 and 40,000 Hz.

6. The method according to claim 1 , wherein separation of the at least one L/L emulsion performed with a de-emulsification rate of at least 95% is achieved in less than 3 minutes.

7. The method according to claim 1 , wherein separation of the at least one L/L emulsion performed with a de-emulsification rate of at least 95% is achieved in less than 2 minutes.

Assignments (1)
CHANGE OF ADDRESS Recorded Feb 23, 2022
From: BOREALIS AG
To: BOREALIS AG
Reel/Frame 059219/0949 →