IP Library Granted Patent US 10,625,178
Granted Patent B2
US 10,625,178 · App. 16/120,727 · Granted Apr 21, 2020

Removal of organic solvents from aqueous process streams

Inventors: Markku Kuosa (Lappeenranta, FI); Antti Häkkinen (Lappeenranta, FI); Leena Tanttu (Lappeenranta, FI); Timo Jauhiainen (Lappeenranta, FI); Bjarne Ekberg (Turku, FI)
Assignee: OUTOTEC (FINLAND) OY
B01D17/10B01D17/04B01D17/045B01D24/105B01D39/06C22B3/0005C22B3/04C25C1/00B01D2239/1241C02F1/40C02F2103/16Y02P10/234
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 10,625,178
App. No.
16/120,727
Granted
Apr 21, 2020
Kind
B2
Abstract

A method for separating organic solvent(s) from an aqueous process stream including organic solvent(s), includes passing the aqueous stream including organic solvent(s) through a granular bed including glass granules, wherein at least 90% of said glass granules have a maximum particle diameter smaller than 1.0 mm.

Claims (24)

1. A method for separating organic solvent(s) from an aqueous process stream comprising organic solvent(s), the method comprising:

passing said aqueous process stream comprising organic solvent(s) through a granular bed comprising glass granules, wherein at least 90% of said glass granules have a maximum particle diameter smaller than 1.0 mm, and wherein

said aqueous process stream comprises organic solvent(s) is an electrolyte solution resulting from a metal leaching process.

2. The method as claimed in claim 1 , wherein the cross section filtration velocity is from 10 to 80 m/h.

3. The method as claimed in claim 1 , wherein at least 90% of said glass granules have a maximum particle diameter smaller than 0.85 mm.

4. The method as claimed in claim 1 , wherein at least 50% of said glass granules have a maximum particle diameter greater than 0.1 mm.

5. The method as claimed in claim 1 , wherein at least 90% of said glass granules have a maximum particle diameter greater than 0.2 mm.

6. The method as claimed in claim 1 , wherein at least 80% of said glass granules have a maximum particle diameter smaller than 0.7 mm.

7. The method as claimed in claim 1 , wherein at least 50% of said glass granules have a maximum particle diameter smaller than 0.6 mm.

8. The method as claimed in claim 1 , wherein at least 50% of said glass granules have a maximum particle diameter from 0.3 to 0.7 mm.

9. The method as claimed in claim 1 , wherein said glass granules are spherical.

10. A method of using glass particles for separating organic solvent(s) from an aqueous process stream comprising organic solvent(s), comprising:

utilizing glass granules wherein at least 90% of said glass granules have a maximum particle diameter smaller than 1.0 mm, and wherein

the aqueous process stream comprising organic solvent(s) is an electrolyte solution resulting from a metal leaching process.

11. The method as claimed in claim 10 , wherein at least 90% of said glass granules have a maximum particle diameter smaller than 0.85 mm.

12. The method as claimed in claim 10 , wherein at least 50% of said glass granules have a maximum particle diameter greater than 0.2 mm.

13. The method as claimed in claim 10 , wherein at least 50% of said glass granules have a maximum particle diameter from 0.3 to 0.7 mm.

14. The method as claimed in claim 10 , wherein said glass granules are spherical.

15. A method for recovering metal(s) from a starting material comprising said metal(s), comprising:

(i) leaching the starting material in a leaching solution to obtain a pregnant leaching solution;

(ii) extracting the metal(s) from the pregnant leaching solution by a extraction solution comprising organic solvent(s) to obtain an organic solution comprising the metal(s);

(iii) stripping metals(s) from the organic solution comprising the metal(s) with an aqueous solution to obtain an electrolyte solution comprising said metal(s);

(iv) removing any remaining organic solvent(s) from the electrolyte solution by the method claimed in claim 1 , to obtain a purified electrolyte solution; and

(v) recovering metal(s) from the purified electrolyte solution.

Assignments (4)
CHANGE OF NAME Recorded Sep 19, 2025
From: METSO OUTOTEC FINLAND OY
To: METSO FINLAND OY
Reel/Frame 072909/0754 →
MERGER Recorded Oct 16, 2022
From: OUTOTEC (FINLAND) OY
To: METSO MINERALS OY
Reel/Frame 061685/0481 →
CHANGE OF NAME Recorded Oct 16, 2022
From: METSO MINERALS OY
To: METSO OUTOTEC FINLAND OY
Reel/Frame 061685/0552 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 14, 2018
From: KUOSA, MARKKU; HÄKKINEN, ANTTI; TANTTU, LEENA; JAUHIAINEN, TIMO; EKBERG, BJARNE
To: OUTOTEC (FINLAND) OY
Reel/Frame 046876/0435 →