Method for synthesizing high-purity montmorillonite
A method for synthesizing high purity montmorillonite is disclosed. According to this synthesis method, bentonite is dissolved in aqua regia to produce a solution and then sodium hydroxide (NaOH) is added to the solution to produce a mixed solution. Then, the mixed solution is kept in a sealed state at a temperature of 90° C. inclusive to 100° C. exclusive to synthesize montmorillonite crystals.
1. A method for synthesizing montmorillonite, the method comprising:
dissolving bentonite in aqua regia to produce a first solution;
adding sodium hydroxide (NaOH) to the first solution to produce a mixed solution; and
maintaining the mixed solution at a temperature of 90° C. inclusive to 100° C. exclusive to synthesize montmorillonite crystals,
wherein adding the sodium hydroxide (NaOH) to the first solution includes adding to the first solution a sodium hydroxide aqueous solution having a concentration of 3 M to 7 M and
wherein the sodium hydroxide aqueous solution is added to the first solution so that pH of the mixed solution is in a range of 11 to 13.
2. The method of claim 1 , wherein the bentonite includes finely-pulverized particles made of natural bentonite, each particle having a size of 2 mm or smaller,
wherein the aqua regia includes a mixture of hydrochloric acid (HCl) and nitric acid (HNO 3 ) at a molar ratio of about 1:3.
3. The method of claim 1 , wherein maintaining the mixed solution includes maintaining the mixed solution in a sealed state for about 20 to 30 hours.
4. The method of claim 1 , wherein the synthesized montmorillonite crystals have a specific surface area of about 125 to 135 cm 2 /g.