IP Library Granted Patent US 10,744,078
Granted Patent B2
US 10,744,078 · App. 16/140,288 · Granted Aug 18, 2020

Compositions and methods for topical application and transdermal delivery of botulinum toxins

Inventors: Michael D Dake (Stanford, CA); Jacob M Waugh (Palo Alto, CA)
Assignee: REVANCE THERAPEUTICS, INC.
A61K8/64A61K9/00A61K9/0014A61K38/4893A61K47/34A61Q19/08A61K9/0019A61K2800/56C12Y304/24069
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Quick Facts
Patent No.
US 10,744,078
App. No.
16/140,288
Granted
Aug 18, 2020
Kind
B2
Abstract

Improved formulations for transdermal delivery of botulinum toxin are disclosed. The formulations include, for example, botulinum toxin non-covalently associated with a positively charged backbone having branching or efficiency groups. The formulations also include a partitioning agent, oligo-bridge, or polyanion bridge, and may optionally contain a viscosity modifying agent. The formulations are designed for topical application onto the skin of a patient and may be used to treat wrinkles, hyperhidrosis, and other health-related problems. Kits for administration are also described.

Claims (26)

1. A method of treating hyperhidrosis in a patient in need thereof, said method comprising:

topically administering to an affected area of the patient in need of treatment, a pharmaceutically acceptable composition comprising:

botulinum toxin,

a carrier comprising a positively charged polymeric backbone with positively charged efficiency groups covalently attached thereto;

a poloxamer; and

a dermatologically or pharmaceutically acceptable excipient, diluent, or medium;

wherein the botulinum toxin is non-covalently associated with the positively charged polymeric backbone; and wherein the carrier comprising the positively charged backbone is the sole necessary agent for non-covalently associating with the botulinum toxin and delivering the botulinum toxin to the affected area so as to treat the hyperhidrosis in said patient.

2. The method according to claim 1 , wherein the hyperhidrosis is selected from one or more of axillary hyperhidrosis and forehead hyperhidrosis.

3. The method according to claim 1 , wherein the positively charged polymeric backbone is polylysine and the positively charged efficiency groups are amino acid sequences selected from the group consisting of (gly)p-RGRDDRRQRRR-(gly)q (SEQ ID NO: 2), (gly)p-YGRKKRRQRRR-(gly)q (SEQ ID NO: 3), and (gly)p-RKKRRQRRR-(gly)q (SEQ ID NO: 4), wherein the subscripts p and q are each independently an integer of from 0 to 20.

4. The method according to claim 1 , wherein the positively charged polymeric backbone is polylysine and the positively charged efficiency groups include amino acid sequence (gly)p-RGRDDRRQRRR-(gly)q (SEQ ID NO: 2), wherein the subscripts p and q are each independently an integer of from 2 to 5.

5. The method according to claim 1 , wherein the positively charged polymeric backbone is polylysine and the positively charged efficiency groups include amino acid sequence (gly)p-YGRKKRRQRRR-(gly)q (SEQ ID NO: 3), wherein the subscripts p and q are each independently an integer of from 2 to 5.

6. The method according to claim 1 , wherein the positively charged polymeric backbone is polylysine and the positively charged efficiency groups include amino acid sequence (gly)p-RKKRRQRRR-(gly)q (SEQ ID NO: 4), wherein the subscripts p and q are each independently an integer of from 2 to 5.

7. The method according to claim 4 , wherein the botulinum toxin is of serotype A.

8. The method according to claim 5 , wherein the botulinum toxin is of serotype A.

9. The method according to claim 6 , wherein the botulinum toxin is of serotype A.

10. The method according to claim 7 , wherein the botulinum toxin has a molecular weight of 150,000.

11. The method according to claim 8 , wherein the botulinum toxin has a molecular weight of 150,000.

12. The method according to claim 9 , wherein the botulinum toxin has a molecular weight of 150,000.

13. The method according to claim 7 , wherein the amino acid sequence is attached to the polylysine via either the C-terminus or the N-terminus of the amino acid sequence.

14. The method according to claim 8 , wherein the amino acid sequence is attached to the polylysine via either the C-terminus or the N-terminus of the amino acid sequence.

15. The method according to claim 9 , wherein the amino acid sequence is attached to the polylysine via either the C-terminus or the N-terminus of the amino acid sequence.

16. The method according to claim 3 , wherein the composition comprises botulinum toxin of serotype, and polylysine having covalently attached thereto positively charged efficiency groups having the amino acid sequence (gly)p-RKKRRQRRR-(gly)q (SEQ ID NO. 4), wherein the subscripts p and q are each independently an integer of from 0 to 20.

17. The method according to claim 16 , wherein the positively charged efficiency groups comprise from about 0.1% to about 30% by weight of the total carrier weight in the composition.

18. The method according to claim 16 , wherein the polylysine has a molecular weight of about 21,000.

19. The method according to claim 16 , wherein the botulinum toxin of serotype A has a molecular weight of 150,000.

20. The method according to claim 1 , wherein the dermatologically or pharmaceutically acceptable excipient, diluent, or medium is an aqueous diluent comprising a saline solution of 15% poloxamer, and wherein the carrier and the botulinum toxin are present in the saline solution in a ratio corresponding to 0.5 μg carrier to 100 U of toxin.

Assignments (6)
SECURITY INTEREST Recorded Feb 17, 2025
From: REVANCE THERAPEUTICS, INC.
To: JPMORGAN CHASE BANK, N.A.
Reel/Frame 070239/0739 →
RELEASE OF SECURITY INTEREST Recorded Feb 7, 2025
From: ATHYRIUM BUFFALO LP
To: REVANCE THERAPEUTICS, INC
Reel/Frame 070153/0630 →
SECURITY INTEREST Recorded Feb 7, 2025
From: REVANCE THERAPEUTICS, INC.; CROWN LABORATORIES, INC.
To: HAYFIN SERVICES LLP, AS ADMINISTRATIVE AGENT
Reel/Frame 070153/0663 →
SECURITY INTEREST Recorded Feb 7, 2025
From: REVANCE THERAPEUTICS, INC.; BELLUS MEDICAL, LLC; CROWN LABORATORIES, INC.
To: HAYFIN SERVICES LLP, AS ADMINISTRATIVE AGENT
Reel/Frame 070153/0736 →
SECURITY INTEREST Recorded Mar 18, 2022
From: REVANCE THERAPEUTICS, INC.
To: ATHYRIUM BUFFALO LP
Reel/Frame 059437/0654 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 25, 2019
From: DRAKE, MICHAEL D.; WAUGH, JACOB M.
To: REVANCE THERAPEUTICS, INC.
Reel/Frame 048989/0460 →