IP Library Granted Patent US 10,583,392
Granted Patent B2
US 10,583,392 · App. 16/107,535 · Granted Mar 10, 2020

Decontamination of sulfur contaminants from a vessel

Inventor: Stephen D. Matza (Sugar Land, TX)
Assignee: United Laboratories International, LLC
B01D53/52C02F1/72B01D2251/10B01D2252/20436B01D2255/20738C02F1/725C02F2101/101C02F2103/365C02F2209/02C02F2301/046C02F2303/02C02F2305/02
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Quick Facts
Patent No.
US 10,583,392
App. No.
16/107,535
Granted
Mar 10, 2020
Kind
B2
Abstract

A method for treating sulfur contaminants is provided. The method comprises introducing a methylmorpholine-N-oxide solution to a vessel, wherein the vessel comprises a water layer and a gas layer, wherein the water layer and the gas layer comprise the hydrogen sulfide; introducing methylmorpholine-N-oxide into the water layer; and treating the water layer by allowing the methylmorpholine-N-oxide to react with the hydrogen sulfide.

Claims (11)

1. A method for removing hydrogen sulfide, comprising:

(A) introducing a methylmorpholine-N-oxide solution to a vessel, wherein the vessel comprises a water layer and a gas layer, wherein the water layer and the gas layer comprise the hydrogen sulfide;

(B) introducing methylmorpholine-N-oxide into the gas layer;

(C) introducing steam to the vessel, wherein steam removes at least a portion of the hydrogen sulfide from the water layer;

(D) allowing the steam comprising at least a portion of hydrogen sulfide from the water layer to evaporate into the gas layer;

(E) adjusting a hydrogen sulfide rate of evaporation by increasing the vessel temperature;

(F) treating the gas layer by allowing the methylmorpholine-N-oxide to react with the hydrogen sulfide; and

(G) treating the water layer by reducing a temperature of the gas layer to a temperature below the boiling point of methylmorpholine-N-oxide thereby allowing the methylemorpholine-N-oxide to condense into the water layer.

2. The method of claim 1 , further comprising allowing the hydrogen sulfide in the water layer to react with the methylmorpholine-N-oxide.

3. The method of claim 1 , wherein the treating the water layer comprises converting the hydrogen sulfide to elemental sulfur.

4. The method of claim 3 , wherein the elemental sulfur is removed from the vessel.

Assignments (4)
MERGER Recorded Mar 15, 2025
From: CR3 ZYMEFLOW, INC.
To: ZYMEFLOW, INC.
Reel/Frame 070523/0169 →
MERGER Recorded Mar 13, 2025
From: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
To: CR3 ZYMEFLOW, INC.
Reel/Frame 070508/0396 →
MERGER Recorded Mar 12, 2025
From: UNITED LABORATORIES INTERNATIONAL, LLC
To: TRISTAR GLOBAL ENERGY SOLUTIONS, INC.
Reel/Frame 070491/0243 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 30, 2019
From: MATZA, STEPHEN D.
To: UNITED LABORATORIES INTERNATIONAL. LLC
Reel/Frame 050225/0753 →
Cited By (1)
US 12,503,657