IP Library Granted Patent US 10,584,304
Granted Patent B2
US 10,584,304 · App. 16/101,256 · Granted Mar 10, 2020

Systems and methods for extracting oil from plant material

Inventors: Blake A. Schnell (Harrisburg, SD); Kristin M. Calar (Sioux Falls, SD); John C. Keeler (Sioux Falls, SD); Matthew J. Rindsig (Harrisburg, SD); Benjamin G. Oster (Brandon, SD); Brett A. Flittie (Harrisburg, SD); Steven T. Bly (Sioux Falls, SD)
Assignee: POET RESEARCH, INC.
C11B13/00C11B7/005C12P7/06C12P7/64C12Y302/01001C11B1/04
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Quick Facts
Patent No.
US 10,584,304
App. No.
16/101,256
Granted
Mar 10, 2020
Kind
B2
Abstract

Disclosed are methods and systems for recovering oil from processed plant materials and by-products formed during a milling process used for producing ethanol.

Claims (39)

1. A method of extracting oil from a wet cake, wherein the method comprises:

(a) providing a wet cake comprising:

a total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the wet cake;

(b) applying pressure to the wet cake to separate the wet cake into a liquid fraction and a solids fraction; and

(c) recovering or separating oil from the liquid fraction.

2. The method of claim 1 , wherein applying pressure comprises mechanically pressing the wet cake against a screen to separate the wet cake into a liquid fraction and a solid fraction.

3. The method of claim 1 , wherein applying pressure comprises mechanically passing the wet cake through a screw press to separate the wet cake into a liquid fraction and a solid fraction.

4. The method of claim 1 , wherein the average particle size of the wet cake is reduced prior to applying pressure.

5. The method of claim 1 , wherein the applying pressure comprises applying pressure from about 200-600 psi.

6. The method of claim 1 , further comprising heating the wet cake from about 21° C. (70° F.) to about 100° C. (212° F.).

7. The method of claim 1 , further comprising prior to step (b), treating the wet cake with one or more enzymes.

8. The method of claim 7 , wherein the one or more enzymes are selected from amylase enzymes, one or more cellulase enzymes, one or more protease enzymes, and combinations thereof.

9. The method of claim 1 , wherein the wet cake is obtained from ground corn ethanol process.

10. A system for extracting oil from a wet cake, wherein the system comprises:

a) a source of a wet cake comprising

a total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the wet cake;

b) an oil liberation system in fluid communication with the source of the wet cake, wherein the oil liberation system is configured to apply pressure to the wet cake to separate the wet cake into a liquid fraction and a solid fraction;

and

(c) an oil recovery or separation system in fluid communication with the oil liberation system to receive the liquid fraction, wherein the oil recovery or separation system is configured to recover or separate oil from the liquid fraction.

11. A method of extracting oil from a whole stillage or beer, wherein the method comprises:

a) providing whole stillage or beer

(b) separating the whole stillage or beer into a first liquid fraction and a first solids fraction, wherein the first solids fraction has a total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the first solids fraction;

(c) pressing the first solids fraction to separate the first solids fraction into a second liquid fraction and a second solids fraction and to move oil into the second liquid fraction; and

(d) recovering or separating oil from the second liquid fraction.

12. The method of claim 11 , further comprising prior to step cc), exposing the first solid fraction to a gas pressure from about 200-600 psi and/or heating from about 21° C. (70° F.) to about 100° C. (212° F.).

13. The method of claim 11 , wherein separating the whole stillage or beer comprises contacting the whole stillage or beer against a gravity screen.

14. The method of claim 11 , further comprising adding an aqueous carrier to the first solids fraction to provide the total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the first solids fraction.

15. The method of claim 14 , wherein the aqueous carrier comprises thin stillage, ethanol, or combinations thereof.

16. The method of claim 14 , wherein the aqueous carrier comprises at least 50 percent water based on the total volume of the carrier.

17. The method of claim 14 , wherein the aqueous carrier does not include added exogenous organic solvent.

18. The method of claim 11 , further comprising:

(a) adding an aqueous carrier to the second solids fraction to provide a total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the second solids fraction;

(b) pressing the second solids fraction to separate the second solids fraction into a third liquid fraction and a third solids fraction and to move oil into the third liquid fraction; and

(c) recovering or separating oil from the third liquid fraction.

19. The method of claim 18 , wherein pressing the first solids fraction occurs in a first screw press and pressing the second solids fraction occurs in a second screw press.

20. The method of claim 1 , wherein the solids fraction is a first solids fraction and the liquid fraction is a first liquid fraction, and wherein the first solids fraction comprises a total solids content in a range from 15 to less than 35% (wt/wt) based on the total weight of the first solids fraction and further comprising:

(a) applying pressure to the first solids fraction to separate into a second liquid fraction and a second solids fraction;

(b) recovering or separating oil from the second liquid fraction; and

(c) repeating steps (a) to (b).

Assignments (5)
SECURITY INTEREST Recorded Apr 3, 2020
From: POET RESEARCH, INC.
To: COBANK, ACB, AS ADMINISTRATIVE AGENT
Reel/Frame 052312/0801 →
SECURITY INTEREST Recorded Apr 2, 2020
From: POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 052295/0712 →
RELEASE OF SECURITY INTEREST RECORDED AT REEL/FRAME 47875/0306 Recorded Apr 2, 2020
From: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
To: POET NUTRITION, INC.; POET RESEARCH, INC.
Reel/Frame 052303/0267 →
SECURITY INTEREST Recorded Dec 31, 2018
From: POET NUTRITION, INC.; POET RESEARCH, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 047875/0306 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 30, 2018
From: SCHNELL, BLAKE A.; CALAR, KRISTIN M.; KEELER, JOHN C.; RINDSIG, MATTHEW J.; OSTER, BENJAMIN G.; FLITTIE, BRETT A.; BLY, STEVEN T.
To: POET RESEARCH, INC.
Reel/Frame 047634/0425 →