IP Library Granted Patent US 10,953,080
Granted Patent B2
US 10,953,080 · App. 16/166,455 · Granted Mar 23, 2021

Oil-based adjuvants

Inventors: Paul Joseph Dominowski (Kalamazoo, MI); Dennis L. Foss (Mattawan, MI); Guillermo Gallo (Kalamazoo, MI); John Morgan Hardham (Kalamazoo, MI); Richard Lee Krebs (Ashland, NE); Sandra Ann Marie Lightle (Kalamazoo, MI); Suman Mahan (Kalamazoo, MI); Sangita Mediratta (Kalamazoo, MI); Kaori Mohr (Kalamazoo, MI); Duncan Mwangi (Portage, MI); Sharath K. Rai (Portage, MI); Sarah A. Salmon (Kalamazoo, MI); Shaunak Vora (Kalamazoo, MI); Lauren Wilmes (Lincoln, NE)
Assignee: Zoetis Services LLC
A61K39/092A61K39/0002A61K39/002A61K39/0003A61K39/0005A61K39/012A61K39/0258A61K39/05A61K39/08A61K39/085A61K39/118A61K39/12A61K39/39G01N33/56944A61K2039/552A61K2039/55561A61K2039/55566A61K2039/55572A61K2039/55577A61K2039/55583G01N2333/315G01N2469/10Y02A50/30
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Quick Facts
Patent No.
US 10,953,080
App. No.
16/166,455
Granted
Mar 23, 2021
Kind
B2
Abstract

The instant invention provides various formulations comprising combinations of immunostimulating oligonucleotides, polycationic carriers, sterols, saponins, quaternary amines, TLR-3 agonists, glycolipids, and MPL-A or analogs thereof in oil emulsions, use thereof in preparations of immunogenic compositions and vaccines, and use thereof in the treatment of animals.

Claims (16)

1. An adjuvant formulation comprising an oily phase and an aqueous phase, wherein the oily phase comprises at least 36% of the formulation v/v, wherein said formulation comprises monophosphoryl lipid A (MPL-A) or an analog thereof and an immunostimulatory oligonucleotide, wherein said adjuvant formulation is a water-in-oil emulsion.

2. The adjuvant formulation of claim 1 , wherein

the immunostimulatory oligonucleotide is a CpG or an oligoribonucleotide; and

said formulation further comprises a polycationic carrier, wherein the polycationic carrier is selected from the group consisting of dextran, dextran DEAE (and derivatives thereof), PEGs, guar gums, chitosan derivatives, polycellulose derivatives like hydroxyethyl cellulose (HEC) polyethylenimene, poly aminos.

3. The adjuvant formulation according to claim 1 , further comprising a glycolipid according to formula I

wherein, R 1 is hydrogen, or a saturated alkyl radical having up to 20 carbon atoms; X is —CH 2 —, —O— or —NH—; R 2 is hydrogen, or a saturated or unsaturated alkyl radical having up to 20 carbon atoms; R 3 , R 4 , and R 5 are independently hydrogen, —SO 4 2− , —PO 4 2− , —COC 1-10 alkyl; R 6 is L-alanyl, L-alpha-aminobutyl, L-arginyl, L-asparginyl, L-aspartyl, L-cysteinyl, L-glutamyl, L-glycyl, L-histidyl, L-hydroxyprolyl, L-isoleucyl, L-leucyl, L-lysyl, L-methionyl, L-ornithinyl, L-phenyalany, L-prolyl, L-seryl, L-threonyl, L-tyrosyl, L-tryptophanyl, and L-valyl or their D-isomers.

4. The adjuvant formulation of claim 3 , wherein the glycolipid is N-(2-Deoxy-2-L-leucylamino-β-D-glucopyranosyl)-N-octadecyldodecanoylamide or a salt thereof.

5. The adjuvant formulation of claim 1 , further comprising a sterol.

6. The adjuvant formulation of claim 5 , further comprising a saponin.

7. The adjuvant formulation of claim 5 , wherein the sterol is selected from the group consisting of ergosterol, lanosterol and cholesterol.

8. The adjuvant formulation of claim 1 , comprising the source of aluminum, which is an aluminum hydroxide gel.

9. A vaccine composition comprising an effective amount of an antigen and the adjuvant formulation according to claim 1 , wherein the oily phase of the composition is at least 40%.

10. The adjuvant formulation of claim 1 , wherein the oily phase comprises over 45% of the vaccine composition v/v.

11. The adjuvant formulation of claim 1 , wherein the oily phase comprises over 50% of the vaccine composition v/v.

12. A vaccine composition comprising the adjuvant formulation according to claim 11 and an effective amount of an antigen, wherein the antigen comprises at least one of viruses, bacteria, parasites, nucleic acid based antigens, polynucleotides, protein extract, cells, tissues, polysaccharides, glycoproteins, carbohydrates, fatty acids, teichioc acid, peptidoglycans, lipids, or glycolipids, and a combination thereof, wherein said vaccine composition is a W/O emulsion.

13. The vaccine composition according to claim 12 , wherein antigen comprises at least one of viruses, bacteria, parasites, lipids, glycolipids or DNA vaccines.

Assignments (4)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 5, 2025
From: ZOETIS LLC
To: ZOETIS SERVICES LLC
Reel/Frame 070407/0113 →
ADDRESS CHANGE OF ASSIGNEE Recorded Mar 5, 2025
From: ZOETIS SERVICES LLC
To: ZOETIS SERVICES LLC
Reel/Frame 070407/0547 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 3, 2024
From: DOMINOWSKI, PAUL JOSEPH; FOSS, DENNIS L.; GALLO, GUILLERMO; HARDHAM, JOHN MORGAN; KREBS, RICHARD LEE; LIGHTLE, SANDRA ANN MARIE; MAHAN, SUMAN; MEDIRATTA, SANGITA; MOHR, KAORI; MWANGI, DUNCAN; RAI, SHARATH K.; SALMON, SARAH A.; VORA, SHAUNAK
To: ZOETIS LLC
Reel/Frame 066995/0285 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 3, 2024
From: WILMES, LAUREN
To: ZOETIS LLC
Reel/Frame 066995/0949 →