IP Library Granted Patent US 10,557,845
Granted Patent B2
US 10,557,845 · App. 16/114,108 · Granted Feb 11, 2020

Flavors, flavor modifiers, tastants, taste enhancers, umami or sweet tastants, and/or enhancers and use thereof

Inventors: Catherine Tachdjian (San Diego, CA); Andrew P. Patron (San Marcos, CA); Sara L. Adamski-Werner (San Diego, CA); Farid Bakir (San Diego, CA); Qing Chen (San Diego, CA); Vincent Darmohusodo (Encinitas, CA); Stephen Terrence Hobson (San Marcos, CA); Xiaodong Li (San Diego, CA); Ming Qi (Shanghai, CN); Daniel H. Rogers (San Diego, CA); Marketa Rinnova (San Diego, CA); Guy Servant (San Diego, CA); Xiao-Qing Tang (San Diego, CA); Mark Zoller (La Jolla, CA); David Wallace (San Diego, CA); Amy Xing (San Diego, CA); Klaus Gubernator (Del Mar, CA)
Assignee: Firmenich Incorporated
G01N33/543A23L2/56A23L27/202A23L27/203A23L27/2054A23L27/88A61K8/4973A61K8/55A61K47/22A61K47/24C07C233/65C07C235/54C07C275/30C07C275/34C07D209/08C07D209/42C07D213/40C07D213/81C07D213/85C07D215/48C07D217/06C07D231/14C07D261/18C07D263/56C07D271/12C07D275/03C07D277/64C07D285/135C07D307/52C07D307/68C07D307/79C07D307/82C07D307/84C07D317/68C07D333/24C07D333/38C07D401/04C07D405/12C07D409/12C07D417/12C07F9/65517G01N33/5041G01N33/566G01N33/74A23V2002/00G01N2333/726
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Quick Facts
Patent No.
US 10,557,845
App. No.
16/114,108
Granted
Feb 11, 2020
Kind
B2
Abstract

The present invention relates to the discovery that certain non-naturally occurring, non-peptide amide compounds and amide derivatives, such as oxalamides, ureas, and acrylamides, are useful flavor or taste modifiers, such as a flavoring or flavoring agents and flavor or taste enhancer, more particularly, savory (the “umami” taste of monosodium glutamate) or sweet taste modifiers,—savory or sweet flavoring agents and savory or sweet flavor enhancers, for food, beverages, and other comestible or orally administered medicinal products or compositions.

Claims (38)

1. A method for modulating the taste of an ingestible composition comprising: combining the ingestible composition with at least a savory flavor modulating amount of an amide compound, or a comestibly acceptable salt thereof, having the following formula, so as to form a taste modified ingestible composition:

wherein:

A is phenyl;

m is 1 or 2;

each R 1′ is independently selected from fluoro, chloro, SCH 3 , SEt, methyl, ethyl, isopropyl, vinyl, , methoxy, ethoxy, isopropoxy, and trifluoromethoxy;

i) R 2 is a C 3 -C 10 branched alkyl optionally substituted with one to two substituents each independently selected fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy; or

ii) R 2 is a 1-(1,2,3,4) tetrahydronapthalene ring or an 2,3-dihydro-1H-indene ring having the following formula:

wherein n is 1, 2, or 3, and each R 2′ can be bonded to either the aromatic or non-aromatic ring and is independently selected from hydrogen, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy groups; or

iii) R 2 is a cycloalkyl ring having 5 to 8 ring carbon atoms optionally substituted with one to four substituents independently selected from fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy;

wherein the amide compound has a molecular weight of 500 grams per mole or less; and

wherein the modified ingestible composition is a food for human or animal consumption.

2. The method of claim 1 , wherein the modified ingestible composition is a food for human or animal consumption.

3. The method of claim 1 , wherein the modified ingestible composition is a food for human consumption.

4. The method of claim 1 , wherein the modified ingestible composition is a pharmaceutical composition for oral administration.

5. The method of claim 1 , wherein the modified ingestible composition is an oral hygiene product.

6. The method of claim 1 , wherein the amide compound is present in the modified ingestible composition at a concentration from about 0.01 ppm to about 30 ppm.

7. The method of claim 1 , wherein the amide compound is present in the modified ingestible composition in a concentration from about 0.05 ppm to about 15 ppm.

8. The method of claim 1 , wherein the amide compound is present in the modified ingestible composition in a concentration from about 0.1 ppm to about 5 ppm.

9. The method of claim 1 , wherein the amide compound is present in the modified ingestible composition in a concentration from about 0.1 ppm to about 3 ppm.

10. The method of claim 1 , wherein m is 1.

11. The method of claim 1 , wherein m is 2.

12. The method of claim 1 , wherein each R 1′ is independently selected from fluoro, chloro, SCH 3 , SEt, methyl, ethyl, isopropyl, vinyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

13. The method of claim 1 , wherein R 2 is a C 3 -C 10 branched alkyl optionally substituted with one to four substituents independently selected from fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, trifluoromethyl, methoxy.

14. The method of claim 1 , wherein R 2 is a C 3 -C 10 branched alkyl optionally substituted with one or two substituents independently selected from hydroxy, fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

15. The method of claim 1 , wherein R 2 is a cycloalkyl ring having 5 to 8 ring carbon atoms optionally substituted with one to two substituents independently selected from fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

16. The method of claim 1 , wherein R 2 is a cycloalkyl ring having 5 to 8 ring carbon atoms optionally substituted with one to four substituents independently selected from methyl, ethyl, isopropyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

17. The method of claim 1 , wherein R 2 is a 1-(1,2,3,4)tetrahydronapthalene ring or an 2,3-dihydro-1H-indene ring having the following formula:

wherein each R 2′ can be bonded to either the aromatic or non-aromatic ring and is independently selected from hydrogen, fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy groups.

18. The method of claim 1 , wherein R 2 has the following formula:

wherein each R 2′ are independently selected from the group consisting of hydrogen, fluoro, chloro, COOCH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy.

19. The method of claim 1 , wherein (R 1′ ) m — A is

wherein m is 1, 2, or 3, and each R 1′ is independently selected from fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, vinyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy and wherein

i) R 2 is a C 3 -C 10 branched alkyl optionally substituted with one or two substituents each independently selected from fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy; or

ii) R 2 is a 1-(1,2,3,4) tetrahydronapthalene ring or an 2,3-dihydro-1H-indene ring having the following formula:

wherein n is 1, 2, or 3, and each R 2′ can be bonded to either the aromatic or non-aromatic ring and is independently selected from hydrogen, fluoro, chloro, NH 2 , NHCH 3 , N(CH 3 ) 2 , CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, vinyl, trifluoromethyl, methoxy, ethoxy isopropoxy, and trifluoromethoxy groups; or

iii) R 2 is a cycloalkyl ring having 5 to 8 ring carbon atoms optionally substituted with one to four substituents independently selected from fluoro, chloro, CO 2 CH 3 , SCH 3 , SEt, methyl, ethyl, isopropyl, trifluoromethyl, methoxy, ethoxy, isopropoxy, and trifluoromethoxy;

wherein the amide compound has a molecular weight of 500 grams per mole or less; and

wherein the modified ingestible composition is a food for human or animal consumption.

Assignments (3)
MERGER Recorded Dec 31, 2019
From: SENOMYX, INC.
To: FIRMENICH INCORPORATED
Reel/Frame 051394/0618 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2019
From: ROGERS, DANIEL H.
To: SENOMYX, INC.
Reel/Frame 049923/0615 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2019
From: TACHDJIAN, CATHERINE; PATRON, ANDREW P.; ADAMSKI-WERNER, SARA L.; BAKIR, FARID; CHEN, QING; DARMOHUSODO, VINCENT; HOBSON, STEPHEN TERRENCE; LI, XIAODONG; QI, MING; RINNOVA, MARKETA; SERVANT, GUY; TANG, XIAO-QING; ZOLLER, MARK; WALLACE, DAVID; XING, AMY; GUBERNATOR, KLAUS
To: SENOMYX, INC.
Reel/Frame 049926/0558 →
Continuity (7)
Division 14509761 · Oct 8, 2014
Division 13336272 · Dec 23, 2011
Division 12257017 · Oct 23, 2008
Division 10913303 · Aug 6, 2004
Provisional Application 60552064 · Mar 9, 2004
Provisional Application 60494071 · Aug 6, 2003
Related Publication 20180364220A1 · Dec 20, 2018